CN114766718B - Cigarette aroma-carrying particles, preparation method and application thereof - Google Patents
Cigarette aroma-carrying particles, preparation method and application thereof Download PDFInfo
- Publication number
- CN114766718B CN114766718B CN202210433876.XA CN202210433876A CN114766718B CN 114766718 B CN114766718 B CN 114766718B CN 202210433876 A CN202210433876 A CN 202210433876A CN 114766718 B CN114766718 B CN 114766718B
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- essence
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- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 3
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- DCVGCQPXTOSWEA-UHFFFAOYSA-N 4-[[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]pyrazol-3-yl]methyl]-1-methylpiperazin-2-one Chemical compound CN1CCN(CC2=NN(CC(=O)N3CCC4=C(C3)N=NN4)C=C2C2=CN=C(NC3CC4=C(C3)C=CC=C4)N=C2)CC1=O DCVGCQPXTOSWEA-UHFFFAOYSA-N 0.000 description 1
- DEXFNLNNUZKHNO-UHFFFAOYSA-N 6-[3-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperidin-1-yl]-3-oxopropyl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1CCN(CC1)C(CCC1=CC2=C(NC(O2)=O)C=C1)=O DEXFNLNNUZKHNO-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0229—Filter rod forming processes
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a cigarette aroma-carrying granule, a preparation method and application thereof, and relates to the technical field of cigarettes. The cigarette fragrance-carrying particles comprise a core material and a shell coated on the core material, wherein the core material is a granular fragrance-carrying material, and the shell is a waxy coating material; wherein the granular fragrance-carrying material is formed by carrying essence and perfume on granular adsorptive plant materials. The cigarette aroma-carrying particles provided by the embodiment of the invention have the advantages of aroma locking, aroma retention, aroma release stability and the like, the particles with wax film coatings can well lock aroma substances when the cigarettes are not burnt, and the wax coating is heated and melted when the cigarettes are burnt, so that essence and spice in the core material are released, and the configuration particles have wide application prospects in heating sections of traditional cigarettes and heated non-combustible cigarettes.
Description
Technical Field
The invention relates to the technical field of cigarettes, in particular to a cigarette fragrance-carrying granule, a preparation method and application thereof.
Background
The fragrance carrying performance of the cigarette material is one research direction of considerable attention in the industry, and common fragrance carrying technologies of the cigarette material comprise a plurality of modes of midline fragrance carrying, bead explosion fragrance carrying, forming agent fragrance carrying, tipping paper fragrance carrying, particle fragrance carrying and the like. The method is characterized in that the explosive bead-carried incense is the solution with the best incense-carrying and fragrance-retaining effects at present, and the essence is released only when the capsule is pinched and exploded in a smoking room of a consumer, but the development of the explosive bead cigarette is limited under the influence of industry policies and use cost, so that other types of cigarette-carried materials are paid more attention.
The particle fragrance carrying technology is widely studied at present, and in order to improve the fragrance retaining effect of particles, related researchers mainly improve the following aspects:
(1) Using an adsorptive plant material with stronger adsorptivity as a fragrance-carrying base material;
(2) Slowly releasing essence by microcapsule technology and thermosensitive phase change gel technology;
(3) Natural plant materials with a stable characteristic aroma are used directly.
The above methods improve the fragrance carrying performance of the tobacco particles to a certain extent, but the above methods are not easy to lock the essence and the perfume in the material preservation process, and the fragrance is lost to a certain extent. In addition, the existing fragrance-carrying material still has the problems of poor fragrance release stability, poor fragrance coordination and the like when being applied to cigarette burning and sucking.
In view of this, the present invention has been made.
Disclosure of Invention
The invention aims to provide a cigarette aroma-carrying granule, a preparation method and application thereof, and aims to improve aroma locking, aroma retaining and aroma releasing effects.
The invention is realized in the following way:
In a first aspect, the invention provides a fragrance-carrying granule for cigarettes, which has a double-layer structure, wherein the inner layer is a fragrance-carrying granular core material, the outer layer is a shell coated on the surface of the granular core material, and the shell is a waxy coating material;
wherein the granular fragrance-carrying material is formed by carrying essence and perfume on granular adsorptive plant materials.
