WO1996009773B1 - Flavor encapsulation - Google Patents
Flavor encapsulationInfo
- Publication number
- WO1996009773B1 WO1996009773B1 PCT/US1995/011967 US9511967W WO9609773B1 WO 1996009773 B1 WO1996009773 B1 WO 1996009773B1 US 9511967 W US9511967 W US 9511967W WO 9609773 B1 WO9609773 B1 WO 9609773B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- dense
- amorphous solid
- matrix
- melt
- coffee grinder
- Prior art date
Links
- 239000000796 flavoring agent Substances 0.000 title claims abstract 8
- 238000005538 encapsulation Methods 0.000 title 1
- 235000019634 flavors Nutrition 0.000 title 1
- 239000011159 matrix material Substances 0.000 claims abstract 14
- 239000000155 melt Substances 0.000 claims abstract 3
- 238000000034 method Methods 0.000 claims abstract 3
- 239000007787 solid Substances 0.000 claims 15
- 239000007789 gas Substances 0.000 claims 8
- 229920002774 Maltodextrin Polymers 0.000 claims 2
- GUBGYTABKSRVRQ-YOLKTULGSA-N Maltose Natural products O([C@@H]1[C@H](O)[C@@H](O)[C@H](O)O[C@H]1CO)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 GUBGYTABKSRVRQ-YOLKTULGSA-N 0.000 claims 2
- 229920000057 Mannan Polymers 0.000 claims 2
- LUEWUZLMQUOBSB-GFVSVBBRSA-N Mannan Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](O[C@H]3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-GFVSVBBRSA-N 0.000 claims 2
- 239000000416 hydrocolloid Substances 0.000 claims 2
- 239000004014 plasticizer Substances 0.000 claims 2
- 102000004169 proteins and genes Human genes 0.000 claims 2
- 108090000623 proteins and genes Proteins 0.000 claims 2
- 239000006188 syrup Substances 0.000 claims 2
- 235000020357 syrup Nutrition 0.000 claims 2
- OMDQUFIYNPYJFM-XKDAHURESA-N (2R,3R,4S,5R,6S)-2-(hydroxymethyl)-6-[[(2R,3S,4R,5S,6R)-4,5,6-trihydroxy-3-[(2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 claims 1
- 229920000926 Galactomannan Polymers 0.000 claims 1
- 239000005913 Maltodextrin Substances 0.000 claims 1
- 229920002472 Starch Polymers 0.000 claims 1
- 241000209149 Zea Species 0.000 claims 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 235000010980 cellulose Nutrition 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 235000005822 corn Nutrition 0.000 claims 1
- 235000005824 corn Nutrition 0.000 claims 1
- 150000002016 disaccharides Chemical class 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 235000019534 high fructose corn syrup Nutrition 0.000 claims 1
- 230000003301 hydrolyzing Effects 0.000 claims 1
- 229940035034 maltodextrin Drugs 0.000 claims 1
- 102000035365 modified proteins Human genes 0.000 claims 1
- 108091005569 modified proteins Proteins 0.000 claims 1
- 150000002772 monosaccharides Chemical class 0.000 claims 1
- 235000019698 starch Nutrition 0.000 claims 1
Abstract
A process for incorporating a volatile component into a matrix comprising: (a) forming a melt comprising said volatile component (12) and said matrix (10), (b) solidifying said melt under a pressure sufficient to prevent substantial volatilization of said volatile component (8). In a preferred embodiment, the volatile component is a volatile aroma compound such as those contained in coffee grinder gas or emitted when baking dough or roasting a food.
Claims
62
AMENDED CLAIMS
[received by the International Bureau on 28 March 1996 (28.03.96); original claims 1-27 cancelled; new claims 28-39 added; remaining claims unchanged (2 pages)]
28. A dense, amorphous solid, comprising a matrix and a volatile aroma compound encapsulated in said matrix, wherein said matrix has a Tg of at least 35°C and said volatile aroma compound is coffee grinder gas.
