WO1998020365A1 - Ultraviolet light illumination and viewing system and method for fluorescent dye leak detection - Google Patents

Ultraviolet light illumination and viewing system and method for fluorescent dye leak detection Download PDF

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Publication number
WO1998020365A1
WO1998020365A1 PCT/US1997/019841 US9719841W WO9820365A1 WO 1998020365 A1 WO1998020365 A1 WO 1998020365A1 US 9719841 W US9719841 W US 9719841W WO 9820365 A1 WO9820365 A1 WO 9820365A1
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WO
WIPO (PCT)
Prior art keywords
light
ultraviolet
wavelengths
filter
fluorescing
Prior art date
Application number
PCT/US1997/019841
Other languages
French (fr)
Inventor
Kenneth J. Kranz
Original Assignee
Corrosion Consultants, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Corrosion Consultants, Inc. filed Critical Corrosion Consultants, Inc.
Priority to EP97947315A priority Critical patent/EP0983522A1/en
Priority to AU52429/98A priority patent/AU5242998A/en
Priority to JP52160298A priority patent/JP3434518B2/en
Publication of WO1998020365A1 publication Critical patent/WO1998020365A1/en

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64—Fluorescence; Phosphorescence
    • G01N21/6447—Fluorescence; Phosphorescence by visual observation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/88—Investigating the presence of flaws or contamination
    • G01N21/91—Investigating the presence of flaws or contamination using penetration of dyes, e.g. fluorescent ink