In an alternative embodiment, the mass ratio of waxy coating material to core material is 0.5-25:100, preferably 3-7:100;
Preferably, the waxy coating material is selected from at least one of soy wax, rice bran wax, sugar cane wax, coconut wax, candelilla wax and palm wax.
In an alternative embodiment, the particulate adsorbent plant material is a granule formed from at least one adsorbent plant material by the action of a binder;
preferably, the binder is a vegetable gum; more preferably, the binder is selected from at least one of carrageenan, xanthan gum, gelatin, acacia and guar gum.
In an alternative embodiment, the adsorbent plant material is selected from at least one of porous corn starch, tapioca starch, rush meal, pomelo peel meal, and sorghum stalk core meal.
In an alternative embodiment, the flavoring agent is selected from at least one of tobacco flavoring, floral flavoring, peppermint flavoring, fruit flavoring, tea flavoring, medicinal flavoring, and bouquet flavoring.
In a second aspect, the present invention provides a method for preparing the aroma-carrying granule for cigarettes according to any one of the foregoing embodiments, mixing the particulate adsorptive plant material with the essence and the aroma to carry out aroma-carrying treatment to obtain a particulate aroma-carrying material, and coating the particulate aroma-carrying material with a waxy coating material.
In an alternative embodiment, the essence and the perfume are sprayed on the granular adsorptive plant material to carry out perfume carrying treatment to obtain granular perfume carrying material, and the wax coating material in a heating and melting state is sprayed on the granular perfume carrying material to carry out coating so as to form a wax film;
preferably, the method further comprises: sieving the particles with the wax film to obtain products with different particle size ranges;
more preferably, the products of the different particle size ranges include a first product having a particle size of 14-28 mesh and a second product having a particle size of 28-60 mesh.
In an alternative embodiment, the mass ratio of the perfuming amount to the particulate adsorbent plant material during the perfuming treatment of the particulate adsorbent plant material is from 1 to 20:100;
Preferably, the process for preparing the particulate adsorbent plant material comprises: uniformly mixing an adsorptive plant material, a binder and water, granulating to obtain a granular wet material, drying the granular wet material, and screening to obtain granules with the particle size of 14-60 meshes serving as an essence carrier;
Preferably, the raw materials for granulating comprise, in parts by weight: 50-80 parts of adsorptive plant material, 1-10 parts of adhesive and 20-60 parts of water;
preferably, the wet granular material is dried at a drying temperature of 50 to 80 ℃ and the moisture content after drying is controlled to 7 to 8wt%.
In an alternative embodiment, the coating process comprises: the waxy coating material is melted into coating liquid at 70-90 ℃, and the coating liquid is uniformly sprayed on the surface of the granular fragrance-carrying material in a coating machine through an atomization device, so that the coating liquid is solidified to form a wax film.
In a third aspect, the present invention provides a use of the flavour carrier particles for cigarettes according to any one of the preceding embodiments or the flavour carrier particles for cigarettes prepared by the method of preparation according to any one of the preceding embodiments in the preparation of cigarettes;
Preferably, the first product with the grain diameter of 14-28 meshes obtained by screening is used as a base material of a smoke generating material, and is applied to a heating section for heating a non-combustible cigarette after being carried with a cigarette smoke generating agent;
Preferably, the second product with the particle size of 28-60 meshes obtained by screening is manufactured into a binary composite filter rod by a filter rod forming machine, the particles are dispersed in the tows of the rod segments, and the filling amount of the second product in the tows of the rod segments is 0.5-1.5mg/mm.
The invention has the following beneficial effects: the granular aroma-carrying material is formed by carrying essence and spice on granular adsorptive plant materials, and the shell is formed by coating the granular aroma-carrying material serving as a core material and a waxy coating material. The cigarette aroma-carrying particles provided by the embodiment of the invention can well play a role in aroma locking in the storage process of cigarettes, and when a cigarette is burnt, the wax coating is heated and melted to release essence and spice in the core material, so that the cigarette aroma-carrying particles have the advantages of good aroma locking, aroma retaining and aroma releasing effects, and have wide application prospects in the heating sections of traditional cigarettes and heated non-combustible cigarettes.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings that are needed in the embodiments will be briefly described below, it being understood that the following drawings only illustrate some embodiments of the present invention and therefore should not be considered as limiting the scope, and other related drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a process flow diagram of a preparation method according to an embodiment of the present invention;
FIG. 2 is a schematic illustration of the application of waxy coated flavor-bearing particles in conventional cigarettes;
Figure 3 is a schematic illustration of the application of waxy coated flavor particles in a particulate heated non-combustible cigarette.