29. The dense, amorphous solid of Claim 28, prepared by a process comprising:
(a) forming a melt comprising said volatile aroma compound and a matrix material; and
(b) solidifying said melt under a pressure sufficient to prevent substantial volatilization of said volatile aroma compound, to directly obtain a dense, glassy matrix having a Tg of at least 35°C.
30. The process of Claim 29, wherein said melt is formed by:
(a) admixing a solid matrix material with a plasticizer and heating to form a melt;
(b) reducing the pressure on said melt so as to remove any gases present and to volatize at least a portion of said plasticizer and removing said portion from said melt; and
(c) admixing with the resulting melt said volatile aroma compound under pressure and temperature conditions sufficient to prevent substantial volatilization of said volatile aroma compound.
31. The dense, amorphous solid of Claim 29, wherein said coffee grinder gas is immiscible in said matrix.
32. The dense, amorphous solid of Claim 29, wherein said coffee grinder gas is soluble in the matrix.
33. The dense, amorphous solid of Claim 29, wherein said coffee grinder gas is natural coffee grinder gas.
63
34. The dense, amorphous solid of Claim 29, wherein said coffee grinder gas is synthetic coffee grinder gas.
35. The dense, amorphous solid of Claim 29, wherein said matrix material is selected from the group consisting of maltodextrins, corn syrup solids, maltose syrup solids, high fructose corn syrup solids, starches, hydrocolloids, gums, proteins, partially hydrolyzed proteins, modified proteins, modified hydrocolloids and modified celluloses.
36. The dense, amorphous solid of Claim 29, wherein said matrix material comprises a mannan oligomer.
37. The dense, amorphous solid of Claim 36, wherein said mannan oligomer is obtained by hydrolyzing spent coffee grounds.
38. The dense, amorphous solid of Claim 29, wherein said matrix material comprises a galacto-mannan.
39. The dense, amorphous solid of Claim 29, wherein said matrix material comprises a maltodextrin and a compound selected from the group consisting of monosaccharides and disaccharides.
AMENDEDSHEET(ARTICLE 1
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP95935021A EP0783251A4 (en) | 1994-09-29 | 1995-09-28 | Flavor encapsulation |
| AU37197/95A AU3719795A (en) | 1994-09-29 | 1995-09-28 | Flavor encapsulation |
| JP8511870A JPH10506784A (en) | 1994-09-29 | 1995-09-28 | Flavoring encapsulation |
| MXPA/A/1997/002317A MXPA97002317A (en) | 1994-09-29 | 1997-03-26 | Encapsulation of sa |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US31490994A | 1994-09-29 | 1994-09-29 | |
| US314,909 | 1994-09-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO1996009773A1 WO1996009773A1 (en) | 1996-04-04 |
| WO1996009773B1 true WO1996009773B1 (en) | 1996-05-09 |
Family
ID=23222021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US1995/011967 WO1996009773A1 (en) | 1994-09-29 | 1995-09-28 | Flavor encapsulation |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0783251A4 (en) |
| JP (1) | JPH10506784A (en) |
| AU (1) | AU3719795A (en) |
| CA (1) | CA2200849A1 (en) |
| WO (1) | WO1996009773A1 (en) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5750178A (en) * | 1996-06-18 | 1998-05-12 | Nestec S.A. | Method of making coffee particles containing aroma |
| EP1342548B1 (en) | 1996-10-28 | 2015-12-23 | General Mills, Inc. | Embedding and encapsulation of controlled release particles and encapsulated product |
| ATE277739T1 (en) * | 1996-10-28 | 2004-10-15 | Gen Mills Inc | EMBEDDING AND ENCAPSULATING PARTICLES FOR CONTROLLED DELIVERY |
