US3757428A

US3757428A - Method and apparatus for drying lumber

Info

Publication number: US3757428A
Application number: US00267132A
Authority: US
Inventors: D Runciman
Original assignee: Individual
Current assignee: Individual
Priority date: 1972-06-28
Filing date: 1972-06-28
Publication date: 1973-09-11
Anticipated expiration: 1990-09-11
Also published as: ZA733797B; JPS4941505A; AU467735B2; BR7304736D0; CA992740A; AU5546473A

Abstract

A method and apparatus for drying stacked lumber by solvent extraction, said apparatus including an elongate chamber through which stacked batches of lumber to be dried are moved. The elongate chamber includes a first compartment in which a stacked batch of lumber is steamed. A second longitudinally adjacent compartment wherein a liquid mixture of a solvent and water near its boiling point wets the stacked lumber in the presence of a vapor mixture of steam and solvent such that the solvent in the liquid phase replaces water within the lumber. As the stacked lumber is moved through this second compartment both the liquid and vapor phases in contact with the lumber have progressively greater solvent contents. The wetting liquid flows progressively through a series of weirs counter the direction of lumber movement, while the vapor moves between the stacked lumber in the direction opposite liquid flow and in this manner, the solvent drying the lumber is itself distilled within the chamber. A condenser adjacent the exit end of the second compartment withdraws vapor having a high solvent content from the compartment and returns solvent condensed therefrom to the dry wood end of the compartment where it is again used to wet the lumber. A third compartment is provided longitudinally adjacent the second compartment wherein the stacked lumber is subjected to steam or a steam and air combination to remove a desired percentage of solvent in the wood to produde substantially dry lumber. A method of drying lumber by solvent extraction including the steps of steam conditioning wood for drying; wetting the lumber to be dried with a substantially closed chamber with a watersolvent liquid mixture maintained at or near its boiling point; increasing the solvent content of the liquid mixture such that solvent replaces substantially all of the moisture in said lumber; simultaneously distilling the solvent within the substantially close chamber; and raising the temperature of the lumber to drive off the solvent therein to produce substantially dry lumber.

Description

United States Patent 191 Runciman 1451 Sept. 11, 1973 METHOD AND APPARATUS FOR DRYING LUMBER [76] Inventor: Donald A. Runciman, l522l-15th St., Seattle, Wash. 98148 {22] Filed: June 28, 1972 [21] Appl. No.: 267,132

[52] US. Cl 34/9.5, 34/13.8, 34/13.4,

34/48, 34/D1G. 19, 432/66 [51] Int. Cl. F26b 3/04 [58] Field of Search 34/9.5, 13.8, 13.4,

34/14,16.5,15, 77, 78,100,196, DIG. 19, 48, 201, 212, 216, 217; 832/1, 2, 6, 9,14, 23,

Canada 314/138 Primary Examiner-John J. Camby Assistant ExaminerHenry Cv Yuen A Attorney John O. Graybeal, James R. Uhlir et a].

[57] ABSTRACT A method andapparatus for drying stacked lumber by solvent extraction, said apparatus including an elongate chamber through which stacked batches of lumber to be dried are moved. The elongate chamber includes a first compartment in which a stacked batch of lumber is steamed. A second longitudinally adjacent compartment wherein a liquid mixture of a solvent and water near its boiling point wets the stacked lumber in the presence of a vapor mixture of steam and solvent such that the solvent in the liquid phase replaces water within the lumber. As the stacked lumber is moved through this second compartment both the liquid and vapor phases in contact with the lumber have progressively greater solvent contents. The wetting liquid flows progressively through a series of weirs' counter the direction of lumber movement, while the vapor moves between the stacked lumber in the direction opposite liquid flow and in this manner, the solvent drying the lumber is itself distilled within the chamber. A condenser adjacent the exit end of the second compartfnent withdraws vapor having a high solvent content from the compartment and returns solvent condensed therefrom to the dry wood end of the compartment where it is again used to wet the lumber. A third compartment is provided longitudinally adjacentthe second compartment wherein the stacked lumber is subjected to steam or a steam and air combination to remove a desired percentage of solvent in the wood to produde substantially dry lumber.

A method of drying lumber by solvent extraction including the steps of steam conditioning wood for drying; wetting the lumber to be dried with a substantially closed chamber with a water-solvent liquid mixture maintained at or near its boiling point; increasing the solvent content of the liquid mixture such that solvent replaces substantially all of the moisture in said lumber; simultaneously distilling the solvent within the substantially close chamber; and raising the temperature of the lumber to drive off the solvent therein to produce substantially dry lumber.