Icon: 001-acetate tow segments; 002-composite strand segments; 003-tipping paper; 004-cigarette paper; 005-tobacco shred section; 006-binary composite filter rod portion; 007-cut tobacco segment portion of a cigarette; a heating section; b-a heat insulation section; c-a filter tow segment; d-waxy coated particles; e-paper tube wall; f-tows.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention more clear, the technical solutions of the embodiments of the present invention will be clearly and completely described below. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
Referring to fig. 1, an embodiment of the present invention provides a method for preparing a cigarette fragrance-carrying granule, which includes the following steps:
s1, preparation of granular adsorptive plant material
The particulate adsorbent plant material is a granule formed from at least one adsorbent plant material by the action of a binder, the granule being of a shape not limited, and generally being approximately spherical.
In practice, the process for preparing the particulate adsorbent plant material comprises: the adsorptive plant material, the adhesive and the water are uniformly mixed and then granulated to obtain a granular wet material, and the granular wet material is dried and then screened (primary screening) to obtain the granules with the particle size of 14-60 meshes for subsequent fragrance carrying treatment. The granular absorbent plant material is prepared by adopting a general wet granulation method, and is granulated by adopting a general swing granulator, and the granules meeting the particle size requirement are obtained by sieving after the granulation is completed.
The type of the adsorptive plant material is not limited, and may be a plant material generally used for having an effect of adsorbing essence. In some embodiments, the adsorbent plant material is selected from at least one of porous corn starch, tapioca starch, rush powder, pomelo peel powder, and sorghum stalk core powder, which may be one or more.
The binder is not limited in kind, and may be a general food-grade wet granulation binder, such as vegetable gum. In some embodiments, the binder is selected from at least one of carrageenan, xanthan gum, gelatin, acacia gum and guar gum, and may be one or more.
In some embodiments, the raw materials used for granulation comprise, in parts by weight: 50-80 parts of adsorptive plant material, 1-10 parts of adhesive and 20-60 parts of water, and the uniformity of the prepared granules is higher by controlling the dosage of each component in the granulating raw material.
In some embodiments, the wet particulate material is dried at a drying temperature of 50-80 ℃ and the moisture content after drying is controlled to 7-8wt%. The drying temperature is not too high or too low, which would affect the properties of the material itself, and too low a temperature would result in too long a drying time.
S2, preparing granular fragrance-carrying material
The granular adsorptive plant material and the essence and perfume are mixed for carrying perfume treatment to obtain the granular perfume carrying material, and the granular perfume carrying material is used as a core material in the embodiment of the invention.
The fragrance carrying mode is not limited, and can be selected according to the types of the essence and the perfume. In some embodiments, the aroma and flavor are sprayed onto the particulate adsorbent plant material to perform a flavor-carrying treatment to provide a particulate flavor-carrying material. In the actual operation process, the granular adsorptive plant material is stirred in a stirring kettle, and essence and perfume are uniformly sprayed on the surfaces of the particles by utilizing a sprayer while stirring.
The types of the essence and the spice are not limited, and the common essence and spice for cigarettes can be selected. In some embodiments, the flavoring agent is at least one selected from tobacco essence, flower essence, peppermint essence, fruit essence, tea essence, medicinal essence and wine essence, and can be one or a mixture of several.
In some embodiments, the mass ratio of the flavoring amount to the particulate adsorbent plant material during the aroma-loading treatment is 1-20:100, e.g., the mass ratio of the aroma-loading amount to the particulate adsorbent plant material may be 1:100, 5:100, 10:100, 15:100, 20:100, etc., or any value between the above adjacent ratio values.
S3, coating
The wax coating material is used for coating the granular fragrance-carrying material, and the wax coating material is used as a shell, so that the wax coating material has a good barrier effect on the essence and the spice in the core material in the storage process, and can lock the essence and the spice in the core material at normal temperature; and when the cigarettes are sucked, the wax coating is heated and melted, and essence and spice in the core material are released.