Definitions

  • This invention concern liquid leak detection methods and more particularly leak detection using dyes which fluoresce when illuminated by light of particular wavelengths, typically ultraviolet light, commonly referred to as "black light”.
  • Ultraviolet light sources are commonly employed for such uses as disinfection, prospecting, document examination, dental work curing, as well as leak detection.
  • the fluorescing dye is typically mixed with lubricating oil which in turn is mixed with fluid in the equipment being inspected, such as in the refrigerant of an air conditioning system.
  • the dye in the fluid leaked out will fluoresce when illuminated with ultraviolet light, so that the leaked fluid will be readily visible.
  • Such dyes will fluoresce or emit light at certain visible band wavelengths, when excited by shorter wavelength ultraviolet light.
  • a powerful light source emitting light at the proper wavelength should desirably be used, which source does not also emit visible light.
  • This overheating can crack or shorten the lens, particularly if water drops impinge on the lens, the shattered glass presenting a hazard to the user.
  • reflectors In attempting to create a more powerful light source, reflectors are commonly provided which concentrate and direct ultraviolet wavelength light emitted from a quartz envelope lamps. Prior art reflectors have typically been crudely formed and had low efficiency due to destruction interference set up by protective coatings such as silicon dioxide.
  • a system comprised of an improved parabolic reflector and filter associated with an ultraviolet lamp, combined with viewing eyeglasses which filter certain visible wavelengths for achieving maximum contrast of the fluorescing light emitted from a dye exposed to the illumination by a leak.
  • the improved reflector has an accurately formed parabolic shape. Two coatings of precisely control thickness applied to the reflecting surface and having substantially different refraction induces. These coatings minimize the interference of a reflected ultraviolet light beam with the incident light beam by inducing offsetting phase shifts such that the reflected light is closely in phase with the incident light.
  • the ultraviolet light source is preferably a quartz envelop tungsten halogen lamp mounted at the focal point of the reflector parabola.
  • the ultraviolet light beam from the reflection is then passed through an optical filter to selectively remove visible light from the reflected light beam by a process of selective reflectance rather than absorbance so as to minimize heat build up in the filter, as has occurred in previous light absorbing filters used for removing visible light.
  • a series of coatings are applied to a borosilicate glass disc in order to achieve this.
  • Successive coating layers of high and low refraction indices are used to produce selective reflectance of a wavelength band above the ultraviolet wavelengths but shorter than the infrared band, i.e., from 475 nm to 700 n .
  • the infrared light is transmitted through the filter to reduce heating of the confined space behind the filter.
  • the final element of the system is a pair of filtering viewing eyeglasses which absorb wavelengths just below the wavelength of the fluorescing light in order to block wavelengths of the illuminating light in this band, to increase the contrast and visibility of the fluorescence of the illuminated dye to the viewer' s eye.
  • FIG. 1 is a diagram of the main components of the system according to the present invention.
  • Figure 2 is an enlarged fragmentary section of the parabolic reflector component.
  • DETAILED DESCRIPTION In the following detailed description, certain specific terminology will be employed for the sake of clarity and a particular embodiment described in accordance with the requirements of 35 USC 112, but it is to be understood that the same is not intended to be limiting and should not be so construed inasmuch as the invention is capable of taking many forms and variations within the scope of the appended claims.
  • the system according to the present invention uses a portable ultraviolet light source not unlike a flashlight, which includes a parabolically shaped reflector 10 mounted in a housing 12, (a portion only shown in fragmentary form) which in turn mounts a lamp 12 located approximately at the focal point of the parabolic shape.
  • the lamp 12 is preferably a Xenon lamp of high color temperature (>3500K) , which produces substantial long wave ultraviolet light emissions.
  • the envelop is made of quartz which is itself highly transmittive to such long wave ultraviolet light.
  • the lamp 14 is also relatively compact allowing it to be placed at the focal point of the reflector parabolic shape.
  • a suitable bulb is available as part number FCR64625HLX from Osram Sylvania.
  • the parabolic reflector is precision electroformed of nickel on an accurately shaped stainless steel mandrel.
  • a focal point of 0.187 inches allows the lamp 14 to be approximately located at the focal point of the parabolic to maximize beam concentration.
  • the lamp 14 is powered by a suitable power supply 16 which may consist of a transformer reducing 110 vac (or 220 vac) to 12 vac.