23 Claims, 6 Drawing Figures PAYENTED I 3 SHEET 2 or 2 METHOD AND APPARATUS FOR DRYING LUMBER BACKGROUND OF THE INVENTION 1. Field of the Invention This invention relates, in general, to a method and apparatus for drying lumber, and in particular, to a method and apparatus for drying lumber rapidly by solvent extraction without a separate solvent distillation unit.

2. Description of the Prior Art In general, it is known that lumber may be dried by heating it in an immiscible solvent maintained at a temperature above the boiling point of water until all the water within the lumber boils off. It is also known that when wet wood is placed in continuous contact with a solvent which is miscible with water, the solvent will re move the water from the wood even if the solvent is used cold or at any other temperature below the boiling point of water. Alcohol is a common example of such a solvent and this principle has long been used in the seasoning and treating of green wood.

While the use of solvent to extract moisture from lumber is known per se, most prior processes have submerged the wood to be dried in a series of tanks containing solvent. The solvent is circulated through the tanks until the moisture content of the wood has been reduced to a desired level and the wood is then removed from the tanks and the solvent stripped therefrom by conventional means. The solvent-water liquid mixture remaining in the tanks is passed through a conventional distillation column where water is separated from the solvent and the dry solvent returned to the tanks. The construction cost of a conventional distillation column is substantial, and this factor has generally prevented commercial acceptance of these processes.

One known method of drying lumber developed by the Western Pine Association comprises the steps of standing lumber on end in a closed drying chamber and continuously wetting the lumber with hot acetone until the desired water removal is accomplished. The acetone, containing both water and the pitch from the wood, is continuously drained from theextractor and recirculated through a storage tank and heater back to the spray head. When the water contant of the mixture becomes too great, some of the mixture is drawn off from the storage tank and distilled to separate the water and the extractives and to recover pure acetone.

After the spray is shut off, heated air is passed over the lumber to complete drying and removethe acetone. Finally, an inert gas is introduced into the extractor to reduce the fire hazard and increase acetone recovery. Again the need for a separate distillation column has limited commercial acceptance of this process.

U.S. Pat. No. 2,860,070 discloses a wood drying process employing the commercial dry cleaning solvent perchloroethylene. The wood is placed horizontally in a closed chamber and submerged in the solvent which is then heated until an azeotropic mixture of water and the solvent boil off. Vapors are collected in a condenser, separated, and the solvent returned to the closed chamber. Since the solvent is not miscible in water, the drying phenomenon is similar to known boilingin-oil processes, such as that disclosed in U.S. Pat. No. 3,205,589 for example.

One problem to which the instant invention has par-' ticular application is that of drying redwood timber.

Most redwood lumber must be dried to a moisture contant of between 8 percent and 10 percent prior to its final utilization, and since redwood is a slow drying species, requiring the longest drying time of any commercial soft wood species, this represents a major problem in the industry. A good discussion of some of the problems involved in the drying of redwood is found in U.S. Pat. No. 3,309,778 which discloses a method of drying redwood including freezing the wood prior to drying.

A method of solvent drying redwood using methanol has been described in an article titled Solvent Drying of California Redwood, published at pp 297 et seq. of the July, 1965 issue of Forest Products Journal. In the described process, lumber to be dried was inserted in a closed extractor and methanol was distributed over each board. Periodically a portion of solvent mixture in the extractor was removed and distilled and fresh solvent added. When a desired moisture content of the lumber was reached, the solvent was drained from the extractor and the solvent removed from the lumber by air circulation and steaming. Again, this process requires relatively expensive separate distillation equipment to purify the methanol, while disclosing a vapor sealed chamber which is costly to construct and cannot be loaded or unloaded with lumber without shutting down the drying process or risking a serious explosion.