The coating mode is not limited, and the wax coating material can be used for forming a coating on the core material in a spraying mode. In the actual operation process, the wax coating material in a heating and melting state is sprayed on the granular fragrance-carrying material for coating, and the hot wax coating liquid is quickly solidified into wax coating after contacting the surface of the granule.
Specifically, the coating process may include: the waxy coating material is melted into coating liquid at 70-90 ℃, the coating liquid is uniformly sprayed on the surface of the granular fragrance-carrying material in a coating machine through an atomization device, and cold air drying can be used in the coating process, so that the coating liquid is quickly solidified to form a wax film.
In some embodiments, the waxy coating material is selected from one or more of the waxy materials soy wax (melting point 52 ℃), rice bran wax (melting point 60-85 ℃), sugar cane wax (melting point 70-84 ℃), coconut wax (melting point 40-45 ℃), candelilla wax (melting point 68-73 ℃), palm wax (melting point 81-86 ℃), and the like, and may be one or more.
The wax coating material adopted in the embodiment of the invention adopts vegetable wax, has the characteristics of natural smell, coordination with tobacco fragrance, low melting temperature and the like, is an excellent phase change coating material for cigarettes, and widens the melting point range of a wax film by compounding vegetable wax with different melting points, so that essence is released more stably during smoking of cigarettes.
In some embodiments, the mass ratio of waxy coating material to core material is 0.5-25:100, preferably 3-7:100. The dosage of the waxy coating material is too small to achieve a coating effect and not well lock the fragrance of the inner core material; too large an amount of waxy coating material can result in too thick coating shells, low melting efficiency, incomplete release of essence, and the like.
S3, screening
And (3) sieving (secondary sieving) the particles with the wax film to obtain products with different particle size ranges, wherein the sieving can adopt a vibrating sleeve sieve to remove fine powder generated in the processing process and large particles formed by adhesion solidification.
Products with different particle size ranges can be obtained in the sieving process, and the products with different particle size ranges comprise a first product with the particle size of 14-28 meshes and a second product with the particle size of 28-60 meshes for the convenience of subsequent utilization. The first product is used as a base material of a smoke generating material, is loaded with a cigarette smoke generating agent and is applied to a heating section for heating a non-burning cigarette; the second product is suitable for use in a tow composite filter rod.
The embodiment of the invention also provides the fragrance-carrying particles for cigarettes, which have a double-layer structure, wherein the inner layer is a fragrance-carrying granular core material, the outer layer is a shell coated on the surface of the granular core material, and the shell is a waxy coating material; wherein the granular fragrance-carrying material is formed by carrying essence and perfume on granular adsorptive plant materials.
The cigarette fragrance-carrying particles provided by the embodiment of the invention can be prepared by the preparation method, and have the advantages of good fragrance locking, fragrance retaining and fragrance releasing effects.
The embodiment of the invention also provides application of the cigarette aroma-carrying particles in preparing cigarettes, and a proper application mode is selected according to the size of the particles:
Referring to fig. 2, the second product with the particle size of 28-60 meshes obtained by screening is filled in the acetate tow segment to obtain a composite tow segment 002, the composite tow segment 002 and another acetate tow segment 001 are binary-composited by a filter rod forming machine to obtain a composite cigarette filter rod (namely binary composite filter rod part 006 in the figure), the particles are dispersed in the tow of the material rod segment, and the filling amount of the second product in the acetate tow segment is 0.5-1.5mg/mm. In addition, the conventional cigarette further comprises a tobacco section 005 and cigarette paper 004 wrapping the tobacco section 005, so as to form a tobacco section portion 007 of the cigarette, and the binary composite filter rod portion 006 and the tobacco section portion 007 of the cigarette are assembled by the tipping paper 003 to form a complete conventional type cigarette.
Referring to fig. 3, a first product with a particle size of 14-28 mesh obtained by sieving is applied to a heating section for heating a non-combustible cigarette, a paper tube wall E is an outer wall of the heated non-combustible cigarette, the interior of the paper tube wall E is filled with wax coated particles D prepared by the embodiment of the invention to form a heating section a, a wrapped tow F forms a filter tow section C, and a heat insulation section B is arranged between the heating section a and the filter tow section C.