| CA2322641C (en) | 1998-03-23 | 2010-02-16 | General Mills, Inc. | Encapsulation of components into edible products |
| EP1124443B1 (en) * | 1998-11-04 | 2005-02-09 | Firmenich Sa | Solid delivery systems for aroma ingredients |
| US6500463B1 (en) | 1999-10-01 | 2002-12-31 | General Mills, Inc. | Encapsulation of sensitive components into a matrix to obtain discrete shelf-stable particles |
| US6251478B1 (en) | 1999-12-22 | 2001-06-26 | Balchem Corporation | Sensitive substance encapsulation |
| US6436453B1 (en) | 2000-06-16 | 2002-08-20 | General Mills, Inc. | Production of oil encapsulated minerals and vitamins in a glassy matrix |
| US6468568B1 (en) | 2000-06-16 | 2002-10-22 | General Mills, Inc. | Oligosaccharide encapsulated mineral and vitamin ingredients |
| US6572905B2 (en) * | 2000-12-21 | 2003-06-03 | Kraft Foods Holdings, Inc. | Preparation aroma system for dehydrated food product compositions |
| US8334007B2 (en) * | 2003-03-19 | 2012-12-18 | Firmenich Sa | Continuous process for the incorporation of a flavor or fragrance ingredient or composition into a carbohydrate matrix |
| ES2399093T3 (en) * | 2004-05-24 | 2013-03-25 | Nestec S.A. | Arabinogalactan isolate from roasted green coffee for food and administration applications, and process for its production |
| EP1632135A1 (en) * | 2004-08-18 | 2006-03-08 | Nestec S.A. | Inert, glassy matrices for the stabilization of aroma in soluble coffee |
| US7803413B2 (en) | 2005-10-31 | 2010-09-28 | General Mills Ip Holdings Ii, Llc. | Encapsulation of readily oxidizable components |
| WO2008055006A1 (en) | 2006-10-31 | 2008-05-08 | Wm. Wrigley Jr. Company | Flavor releasing cores and their use in chewing gum |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3821447A (en) * | 1972-05-12 | 1974-06-28 | Gen Foods Corp | Method for producing stabilized coffee aromas |
| US4008340A (en) * | 1973-05-21 | 1977-02-15 | General Foods Corporation | Method for stabilizing coffee grinder gas aroma |
| US4232047A (en) * | 1978-05-30 | 1980-11-04 | Griffith Laboratories U.S.A., Inc. | Food supplement concentrate in a dense glasseous extrudate |
| US4689235A (en) * | 1984-01-31 | 1987-08-25 | Scm Corporation | Encapsulation matrix composition and encapsulate containing same |
| US4820534A (en) * | 1984-03-19 | 1989-04-11 | General Foods Corporation | Fixation of volatiles in extruded glass substrates |
| FI95987C (en) * | 1988-08-12 | 1996-04-25 | Gen Foods Corp | Method for making aerated, glassy coffee |
| US5087461A (en) * | 1989-10-02 | 1992-02-11 | Nabisco Brands, Inc. | Double-encapsulated compositions containing volatile and/or labile components, and processes for preparation and use thereof |
| US5009900A (en) * | 1989-10-02 | 1991-04-23 | Nabisco Brands, Inc. | Glassy matrices containing volatile and/or labile components, and processes for preparation and use thereof |
| EP0693884A4 (en) * | 1993-04-16 | 1996-03-27 | Mccormick & Co Inc | Encapsulation compositions |
| US5399368A (en) * | 1994-09-06 | 1995-03-21 | Nestec S.A. | Encapsulation of volatile aroma compounds |
-
1995
- 1995-09-28 AU AU37197/95A patent/AU3719795A/en not_active Abandoned
- 1995-09-28 EP EP95935021A patent/EP0783251A4/en not_active Withdrawn
- 1995-09-28 WO PCT/US1995/011967 patent/WO1996009773A1/en not_active Application Discontinuation
- 1995-09-28 JP JP8511870A patent/JPH10506784A/en active Pending
- 1995-09-28 CA CA002200849A patent/CA2200849A1/en not_active Abandoned
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