BRIEF SUMMARY OF THE INVENTION 7 The instant invention relates to a method of drying lumber by solvent extraction, including passing the lumber through a drying chamber wherein a liquid mixture of solvent and water containing progressively lesser amounts of water and greater amounts of solvent is sprayed over the lumber as it passes there-through such that the solvent replaces water within the lumber. The liquid mixture flows from the dry wood exit end of the chamber toward the wet wood entrance end. Simultaneously, steam enters the drying chamber at its wet wood entrance end and moves through the chamber causing solvent in the liquid mixtureto vaporize. At the dry wood exit end of the chamber, the vapor phase, which has a high solvent content, is condensed and the condensate employed to again wet the stacked lumber.

compartment wherein the lumber to be dried is steamed, a longitudinally spaced second compartment wherein the lumber is wet by a liquid mixture of solvent and water in the presence of steam such that the solvent replaces the water in the lumber, and a longitudinally spaced third chamber wherein the solvent which has replaced the water in the lumber is removed by heating. Each of the compartments include end positioned sealable doors so that lumber may be moved through the elongate chamber while maintaining relatively constant conditions within the second wood drying'compartment while further minimizing the entrance of air into the wood drying compartment or the escape of vapor from the wood drying compartment to the air to reduce the hazard of explosion. The second compartment includes a pluraity of solvent distribution means spaced along its top portion to distribute solvent over the lumber to be dried. Basins are arranged below each solvent distributor to catch liquid runoff from the lumber, and these basins are arranged so that liquid flows from basin to basin from the dry wood exit end of the second compartment toward the entrance end of the elongate chamber and thence to a reboiler. The solvent-water mixture employed to wet the lumber is continually maintained at its boiling point and sumps are associated with each basin so that the solvent-water mixture is recirculated to the overhead sitributor.

It is an object of the present invention, therefore, to provide a method andapparatus for drying lumber by solvent extraction which does not require the construction of a separate distillation column to purify the solvent.

Another object of the present invention is to provide a method and apparatus for solvent drying lumber wherein the solvent is continually distilled within the drying chamber itself.

Still another object of the present invention is to provide a method and apparatus for drying lumber including a single elongate chamber through which lumber may be moved for drying.

One more object is to provide apparatus for drying lumber which may be easily automated thus reducing operational manpower requirements.

Still another object is to provide apparatus for drying lumber by solvent extraction which requires the use of a relatively small amount of solvent at any one time as compared with known immersion techniques.

One more object is to provide a method and apparatus for drying lumber using methanol as a solvent which is safe from tire and explosion.

Still another object is to provide a method and apparatus for drying all types of lumber, but which is particularly useful for drying difficult to dry woods such as redwood.

One more object is to provide an apparatus for drying lumber which is in effect a packed distillation column lying on its side wherein the wood to be dried functions as the packing for the column.

Another object is to provide a method and apparatus for rapidly during lumber which produces high quality dried lumber,

Other and additional advantages will be apparent from the following description taken in conjunction with the accompanying drawings.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. I is a diagrammatic view of a typical lumber drying apparatus made according to the instant invention.

FIG. 2 is a section taken along line 22 of FIG. 1.

FIG. 3 is a section view taken along line 33 of FIG. 2.

FIG. 4 is a perspective view of a typical solvent distribution apparatus useful in the instant invention.

FIG. 5 is a partial perspective view of a typical spacer used to hold pieces of lumber to be dried at a distance from each other.

FIG. 6 is a partial side elevation view of a typical air vent for use in the end compartments of the present invention.

DETAILED DESCRIPTION OF THE INVENTION Referring initially to FIG. 1, an apparatus indicated generally by the index number 10 for drying lumber by solvent extraction and made according to the teachings of the instnt invention is disclosed. As shown, apparatus 10 includes an elongate chamber 12 comprising a first compartment 14, a second compartment 16, and a third compartment 18 separated from each other by

scalable doors

20 and 22 which, as shown, are movable vertically in tracks to allow the second compartment to be sealed with respect to the first and third longitudinally spaced compartments in elongate chamber 12. Overhead

sealable doors

24 and 26 are shown similarly mounted on the entrance and exit ends of elongate chamber 12 to allow the first and third compartments to be sealed with respect to the atmosphere. Seals of varying types, including inflatable seals which employ controlled air pressure to expand the seal, may be mounted on all of the doors to reduce degradation of the temperature and vapor conditions within the apparatus during lumber drying.

Pieces of wet lumber 28 to be dried are stacked on a conveying apparatus such as cart 30 including pairs of wheels 31 which run on tracks 32 which extend longitudinally through chamber 12. Carts 30 are preferably constructed of wood, stainless steel, or some other material which will not be damaged by prolonged contact with the solvent and solvent laden vapor within the drying chamber. In one embodiment of the instant wood drying apparatus, carts 30 may be 20 feet long, 4 feet wide and have side supports 8 feet high, while chamber 12 is approximately feet long but of similar cross-section such that six carts loaded with lumber may be within the chamber at one time. Chamber dimensions, including its length, may be varied depending on the volume and average condition of lumber to be treated, for instance the chamber may be constructed 20 feet wide such that lumber carts having 20 foot long pieces of lumber stacked crosswise thereon may be moved through the chamber in a high volume operation. Treatment time within the chamber for each cart load of lumber may vary between 3 and 6 days depending on the type and condition of the lumber treated and other known factors. If longer drying times are needed for very wet wood, the chamber may be lengthened thereby increasing the length of time the wood is treated therein.