The features and capabilities of the present invention are described in further detail below in connection with the examples.
Example 1
The embodiment provides a preparation method of cigarettes, which comprises a waxy-coated aroma-carrying particle binary filter stick structure, and comprises the following steps:
(1) Preparation of fragrance-carrying particles for cigarettes
And (3) batching: 60 parts of porous corn starch, 37 parts of shaddock ped powder, 3 parts of xanthan gum and 45 parts of purified water are weighed according to parts by weight.
Granulating: the prepared materials are stirred uniformly in a stirrer, and a swinging granulator and an extrusion screen are used for selecting 24 meshes, so that wet granular materials are obtained.
And (3) drying: the wet material was dried with a forced air drying oven to a moisture content of 7-8% and the temperature was set at 80 ℃.
Fragrance carrying: uniformly spraying essence onto the surface of the particles by using a sprayer while stirring in a stirring kettle, wherein the spraying amount is 5% of the total mass of the particles, the essence is formed by combining 50% of mint essence and 50% of sweet orange essence, and the intermediate product of the fragrance-carrying particles is sealed and preserved for later use.
Coating: coconut wax is used as a coating raw material, water bath at 80 ℃ is used for heating to a molten liquid state and stirring is carried out uniformly, the coconut wax is used as a coating liquid, the intermediate product of the aroma-carrying particles is coated in a coating machine, and the mass ratio of the coating liquid to the aroma-carrying particles is 5:100. And in the coating process, cold air is used for drying, and the hot waxy coating liquid is quickly solidified into a waxy coating after contacting the surface of the particle.
Secondary screening: and (3) screening the coated granular intermediate for the second time, and taking the 28-60 mesh screen intermediate as a final waxy coating aroma-carrying granular product.
(2) And (3) forming a particle filter stick: using a filter rod former, a pellet rod was made at an add-on level of 1.5mg per mm, and the rod was combined with a white rod to a binary filter rod according to a 15+15 gauge.
(3) And (3) cigarette forming: and (3) using a cigarette machine of a cigarette enterprise to manufacture the binary filter stick obtained in the step (2) into the aroma-carrying cigarette (as shown in figure 2).
Example 2
The present embodiment provides a method for preparing cigarettes, which differs from embodiment 1 only in that: the coating raw material coconut wax is replaced by palm wax.
Example 3
The present embodiment provides a method for preparing cigarettes, which differs from embodiment 1 only in that: the coating raw material coconut wax was replaced with coconut wax and soybean wax in a 1:1 ratio by weight, and the total coating raw material was the same as in example 1.
Example 4
The present embodiment provides a method for preparing a cigarette, which differs from embodiment 3 only in that: the mass ratio of the dosage of the coating liquid to the perfume-carrying particles is 10:100.
Example 5
The present embodiment provides a method for preparing a cigarette, which differs from embodiment 3 only in that: the mass ratio of the dosage of the coating liquid to the perfume-carrying particles is 7:100.
Example 6
The present embodiment provides a method for preparing a cigarette, which differs from embodiment 3 only in that: the mass ratio of the dosage of the coating liquid to the perfume-carrying particles is 3:100.
Example 7
The present embodiment provides a method for preparing cigarettes, which differs from embodiment 1 only in that: the coating raw materials of coconut wax, soybean wax and sugarcane wax are replaced by coconut wax, soybean wax and sugarcane wax, the mass ratio of the coconut wax, the soybean wax and the sugarcane wax is 2:1:1, and the total dosage of the coating raw materials is the same as that of the example 1.
Example 8
The present embodiment provides a method for preparing cigarettes, which differs from embodiment 1 only in that: the coating raw materials of coconut wax, soybean wax, sugarcane wax and palm wax were replaced with the coconut wax, soybean wax, sugarcane wax and palm wax in a mass ratio of 12:5:2:1, and the total coating raw materials were used in the same amount as in example 1.
Example 9
The embodiment provides a preparation method of a heating non-combustible cigarette, wherein a heating section contains wax-coated aroma-carrying particles, and the preparation process comprises the following steps:
(1) Preparation of fragrance-carrying particles for cigarettes
And (3) batching: weighing 20 parts of porous corn starch, 10 parts of tapioca starch, 20 parts of shaddock ped powder, 50 parts of rush powder, 3 parts of xanthan gum and 50 parts of purified water according to parts by mass.