  • a 12 volt dc power supply such as an auto battery may also be used.
  • the lamp 12 draws 100 watts of power such that a high power source will be required, substantially greater than that required for a typical flashlight.
  • a relay operated by a normally off spring biased switch (not shown) is used to turn the lamp 14 on and off, to minimize the on time of the lamp 14.
  • the reflecting surface 18 of the parabolic reflector 12 has a double layer of coatings, which are designed to eliminate the destructive interference caused by refraction of the interface of each media through which the light passes in being reflected from the surface 18. Refraction of short wavelength ultraviolet light would normally cause a phase difference to develop between the incident and reflective light beam, setting up a destructive interference and reducing the intensity of the reflected ultraviolet light.
  • the surface 18 is given coatings, one of aluminum and one of silicon dioxide. The interface of silicon dioxide and air, and silicon dioxide and aluminum produces a double refraction in an opposite sense, which offset each other to eliminate the potential destructive interference which would otherwise could occur.
  • the first coating 18A is of aluminum, while the second coating
  • 18B is of silicon dioxide (Figure 2) .
  • the thickness of the silicon dioxide should be uniform and accurately held to achieve this effect, the thicknesses determined by the "quarter stack" principle.
  • each interface i.e., the silicon dioxide and air, silicon dioxide and aluminum determines the effective phase shift of the reflected light.
  • a thickness of aluminum of .057 microns and of silicon dioxide of .066 microns has been successfully used for this purpose.
  • the silicon dioxide-air interface causes an approximate 13 degree forward phase shift, the silicon dioxide-aluminum interface a 13 degree lagging phase shift, thereby offsetting each other.
  • Silicon dioxide coatings have heretofore been employed simply to protect the substrate from scratches and oxidation but have not been sufficiently uniform nor of the proper thickness to achieve enhanced reflection of ultraviolet wavelengths.
  • a coated parabolic reflector suitable for this use is available from American Galvano, 312 N. Cota St., Unit 1, Corona, California 91720.
  • a glass disc filter 20 is another component of the system of the present invention which is mounted to receive the ultraviolet beam emanating from the lamp 12 and the parabolic surface 18.
  • the filter 20 is designed to reduce the visible light component of the ultraviolet light received from the lamp 12 and reflector 14.
  • Such filters have been employed in the past but have typically been designed to absorb visible light to prevent its transmittance. This results in excessive heating of the lens when used with high intensity light sources, making it vulnerable to cracking or shattering, as when contacted with water drops due to rapid cooling of localized areas of the glass. According to the concept of the present invention, coatings are applied which cause reflection of the visible light ranges rather then absorbance, greatly reducing heating of the lens 20.
  • the filter 20 itself is preferably of borosilicate glass, commercially available as "Pyrex" (TM) , which has a very low coefficient of thermal expansion to thus minimize cracking from thermal shock.
  • TM borosilicate glass
  • the fluorescing dyes typically used for leak detection have an excitation range of ultraviolet light of wavelengths 320 nm to 475 nm. When excited by such ultraviolet light, fluorescing light of 495 to 500 nm is emitted.
  • Light over 700 nm is in the invisible infrared range, which is allowed to be transmitted out of the confined space through the filter 20 to avoid overheating particularly of the reflector 14.
  • McCloud two layers of high and low refractive indices may be stacked to cause reflection of wavelengths only from 475 nm to 700 nm, allowing transmission of wavelengths from 320 nm to 475 nm and 700 nm to 1300 nm.
  • the stack may be formed by the filter and a coating on the inside surface of the filter 20, which may be of titanium oxide.
  • the glass and titanium oxide are of a thickness necessary to reflect the wavelength ranges described.
  • coatings may be applied in various thicknesses, such as magnesium fluoride, which may also be applied to the other surface of the borosilicate to eliminate any residual transmitted visible lights.
  • the general methodology is to create a bandwidth of reflected light above 475 nm extending approximately to 700 nm. The mean wavelength around which this bandwidth is centered would be 537.5 nm and a reflected bandwidth of 225 nm should therefore be employed.
  • a suitable reflecting-transmitting filter lens for this purpose is available from:
  • the system also involves the use of special viewing glasses 24 which are designed to absorb light wavelengths from 400 to 480 nm so that illuminating light from the source in those ranges reflecting from the inspected body 26 does not mask the emitted fluorescing light wavelengths which are in the 495 to 500 nm range emitted from the illuminated dye in the leaked liquid 28.
  • Such narrow band blocking eyeglass lenses are available from:

Abstract

An illumination and viewing system and method for detecting leaks by observing material (26) caused to fluoresce by being illuminated by a beam of ultraviolet light. The beam is concentrated by a parabolic reflector (10) coated to maximize ultraviolet reflection, and then passed through a filter (20) which reflects visible wavelengths while allowing transmission of ultraviolet and IR wavelengths. The fluorescing light is viewed through eyeglasses (24) which block wavelengths just below the wavelengths of the emitted fluorescing light.

Description

ULTRAVIOLET LIGHT ILLUMINATION AND VIEWING SYSTEM AND METHOD FOR FLUORESCENT DYE LEAK DETECTION
BACKGROUND OF THE INVENTION
This invention concern liquid leak detection methods and more particularly leak detection using dyes which fluoresce when illuminated by light of particular wavelengths, typically ultraviolet light, commonly referred to as "black light".
Ultraviolet light sources are commonly employed for such uses as disinfection, prospecting, document examination, dental work curing, as well as leak detection.
The fluorescing dye is typically mixed with lubricating oil which in turn is mixed with fluid in the equipment being inspected, such as in the refrigerant of an air conditioning system.
If a leak is present, the dye in the fluid leaked out will fluoresce when illuminated with ultraviolet light, so that the leaked fluid will be readily visible.
Such dyes will fluoresce or emit light at certain visible band wavelengths, when excited by shorter wavelength ultraviolet light.
In order to make such leak detection easy and reliable, particularly under bright light ambient conditions, a powerful light source emitting light at the proper wavelength should desirably be used, which source does not also emit visible light.
If visible light is reflected from the surface being inspected, it will render the fluorescing light less conspicuous. Currently available light sources are not of sufficient intensity and also emit significant visible wavelengths such that the contrast of the fluorescent light with the visible reflected light is not great enough for reliable observation. An overheating problem is also encountered in attempting to eliminate visible light by absorption in a filter lens.
This overheating can crack or shorten the lens, particularly if water drops impinge on the lens, the shattered glass presenting a hazard to the user.
In attempting to create a more powerful light source, reflectors are commonly provided which concentrate and direct ultraviolet wavelength light emitted from a quartz envelope lamps. Prior art reflectors have typically been crudely formed and had low efficiency due to destruction interference set up by protective coatings such as silicon dioxide.
It is the object of the present invention to provide a system for ultraviolet light illumination of enhanced intensity for fluorescent leak detection to allow easier and more reliable viewing of fluorescent light emitted from a dye.
It is another object of the present invention to provide an ultraviolet light source which emits an intense ultraviolet beam directed through a glass filter so as to eliminate visible wavelengths but without producing heating of the glass filter. SUMMARY OF THE INVENTION
The above objects and others which will become apparent upon a reading of the following specification and claims are achieved by a system comprised of an improved parabolic reflector and filter associated with an ultraviolet lamp, combined with viewing eyeglasses which filter certain visible wavelengths for achieving maximum contrast of the fluorescing light emitted from a dye exposed to the illumination by a leak. The improved reflector has an accurately formed parabolic shape. Two coatings of precisely control thickness applied to the reflecting surface and having substantially different refraction induces. These coatings minimize the interference of a reflected ultraviolet light beam with the incident light beam by inducing offsetting phase shifts such that the reflected light is closely in phase with the incident light. This result maximizes the intensity of the reflected ultraviolet light beam by minimizing destructive interference between the incident and reflected light beams which could otherwise occur. The ultraviolet light source is preferably a quartz envelop tungsten halogen lamp mounted at the focal point of the reflector parabola.
The ultraviolet light beam from the reflection is then passed through an optical filter to selectively remove visible light from the reflected light beam by a process of selective reflectance rather than absorbance so as to minimize heat build up in the filter, as has occurred in previous light absorbing filters used for removing visible light.
A series of coatings are applied to a borosilicate glass disc in order to achieve this. Successive coating layers of high and low refraction indices are used to produce selective reflectance of a wavelength band above the ultraviolet wavelengths but shorter than the infrared band, i.e., from 475 nm to 700 n .
The infrared light is transmitted through the filter to reduce heating of the confined space behind the filter.
The final element of the system is a pair of filtering viewing eyeglasses which absorb wavelengths just below the wavelength of the fluorescing light in order to block wavelengths of the illuminating light in this band, to increase the contrast and visibility of the fluorescence of the illuminated dye to the viewer' s eye.
The overall result is to produce an intense beam of ultraviolet light containing minimal visible wavelength light using practical components. The fluorescent light is thus strong and is not masked by the incidence of reflected visible light from the illuminating beam. DESCRIPTION OF THE DRAWINGS Figure 1 is a diagram of the main components of the system according to the present invention.
Figure 2 is an enlarged fragmentary section of the parabolic reflector component. DETAILED DESCRIPTION In the following detailed description, certain specific terminology will be employed for the sake of clarity and a particular embodiment described in accordance with the requirements of 35 USC 112, but it is to be understood that the same is not intended to be limiting and should not be so construed inasmuch as the invention is capable of taking many forms and variations within the scope of the appended claims.
The system according to the present invention uses a portable ultraviolet light source not unlike a flashlight, which includes a parabolically shaped reflector 10 mounted in a housing 12, (a portion only shown in fragmentary form) which in turn mounts a lamp 12 located approximately at the focal point of the parabolic shape. The lamp 12 is preferably a Xenon lamp of high color temperature (>3500K) , which produces substantial long wave ultraviolet light emissions. The envelop is made of quartz which is itself highly transmittive to such long wave ultraviolet light. The lamp 14 is also relatively compact allowing it to be placed at the focal point of the reflector parabolic shape. A suitable bulb is available as part number FCR64625HLX from Osram Sylvania.