Chamber 12 may be laid horizontally in a horseshoe or circular shape depending on space requirements and it is also contemplated that the chamber could be disposed vertically, thereby eliminating the need for the plurality of solvent pumps described hereafter with reference to the horizontal unit, but requiring elevator apparatus capable of lifting the wood to be dried therethrough. Forms of conventional horizontal conveying apparatus other than that illustrated, may be used with the apparatus disclosed in FIG. 1, including continuous belt conveyors, for example. While a motive apparatus for the carts 30 has not been illustrated, it will be understood that they may be moved through elongate structure 12 by any conventional means such as a continuous tugger chain or cable or the like.

FIG. 5 illustrates one type of spacer 34 positionable between the pieces of lumber 28 as they are stacked on carts 30 to maintain vapor circulation gaps therebetween. Spacer 34 may include a central spine portion 36 and oppositely disposed space ribs 38 as shown, or any other similarly functioning shape. In the illustrated embodiment, spacer 34 may be /5 inch high, 1 inches wide and 48 inches long such that when it is positioned transverse cart 30 it substantially spans the width of the cart. As will be more completely described hereafter, heated vapor travels longitudinally through the spaces between the stacked lumber from the wet wood input end of compartment 16 toward the dry wood exit end of the compartment to assist in solvent wetting of all surfaces of the stacked lumber. It will be understood that the lumber is stacked on the carts such that the treating liquid may flow over and around all sides of each piece.

In one mode of operation, compartment 16 is filled with four carts 30 of lumber stacked with spacers 34 between individual pieces while compartment 18 houses a single cart load of lumber. Initially,

doors

20, 22 and 26 are closed and sealed while door 24 is opened to allow a cart of wet lumber to be moved into the compartment 14 to the position shown in FIG. 1. Reboiler or steam generator 40 of a conventional type operates slightly over atmospheric pressure and is interconnected by means of steam carrying conduits 42 to each of the

compartments

14, 16 and 18. Steam may be directed to one or more of the compartments as desired during operation by opening or closing valves mounted along the conduits 42. For example, with

doors

20, 22 and 26 sealed and door 24 opened, valve 44 is closed while

valves

46 and 48 are opened such that steam is directed from reboiler 40 to both of the compartments l6 and 18. When the wet stacked lumber is moved into compartment 14, door 24 is closed and sealed, door raised, and valve 46 closed while valve 44 is opened to direct steam directly into compartment 14 through orifice 50.

Air vent 51 is shown in FIG. I mounted on the side of compartment 14 and is more completely disclosed in FIG. 6. As steam enters the top of chamber 14, the cold air therein is pushed out tube 53 near the bottom of the compartment. When the cold air has been substantially exhausted from the compartment and steam begins to be forced out pipe 53, the steam is condensed in condenser 55, filling the neck 57 of tube 53 until the differ ential pressure is sufficient to stop the flow of steam therethrough. A similar air vent 51 is also shown in FIG. 1 to be mounted on compartment 18 to operate in a similar manner when cold air is driven therefrom afte the closing of door 26.

As'described more completely hereafter, the steam overflows compartment 14' into compartment 16 and moves between the lumber stacked on the carts therein toward the dry wood exit end of the compartment at door 22. Asthe steam moves through compartment 16 it is progressively cooled by contact with boiling solvent wetting the lumber. The steam'or vapor phase, as it is more properly called, takes on a progressively greater vaporized solvent content as it moves toward the dry wood exit end of compartment 16, while the solvent or liquid phase flowing from the dry wood end of the compartment toward the wet wood entrance end takes on a progrssively grater water content. Further, as the solvent flows toward the wet wood entrance end of compartment 16, it encounters a vapor phase having a progressively higher temperature such that progressively greater amounts of solvent are vaporized, which vaporized solvent, as mentioned above, is driven toward the dry wood wxit end of the compartment. In this manner it will be understood that the compartment 16 continually distills the solvent employed to replace the water within the lumber, thus eliminating the need for the separate distillation column found generally in the prior art.