Granulating: mixing the above materials, stirring, and selecting 15 mesh with a swing granulator to obtain wet granule materials.
And (3) drying: the wet material was dried with a forced air drying oven to a moisture content of 7-8% and the temperature was set at 80 ℃.
Fragrance carrying: uniformly spraying essence on the surfaces of the particles by using a sprayer while stirring the particles in a stirring kettle, wherein the spraying amount is 5% of the total mass of the particles (the mass ratio of the spraying amount to the total mass of the particles is 5:100), the essence is formed by combining 100% of mint essence, and the intermediate product of the fragrance-carrying particles is sealed and preserved for later use.
Coating: coconut wax is used as a coating raw material, water bath at 100 ℃ is used for heating to a molten liquid state and stirring is carried out uniformly, and as a coating liquid, the intermediate product of the aroma-carrying particles is coated in a coating machine, wherein the dosage of the coating liquid is 5% (the mass ratio of the dosage of the coating liquid to the aroma-carrying particles is 5:100). And in the coating process, cold air is used for drying, and the hot waxy coating liquid is quickly solidified into a waxy coating after contacting the surface of the particle.
Secondary screening: and (3) carrying out secondary screening on the particles with wax coating, and taking the 14-28 mesh sieve intermediate as a final wax coating fragrance-carrying particle product.
(2) Heating non-combustible cigarette applications: the wax-coated aroma-loaded particles obtained by the secondary screening are manually filled into the heating section of the particle type heating non-combustible cigarette (see figure 3).
Example 10
This example provides a method for preparing a heated non-combustible cigarette, which differs from example 9 only in that: the coconut wax as the coating material is replaced by rice bran wax.
Example 11
This example provides a method for preparing a heated non-combustible cigarette, which differs from example 9 only in that: the coating raw material coconut wax is replaced by palm wax.
Example 12
This example provides a method for preparing a heated non-combustible cigarette, which differs from example 9 only in that: the coconut wax serving as a coating raw material is replaced by coconut wax, soybean wax, sugarcane wax and palm wax, wherein the mass ratio of the coconut wax to the soybean wax to the sugarcane wax to the palm wax is 12:5:2:1, and the dosage of the coating liquid is 5%.
Example 13
This example provides a method for preparing a heated non-combustible cigarette, which differs from example 9 only in that: the coconut wax serving as a coating raw material is replaced by coconut wax, soybean wax, sugarcane wax and palm wax, wherein the mass ratio of the coconut wax to the soybean wax to the sugarcane wax to the palm wax is 1:1:1, and the dosage of the coating liquid is 5%.
Comparative example 1
The only difference from example 1 is that: no coating was performed.
Comparative example 2
The only difference from example 9 is that: no coating was performed.
Test example 1
The tobacco samples obtained in examples 1 to 8 and comparative example 1 were subjected to sensory evaluation after 15 days of storage in a sealed bag, evaluation method: sensory evaluation is carried out by an evaluation group of 5 members, wherein evaluation indexes comprise five indexes of characteristic fragrance (sweet orange fragrance and peppermint fragrance) intensity, characteristic fragrance release stability, coordination, miscellaneous gases and irritation of the granular essence, each index is fully divided into 10 points, and the average score is obtained as a final score. The evaluation results are shown in the following table:
Table 1 cigarette sample evaluation results (fruit flavor style)
The results show that: the wax film is used for helping the retention of essence and spice, so that the characteristic fragrance intensity during burning and sucking is greatly improved; the use of multiple wax film components can improve the stability of characteristic fragrance release and fragrance coordination; the use of a high proportion of a low melting waxy component is advantageous for the release of flavour and fragrance, because the temperature in the filter stick is relatively low (average temperature between 40 and 50 ℃) during smoking of a conventional cigarette; the wax film coating is not easy to be too thin or too thick, the comprehensive quality of the 5% of the using amount ratio of the sensory evaluation wax liquid is better than 10%, 3% and 7%, the too thin wax film can not effectively seal the fragrant substances, and the too thick wax film influences the stable release of the fragrant substances and can introduce a small amount of miscellaneous gas; as can be seen by comparison, the waxy coating formulation of example 8 is the preferred coating formulation.