The parabolic reflector is precision electroformed of nickel on an accurately shaped stainless steel mandrel.
A focal point of 0.187 inches allows the lamp 14 to be approximately located at the focal point of the parabolic to maximize beam concentration.
The lamp 14 is powered by a suitable power supply 16 which may consist of a transformer reducing 110 vac (or 220 vac) to 12 vac.
A 12 volt dc power supply such as an auto battery may also be used. The lamp 12 draws 100 watts of power such that a high power source will be required, substantially greater than that required for a typical flashlight. Preferably, a relay operated by a normally off spring biased switch (not shown) is used to turn the lamp 14 on and off, to minimize the on time of the lamp 14. The reflecting surface 18 of the parabolic reflector 12 has a double layer of coatings, which are designed to eliminate the destructive interference caused by refraction of the interface of each media through which the light passes in being reflected from the surface 18. Refraction of short wavelength ultraviolet light would normally cause a phase difference to develop between the incident and reflective light beam, setting up a destructive interference and reducing the intensity of the reflected ultraviolet light. The surface 18 is given coatings, one of aluminum and one of silicon dioxide. The interface of silicon dioxide and air, and silicon dioxide and aluminum produces a double refraction in an opposite sense, which offset each other to eliminate the potential destructive interference which would otherwise could occur.
The first coating 18A is of aluminum, while the second coating
18B is of silicon dioxide (Figure 2) . The thickness of the silicon dioxide should be uniform and accurately held to achieve this effect, the thicknesses determined by the "quarter stack" principle.
The refractive index of each interface, i.e., the silicon dioxide and air, silicon dioxide and aluminum determines the effective phase shift of the reflected light. A thickness of aluminum of .057 microns and of silicon dioxide of .066 microns has been successfully used for this purpose. The silicon dioxide-air interface causes an approximate 13 degree forward phase shift, the silicon dioxide-aluminum interface a 13 degree lagging phase shift, thereby offsetting each other.
Silicon dioxide coatings have heretofore been employed simply to protect the substrate from scratches and oxidation but have not been sufficiently uniform nor of the proper thickness to achieve enhanced reflection of ultraviolet wavelengths.
A coated parabolic reflector suitable for this use is available from American Galvano, 312 N. Cota St., Unit 1, Corona, California 91720.
A glass disc filter 20 is another component of the system of the present invention which is mounted to receive the ultraviolet beam emanating from the lamp 12 and the parabolic surface 18. The filter 20 is designed to reduce the visible light component of the ultraviolet light received from the lamp 12 and reflector 14.
Such filters have been employed in the past but have typically been designed to absorb visible light to prevent its transmittance. This results in excessive heating of the lens when used with high intensity light sources, making it vulnerable to cracking or shattering, as when contacted with water drops due to rapid cooling of localized areas of the glass. According to the concept of the present invention, coatings are applied which cause reflection of the visible light ranges rather then absorbance, greatly reducing heating of the lens 20.
The filter 20 itself is preferably of borosilicate glass, commercially available as "Pyrex" (TM) , which has a very low coefficient of thermal expansion to thus minimize cracking from thermal shock.
The fluorescing dyes typically used for leak detection have an excitation range of ultraviolet light of wavelengths 320 nm to 475 nm. When excited by such ultraviolet light, fluorescing light of 495 to 500 nm is emitted.
It is thus desirable to allow maximum transmitting of the exciting wavelengths from 320 nm to 475 nm while reflecting wavelengths from 475 nm to 700 nm.
Light over 700 nm is in the invisible infrared range, which is allowed to be transmitted out of the confined space through the filter 20 to avoid overheating particularly of the reflector 14.
Particular coatings are applied to cause the filter 20 to reflect visible light above 475 nm and below 700 nm. Using the "quarterwave stack" principle developed by P. H.
McCloud, two layers of high and low refractive indices may be stacked to cause reflection of wavelengths only from 475 nm to 700 nm, allowing transmission of wavelengths from 320 nm to 475 nm and 700 nm to 1300 nm.
The stack may be formed by the filter and a coating on the inside surface of the filter 20, which may be of titanium oxide.
The glass and titanium oxide are of a thickness necessary to reflect the wavelength ranges described.
Other coatings may be applied in various thicknesses, such as magnesium fluoride, which may also be applied to the other surface of the borosilicate to eliminate any residual transmitted visible lights. The general methodology is to create a bandwidth of reflected light above 475 nm extending approximately to 700 nm. The mean wavelength around which this bandwidth is centered would be 537.5 nm and a reflected bandwidth of 225 nm should therefore be employed. A suitable reflecting-transmitting filter lens for this purpose is available from:
Z, C & R Coatings for Optics, Inc. 1250 E. 223rd. Street Suite 111 Carson, California 90745
The system also involves the use of special viewing glasses 24 which are designed to absorb light wavelengths from 400 to 480 nm so that illuminating light from the source in those ranges reflecting from the inspected body 26 does not mask the emitted fluorescing light wavelengths which are in the 495 to 500 nm range emitted from the illuminated dye in the leaked liquid 28.
Such narrow band blocking eyeglass lenses are available from:
Noire Medical 6155 Pontiac Trail
South Lyon, Michigan 48178
Thus a powerful ultraviolet illuminating light source is provided, and the fluorescent light generated thereby is highly visible due to the minimization of reflected visible light, blocked by the filter 20 and absorbed in the eyeglasses 24.
This in turn makes leak detection inspections much easier and more reliable even at relatively brightly lit sites.