The steam entering compartment 14 is heated by reboiler 40 to approximately 212, and the steam treatment of the cart load of wet lumber within chamber 14 performs the multiple function of cleaning the lumber of sawdust and dirt which may have accumulated thereon, raising its temperature to near 212, and open-. ing the pores of the wood thereby conditioning it for the subsequent portion of the drying treatment carried out in compartment 16. In operation, all of the lumber carts within chamber 12 will be' moved one cart position forward toward dry wood exit door 26 after a uniform time interval. The length of the time interval between movements in controlled by the solvent wetting operations carried on in compartment 16 wherein the moisture in the lumber is replaced by solvent such that a cart load of stacked lumber leaving compartment 16 will have reached a desired minimal moisture content prior to solvent stripping in compartment 18.

At the expiration of one treating interval, valve 48 is closed and door 26 opened while door 22 remains sealed such that the cart 'of dried lumber within compartment 18 may be removed. The solvent removal process in compartment 18 may be controlled such that the lumber leaving chamber 12 has a water content of between 8 percent and 10 percent and a solvent content of approximately 2 percent. Door 26 is then closed and sealed and valve 48 opened to refill chamber 18 with steam. During refilling of compartment 18 with steam, valve 52 on exhaust pipe 54 extending from compartment 18 is initially opened to allow the air within the chamber 18 to be substantially exhausted, at which time valve 52 is closed. Door 22 is then opened and the five remaining carts of stacked lumber are moved forward one cart length such that a cart is positioned within compartment 18 while compartment 14 isemptied.

Doors

20 and 22 are then closed, valve 46 opened, valve 44 closed, and door 24 raised to allow a new cartof wet lumber to be .moved into the chamber as previously described. With the newcart load of wet lumber within chamber 14,- door 24 is closed, and valve 44 opened. to allow steam to replace the-airwithin chamber 14. When a steam atmosphere and tempera ture of near 212F. is obtained within compartment 14, door 20 is opened and valve 46 closed thus producing the general treating arrangement wherein all doors but door 20 are closed and sealed and wherein steam is fed directly into compartments l4 and l8.

Referring now to FIG. .2, solvent distributing weir 56d is shown mounted at the top of compartment 16 above the stacked lumber. It will be understood that compartment 16' includes a plurality of such weirs 56a-56f similarly mounted and spaced longitudinally along the top portion of the compartment. FIG. 4 more completely discloses the construction of a typical distributing weir, including a first main distributing trough 58 into which solvent is fed through pipe 59 running from one of a plurality of sumps at the bottom of the compartment. Trough 58 includes a plurality of spaced openings 60 through which the solvent drains into a plurality of transversely oriented troughs 62 each of which include a number of spaced solvent distributing notches 64 through which solvent flows onto the stacked lumber therebelow.The size and trough and notch arrangement of weirs 56 may be varied to achieve maximum spreading of the solvent over the lumber so that a substantial portion of the lumber is wet directly by the solvent, but direct wetting of all surfaces of the lumber is not necessary since the vapor phase composed of steam and solvent passing the unwetted lumber also tends to condense thereon thus wetting every exposed surface of the stacked lumber.

A conventional spray system comprising pipes having a plurality of spray nozzles positioned around the stacked lumber may be used in place of the illustrated weir trough distributors. However, since higher pumping pressures are required for spray nozzles, and sawdust or other particulate matter tends to plug the nozzles, spraying the boiling solvent presents economic and operational problems which need not be considered when using a weir trough distribution system of the type commonly used in packed distillation columns.

As is best ssen in FIG. 2, a flow barrier or weir 660 including laterally spaced notches 68 is mounted on the bottom of compartments 16. FIG. 1 discloses a plurality of weirs 66a-66g spaced on the bottoms of compartments l4 and 16 to define catch basins 70 in which the liquid dripping from the stacked lumber is caught. The liquid fills the catch basins 70 to a depth regulated by the notches in weirs 66 and then overflows through the notches into the next adjacent basin toward the wet wood entrance end of the chamber. The flow from basin to basin may be induced by sloping the floor of the elongate chamber a slight amount such as 2 inches over the length of the entire chamber, or progressively lowering the bottoms of the notches 68 in the weirs all illustrated in FIG. 3.