Test example 2
The tobacco samples obtained in examples 9 to 13 and comparative example 2 were subjected to sensory evaluation using a dedicated smoking set after being sealed with a sealed bag for 15 days, and the evaluation method was as follows:
Sensory evaluation is carried out by an evaluation group of 5 members, wherein evaluation indexes comprise five indexes of characteristic fragrance (peppermint taste and cool degree) intensity, characteristic fragrance release stability, coordination, miscellaneous qi and stimulation of the granular essence, each index is fully divided into 10 points, and the average score is obtained as a final score. The evaluation results are shown in the following table:
TABLE 2 sensory evaluation results of heating non-combustible cigarette samples (peppermint flavor)
| Evaluation index | Characteristic fragrance intensity | Characteristic fragrance release stability | Coordination of | Miscellaneous gas | Irritation (irritation) |
| Comparative example 2 | 5 | 5 | 8 | 8 | 8 |
| Example 9 | 7 | 6 | 7 | 7 | 7 |
| Example 10 | 8 | 7 | 7 | 7 | 7 |
| Example 11 | 7 | 6 | 7 | 7 | 6 |
| Example 12 | 8 | 8 | 7 | 8 | 7 |
| Example 13 | 9 | 8 | 8 | 8 | 7 |
The results show that: the characteristic aroma and sweetness of the particles coated by the wax film are improved; the samples obtained in examples 12 and 13 using various wax film components exhibited improved stability of characteristic fragrance release; the sample of example 13 has slightly higher characteristic fragrance intensity than the sample of example 12 because the wax film formed by using the high melting point wax component in a large proportion has better sealing property, and the heating section temperature is higher when the non-burning cigarette is heated for smoking, so that the complete release of the essence and the perfume is facilitated (the heating section temperature is between room temperature and 300 ℃). The mint essence has larger irritation to the nasal cavity, and the coordination and irritation index are slightly reduced after the wax film is used, but the sample prepared by the embodiment of the invention is not influenced, and the advantage of improving the fragrance carrying performance is reflected.
In summary, the embodiment of the invention provides a perfume carrier particle for cigarettes, a preparation method and application thereof, which uses a granular perfume carrier material as a core material and a wax coating material for coating to form a shell, and has the following advantages:
(1) The wax coating has good essence blocking effect, can lock the essence and the spice of the inner core at normal temperature, and can be heated and melted to release the essence and the spice in the core material when the cigarette is sucked.
(2) The core material and the coating material selected by the invention are natural plant materials, so that the invention is safe and reliable, and does not generate negative smell to cigarette smoke.
(3) The coating technology has good extension application prospect, is not only suitable for irregular particles produced by a swing granulator, but also can be used for regular particles produced by an extrusion spheronizer, and can be applied to microcapsule products.
(4) The invention has simple process, easy realization, good effects of locking, retaining and releasing the fragrance, and wide application prospect in the heating sections of the traditional cigarettes and the heated non-combustible cigarettes.
The above is only a preferred embodiment of the present invention, and is not intended to limit the present invention, but various modifications and variations can be made to the present invention by those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (13)
1. The cigarette fragrance-carrying granule is characterized by having a double-layer structure, wherein the inner layer is a fragrance-carrying granular core material, the outer layer is a shell coated on the surface of the granular core material, and the shell is a waxy coating material;
Wherein, the granular fragrance-carrying material is formed by carrying essence and spice on granular adsorptive plant materials; the adsorptive plant material is at least one of porous corn starch, tapioca starch, rush powder, shaddock peel powder and sorghum stalk core powder; the essence and spice is at least one selected from tobacco essence, flower essence, peppermint essence, fruit essence, tea essence, medicinal essence and wine essence;
The mass ratio of the waxy coating material to the core material is 3-7:100, the waxy coating material comprises coconut wax, soybean wax, sugarcane wax and palm wax, and the mass ratio of the coconut wax to the soybean wax to the sugarcane wax to the palm wax is 12:5:2:1;
The preparation method of the cigarette fragrance-carrying particles comprises the following steps: spraying the essence and perfume on the granular adsorptive plant material to carry out perfume carrying treatment to obtain the granular perfume carrying material, and spraying the wax coating material in a heating and melting state on the granular perfume carrying material to carry out coating so as to form a wax film;
The preparation process of the granular adsorptive plant material comprises the following steps: uniformly mixing an adsorptive plant material, an adhesive and water, granulating to obtain a granular wet material, drying the granular wet material, and screening to obtain granules with the particle size of 14-60 meshes for fragrance carrying treatment; the raw materials for granulating comprise the following components in parts by mass: 50-80 parts of adsorptive plant material, 1-10 parts of adhesive and 20-60 parts of water.