Claims

1. A system for illuminating an object with ultraviolet light, comprising: an ultraviolet lamp emitting a beam of light containing both ultraviolet and longer wavelengths; a filter positioned to receive said beam of light and transmitting a great proportion ultraviolet light in said beam and reflecting a large proportion of longer visible band wavelength light in said beam.
2. The system according to claim 1 wherein said filter transmits light waves above approximately 700 nm.
3. The system according to claim 1 further including a parabolic reflector, said ultraviolet lamp disposed within said reflector.
4. The system according to claim 3 wherein said ultraviolet lamp is located substantially at a focal point of said parabolic reflector.
5. The system according to claim 4 wherein said parabolic reflector has a reflecting surface coated so as to produce offsetting phase shifts in incident light to minimize destructive interference between an incident beam of ultraviolet light and beam reflected therefrom.
6. The system according to claim 5 wherein coatings of silicon dioxide and aluminum are applied over a substrate forming said parabolic shape.
7. The system according to claim 1 further including viewing eyeglasses absorbing light wavelengths at the longest ultraviolet wavelengths transmitted by said filter.
8. A method of illuminating fluorescing material and viewing light emitted in response to illumination thereof in order to detect the presence of said fluorescing material, comprising the steps of : generating a beam of light containing ultraviolet light of wavelengths causing said material to fluoresce; passing said beam of light through a filter coated to reflect longer visible wavelengths; directing said ultraviolet beam at said material; and viewing fluorescent light emitted by said material.
9. The method according to claim 8 further including the steps of concentrating said beam with a parabolic reflection, and minimizing interference between incident and reflected light by coating said reflector with materials having indices of refraction causing offsetting phase shifts of said incident beam.
10. The method according to claim 8 further including the steps of allowing wavelengths in a range longer than those reflected to be transmitted through said filter.
11. The method according to claim 8 further including the steps of passing said fluorescing light through eyeglasses to remove light close to the fluorescing wavelengths to increase the contrast of said fluorescing light emitted.
12. The method according to claim 11 including the step of preventing light in a range approximately between 400 and 480 nm from passing through said eyeglasses.
PCT/US1997/019841 1996-11-05 1997-11-05 Ultraviolet light illumination and viewing system and method for fluorescent dye leak detection WO1998020365A1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
EP97947315A EP0983522A1 (en) 1996-11-05 1997-11-05 Ultraviolet light illumination and viewing system and method for fluorescent dye leak detection
AU52429/98A AU5242998A (en) 1996-11-05 1997-11-05 Ultraviolet light illumination and viewing system and method for fluorescent dye leak detection
JP52160298A JP3434518B2 (en) 1996-11-05 1997-11-05 Ultraviolet irradiation and inspection system and fluorescent dye leak detection method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US3009296P 1996-11-05 1996-11-05
US60/030,092 1996-11-05

Publications (1)

Publication Number Publication Date
WO1998020365A1 true WO1998020365A1 (en) 1998-05-14