Again as seen in FIG. 2, baffle 720 is positioned within compartment 16 above weir 66c such that it substantially fills the cross sectional area of compartment 16 except for an opening through which carts 30 and their loads of stacked lumber may be moved. FIG. 1 discloses that similarly shaped baffles 72a-72d are positioned above each of the weirs in compartment 16 and are thus located between each of the longitudinally spaced weir rough distributors 56a56f. The baffles '72 snugly surrounds the carts and their loads of stacked lumber and thus prevent the rapid passage of the vapor phase from the wet wood end of compartment 16 to its dry wood end except through the longitudinal spaces between the individual pieces of the stacked lumber. In one embodiment, baffles 72 may be constructed of plastic strips stiffened with wire to allow a degree of flexibility should a baffle be contacted by one of the pieces of lumber stacked on a cart, however, it will be understood that a variety of other materials might also be satisfactorily used to accomplish a similar purpose.

The baffles define-a series of subcompartments A-F within compartment 16, each of which subcompartments includes a weir trough solvent distributor 56, a catch basin 70 and a sump 74 including a pump 82 for pumping the solvent at its boiling temperature from the bottom of each subcompartment through pipe 59 to the weir trough distributor spaced thereabove. Sumps 74 may have a depth of from 2 to 3 feet to provide a positive head for pumps 82 thus allowing the solvent within the sump to be pumped at its boiling temperature to the weir trough distributor thereabove without having the boiling liquid flash to the vapor state. The recirculation rate of solvent should be such that the top surface of the stacked lumber is continuously flooded with the solvent running onto the pieces of lumber stacked therebelow. A seal-less immersible centrifugal pump of a type commercially available may be satisfactorily used to pump the boiling solvent. The sumps reduce the amount of solvent needed within the system as well as reducing the required weight of the entire drying chamber.

FIG. 2 illustrates one mode of constructing chamber 12 wherein an inner sheet metal wall is spaced from an outer surface of tar paper or the like by approximately three inches of fiberglas insulation. It will be understood that the sheet metal walls are appropriately stiffened to withstand the slight pressure head which may be developed within the chamber during operation. The floor of the chamber as well as the walls and ceiling thereof may be constructed in this manner to provide a well insulated but extremely inexpensive structure. Other like materials may also be substituted therefor within the scope of this invention.

Condenser 76, which may be of any suitably sized commercially available type, is connected to a subchamber A located at the dry wood exit end of compartment 16 by means of conduit 78 through which the vapor phase which has been driven to this subcompartment is drawn off. Conduit 80 is illustrated returning the condensed vapor phase at a temperature near its boiling point to weir trough distributor 56a.

In operation of the disclosed apparatus to continuously dry lumber and using methanol as a solvent, steam at near 21 2F. flows from reboiler 40 through orifice 50 into compartment 14. As the steam fills compartment 14, it overflows into compartment 16 where it moves between the spaced lumber mounted on the longitudinally aligned carts through the successive subcompartments F to A in chamber 16 toward the dry wood exit end thereof. Simultaneously, substantially pure methanol from condenser '76 is fed at near its boiling temperature of 148F. to weir trough distributor 56a. The boiling solvent is distributed over and wets the stacked lumber within subchamber A, and then drains into basin a and associated sump 740 where it is pumped back to weir trough distributor 560. -When basin 70a is filled, the solvent flows through the notches in weir 660 into the next adjacent basin 70b where it is again circulated over the stacked lumber in subcompartment B. As the boiling solvent at near 148F. runs over the stacked lumber in the presence of the vapor phase which has migrated through the subcompartments F-A from chamber 14, the solvent tends to condense a portion of the higher temperature water vapor in the vapor phase thus causing the solvent to take on water as it flows toward the wet wood entrance end of compartment 16. Simultaneously, the high temperature water vapor in the vapor phase vaporizes a portion of the boiling solvent threby causing the vapor phase to take on a progressively greater percentage of solvent as it moves toward subcompartment A where it is withdrawn and condensed. The vapor phase within each of the subchambers is a mixture of water and solvent at its boiling point tending toward heat and mass equilibrium, while the liquid phase employed to wet the stacked lumber in each of the subcompartments is a water and boiling liquid solvent mixture which is also tending toward heat and mass equilibrium. It will thus be understood that the entire drying chamber is designed to approach and be maintained at the boiling point of the phase mixture at any point therein.