2. A smoke-carrying particulate according to claim 1, wherein the particulate adsorbent plant material is a particulate formed from at least one adsorbent plant material by the action of a binder.
3. The smoke-carrying particulate of claim 2 wherein the binder is a vegetable gum.
4. A flavour carrier particle for cigarettes according to claim 3, wherein the binder is selected from at least one of carrageenan, xanthan gum, gelatin, acacia and guar gum.
5. A method of preparing the flavour carrier granules for cigarettes according to any one of claims 1 to 4, wherein the flavour and fragrance are sprayed on the particulate adsorptive plant material to carry out flavour carrying treatment to obtain the particulate flavour carrying material, and the waxy coating material in a heated and melted state is sprayed on the particulate flavour carrying material to carry out coating to form a wax film;
The preparation process of the granular adsorptive plant material comprises the following steps: uniformly mixing an adsorptive plant material, an adhesive and water, granulating to obtain a granular wet material, drying the granular wet material, and screening to obtain granules with the particle size of 14-60 meshes for fragrance carrying treatment;
The raw materials for granulating comprise the following components in parts by mass: 50-80 parts of adsorptive plant material, 1-10 parts of adhesive and 20-60 parts of water.
6. The method of manufacturing according to claim 5, further comprising: and sieving the particles with the wax film to obtain products with different particle size ranges.
7. The method of claim 6, wherein the different particle size ranges of the product comprise a first product having a particle size of 14-28 mesh and a second product having a particle size of 28-60 mesh.
8. The method of claim 6, wherein the mass ratio of the perfuming amount to the particulate adsorptive plant material is 1-20:100 during the perfuming treatment of the particulate adsorptive plant material.
9. The method according to claim 8, wherein the wet granular material is dried at a drying temperature of 50 to 80 ℃ and the moisture content after drying is controlled to 7 to 8 wt%.
10. The method of claim 5, wherein the coating process comprises: and (3) melting the waxy coating material into coating liquid at 70-90 ℃, uniformly spraying the coating liquid on the surface of the granular fragrance-carrying material in a coating machine through an atomization device, and solidifying the coating liquid to form a wax film.
11. Use of the flavour carrier granules for cigarettes according to any one of claims 1 to 4 or prepared by the preparation method according to any one of claims 5 to 10 in the preparation of cigarettes.
12. The use according to claim 11, wherein the first product having a particle size of 14-28 mesh obtained by sieving is used as a base material for a smoking material, and the first product is applied to a heating section for heating a non-combustible cigarette after the smoking material for cigarettes is carried.
13. The use according to claim 11, characterized in that the second product with a particle size of 28-60 mesh obtained by screening is made into a binary composite filter rod by means of a rod former, the particles are dispersed in the strand of the rod segment, and the filling amount of the second product in the strand segment is 0.5-1.5mg/mm.
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| CN115226932A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Heated cigarette with uniformly blended aroma-carrying particles and heated cigarette tobacco shreds and preparation method thereof |
| CN115886314A (en) * | 2023-01-17 | 2023-04-04 | 云南养瑞科技集团有限公司 | Preparation method of waxy phase-change slow-release aroma-carrying particles, particles obtained by method and application of particles |
| CN116268563A (en) * | 2023-04-04 | 2023-06-23 | 云南中宝龙天然香料有限公司 | Functional plant particles for enhancing aroma of filter stick as well as preparation method and application thereof |
| CN116391900A (en) * | 2023-04-10 | 2023-07-07 | 云南中烟工业有限责任公司 | Heating cigarette core material and preparation method thereof |
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