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EP (1) EP0983522A1 (en)
JP (1) JP3434518B2 (en)
AU (1) AU5242998A (en)
WO (1) WO1998020365A1 (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999053299A1 (en) * 1998-04-13 1999-10-21 Brasscorp Ltd. Leak detector using fluorescent dyes
EP1103805A2 (en) * 1999-11-29 2001-05-30 Marktec Corporation Ultraviolet light permeable filter for flaw detection apparatus and method for detection of flaws
US6362488B1 (en) * 1997-11-05 2002-03-26 Corrosion Consultants, Inc. Light source and method for carrying out leak detection inspections
JP2002542919A (en) * 1999-04-23 2002-12-17 アトランティウム エルティディ． Liquid and gas sterilization and purification methods
EP1367413A1 (en) * 2002-05-27 2003-12-03 Canon Kabushiki Kaisha Reflector and linear illumination device
EP1707611A2 (en) 2000-09-08 2006-10-04 Nanosolutions GmbH Synthesis of nanoparticles
US7241399B2 (en) 2000-09-08 2007-07-10 Centrum Fuer Angewandte Nanotechnologie (Can) Gmbh Synthesis of nanoparticles
CN104903745A (en) * 2013-01-08 2015-09-09 斯基恩特-X公司 X-ray scintillator containing a multi-layered coating

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Publication number Priority date Publication date Assignee Title
JP6717325B2 (en) * 2018-02-27 2020-07-01 三菱電機ビルテクノサービス株式会社 Oil leak route identification method for passenger conveyor and oil leak route identification support system

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US3107298A (en) * 1960-11-09 1963-10-15 James R Alburger Apparatus for the measurement of fluorescent tracer sensitivity
US3916205A (en) * 1973-05-31 1975-10-28 Block Engineering Differential counting of leukocytes and other cells
US4298005A (en) * 1976-03-05 1981-11-03 Mutzhas Maximilian F Radiation apparatus
US4990789A (en) * 1988-05-10 1991-02-05 Osamu Uesaki Ultra violet rays generator by means of microwave excitation
US5592245A (en) * 1994-08-10 1997-01-07 Moore; J. Paul Apparatus for enhancing visual perception of selected objects in recreational and sporting activities
US5543137A (en) * 1994-09-19 1996-08-06 Repper; George R. Method of protecting against sunburn

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Title
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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6177678B1 (en) 1995-04-05 2001-01-23 Brasscorp Ltd. Method and apparatus for leak detection and non-destructive testing
US6362488B1 (en) * 1997-11-05 2002-03-26 Corrosion Consultants, Inc. Light source and method for carrying out leak detection inspections
WO1999053299A1 (en) * 1998-04-13 1999-10-21 Brasscorp Ltd. Leak detector using fluorescent dyes
USRE43332E1 (en) 1999-04-23 2012-05-01 Atlantium Technologies Ltd. Method and device for disinfecting and purifying liquids and gasses
JP2002542919A (en) * 1999-04-23 2002-12-17 アトランティウム エルティディ． Liquid and gas sterilization and purification methods
EP1103805A2 (en) * 1999-11-29 2001-05-30 Marktec Corporation Ultraviolet light permeable filter for flaw detection apparatus and method for detection of flaws
EP1103805A3 (en) * 1999-11-29 2002-02-13 Marktec Corporation Ultraviolet light permeable filter for flaw detection apparatus and method for detection of flaws
EP1707611A2 (en) 2000-09-08 2006-10-04 Nanosolutions GmbH Synthesis of nanoparticles
US7241399B2 (en) 2000-09-08 2007-07-10 Centrum Fuer Angewandte Nanotechnologie (Can) Gmbh Synthesis of nanoparticles
EP1367413A1 (en) * 2002-05-27 2003-12-03 Canon Kabushiki Kaisha Reflector and linear illumination device
US7336403B2 (en) 2002-05-27 2008-02-26 Canon Kabushiki Kaisha Optical element and illumination apparatus having same
CN104903745A (en) * 2013-01-08 2015-09-09 斯基恩特-X公司 X-ray scintillator containing a multi-layered coating
EP2943808A4 (en) * 2013-01-08 2016-08-03 Scint X Ab X-ray scintillator containing a multi-layered coating

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Publication number Publication date
JP2001505122A (en) 2001-04-17
JP3434518B2 (en) 2003-08-11
AU5242998A (en) 1998-05-29
EP0983522A4 (en) 2000-03-08
EP0983522A1 (en) 2000-03-08

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