For example, in subqompartment F at the wet wood entrance end of compartment 16, the liquid and vapor phases may consist of over 98 percent water and less than 2 percent methanol, thus having a boiling point of approximately 205F. On the other hand, the composition of the liquid and vapor phases in subcompartment A at the dry wood exit end of compartment 16, may consist of over 95 percent methanol and less than 5 percent water, for example, and thus have a boiling point of approximately 149F. subcompartments E through B are filled with liquid-vapor phases having progressively greater proportions of methanol and lesser proportions of water at progressively lower temperatures running between the 195F. temperature in subchamber F progressively downward to the 149F. temperature in subchamber A. As the lumber is moved toward the dry wood exit end of compartment 16, the progressively more concentrated solvent liquid and vapor phases encountered cause the solvent to progressively replace a greater portion of the water within the lumber, until when the stacked lumber is ready for removal into compartment 18, substantially all of the water in the lumber has been replaced by methanol. It will be understood that in this process, water is removed from the lumber as a liquid, not a vapor, thus further adding to the water content of the liquid phase within compartment 16 as it flows toward the wet wood entrance end thereof.

It has been calculated that in order to obtain a moisture content blow percent after solvent stripping in compartment 18, the methanol returned to compartment 16 by the condenser 76 should be 98 percent by wt. methanol. This may be accomplished by maintaining the amount of methanol in the system high enough to produce this purity level. The length of compartment 16 is important in this context, because if the compartment is too short the concentration of the liquid mixture pumped to the reboiler may exceed the relatively low methanol level necessary for economic operation, i.e., for minimal methanol loss in the reboiler. It is estimated that ideally the concentration should be less than 0.2 percent by wt. methanol, but higher methanol concentrations could be tolerated and still maintain economic operation. The effect of a short chamber may be partly overcome by increasing the amount of steam pumped from the reboiler to compartment 14, although this would also increase operating cost to some extent as well as increasing the reflux ratio, overflow/product, of compartment 16. Ideally, it is estimated that the heat input to the reboiler should-be such that four times as much methanol is condensed by the condenser 76 as is carried out to compartment 18 in the lumber. This ratio approximates the reflux ratio in a normal distillation column.

Since the methanol content of the liquid phase is quite small by the time it is drawn off from either sump 74f by condit 81 as illustrated in FIG. 1 or drawn off at the wet wood entrance end of compartment 14, and pumped to reboiler 40, the amount of methanol boiled off and lost is small. To make up for this solvent loss, and for the solvent carried out of the system by the dried lumber, solvent storage container 84 including valve 86 is interconnected with sump 74a by means of conduit 88. Water soluble extractives from the wood, as well as liquid borne debris may be removed from the liquid by skimming or a like process in the reboiler. Chemicals extracted from the lumber by the methanol may be topped off at any desired point within compartment 16 if desired or they may be allowed to remain within the system. If not removed, the methanol extractives are washed into the basins 70 and carried toward the wet wood entrance end of the compartment with the liquid phase. As the water content of the liquid phase increases, the chamical extractives precipitate out of the liquid phase and are either again deposited on the lumber where they are carried with the lumber toward the dry wood exit end of the compartment or carried in the liquid phase to the reboiler where they may be skimmed. Non-condensibles carried by the vapor phase to the condenser 76 may be vented to the atmosphere.

A thermocouple 91 having a sensor 93 within compartment 16 is illustrated to show one means for monitoring the temperature within the wood drying chamber during operation. It will be understood that similar temperature sensing devices could also be positioned within each of the subcompartments of compartment 16. Means may also be provided at intervals within the chamber 12 to allow the specific gravity of the liquid phase to be measured. Variations in specific gravity may be related to the rate of water removal from the lumber within the chamber and this information is useful for determining the length of treatment times.

When a cart load of stacked lumber has moved through compartment 16 and substantially all of the water therein has been removed and replaced by solvent, the cart is moved into compartment 18 in the manner described heretofore. The stacked lumber is steamed in this compartment to remove the solvent from the lumber, thus leaving the lumber with a desired water content which may be between 8 percent and 10 percent, for example. The dried lumber may then be removed from the elongate chamber.

During the steaming operation in compartment 18, it will be understood that the solvent driven off of the wood mixes with the steam to create a mixture composed of varying proportions of solvent and water during different stages of the solvent removal. A pump and conduit system illustrated by dotted line 90 and having interconnections with. the various subcompartments A-F in compartment 16 may be used to direct the mixture removed from chamber 18 to a subcompartment having a like mixture of solvent and water. In this man ner, the heat in compartment 18 may be reused rather than merely exhausted to the atmosphere thereby improving oprerating efliciencyQA monitoring and valve switching system may be used to measure ths solvent content of the mixture withdrawn from chamber 18 and direct it to the appropriate subchamber A-F.

The disclosed apparatus, is thus useful for carrying out a method of drying lumber wherein stacked lumber is first heated by steam and then treated with boiling solvent-water mixtures having progressively greater solvent contents in the presence of a similarly constituted vapor such that the water within the lumber is progressively replaced by solvent. Simultaneously with this treatment, and within the treating chamber, the solvent is continually distilled thereby eliminating the need for a separate distilling column. When substantially all of the water within the lumber has been replaced by solvent, the lumber is stripped of solvent by steaming to produce substantially dry lumber in a relatively short time.

The invention may be embodied in other specific forms without departing from the spirit or central characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore to be embraced therein.

What is claimed is:

1. A method of drying lumber of solvent extraction comprising the steps of:

conveying said lumber within a substantially closed chamber; wetting said lumber with a boiling liquid mixture of solvent and water in the presence of a vapor mixture of solvent and water such that said solvent replaces a portion of the water in said lumber;

progressively increasing the solvent content in said liquid and vapor mixtures to replace substantially all of the water in said lumber; and

stripping said lumber to remove the solvent therein to produce substantially dry lumber.

2. The method of claim 1 including the step of simultenaeously distilling said solvent within said closed chamber.

3. A method of drying wet lumber by solvent extraction comprising the steps of:

steaming said lumber to raise its temperature to near the boiling point of water;

wetting said lumber with a boiling liquid mixture of water and a minor amount of solvent in the presence of a vapor mixture of water and solvent to cause said solvent to replace a minor portion of the water in said lumber;

progressively increasing the amount of solvent in said liquid and vapor mixtures till said solvent comprises a major portion of said mixtures while maintaining said liquid mixture at its'boiling point to cause said solvent to replace a major portion of the water in said lumber; and

heating said lumber to raise its temperature above the boiling point of said solvent to clean said lumber.

4. A methodof drying stacked wet lumber in a methanol distillation column having a relatively cold end wherein liquid methanol at its boiling temperature enters said column and a hot end wherein steam enters said column, including the steps of:

conveying said stacked lumber into the hot end of said distillation column such that said lumber substantially fills the cross sectional area of said column and acts as the packing therefor;

steaming said lumber;

wetting the surface areas of said stacked lumber with a boiling liquid mixture of water and a small amount of methanol in the presence of said steam to replace a small portion of the water in said wood with methanol;

moving said stacked lumber progressively from said hot end toward said cold end of said distillation column while continually wetting said lumber with a boiling liquid mixture of water and methanol in the presence of a steam and methanol vapor mixture; increasing the methanol content of said lumber wetting mixtures as said lumber moves toward said cold end of said column to replace substantially all of the water in said wood with methanol; and

removing said stacked lumber from the relatively solc end of said distillation column and stripping the methanol from said lumber to produce substantially dry lumber. S. The method of claim 4 including the step of distilling said methanol within said column as said stacked lumber moves toward the relatively cold end of said column.

6. The method of claim 4 including the step of withdrawing and condensing the vapor mixture from the cold end of said column to produce substantially pure methanol.

7. A method of drying wet lumber by solvent extraction comprising the steps of:

moving said wet lumber into a first end of a scalable longitudinal chamber and sealing said chamber;

directing steam into said chamber at its first end such that said stem surrounds said lumber and migrates toward the second end of said chamber; directing a boiling liquid solvent having a boiling point below ZIZ F. into said chamber at its second end in a manner such that said solvent wets said lumber and is prgressively distilled by contact with said steam as it flows toward said first end;

progressively moving said lumber from said first end toward said second end to allow said solvent to replace the water within said lumber; and

steaming said lumber to strip substantially all of said solvent therefrom to produce substantially dry lumber.

8. The method of drying wet lumber of claim 7 including the steps of:

withdrawing liquid from the first end of said longitudinal chamber;

reboiling said liquid to produce steam; and

directing said steam into said first end of said chamber.

9. The method of drying wet lumber of claim 7 including the steps of:

withdrawing vapor from the second end of said longitudinal chamber;

condensing said vapor to produce substantially pure,

boiling solvent; and

directing said boiling solvent into the second end of said chamber.

10. The method of drying lumber of claim 9 including the step of adding additional solvent to said boiling solvent leaving said condenser to make up for solvent losses.

11. The method of claim 7 including the steps of periodically monitoring the water content of said lumber as it moves through said longitudinal chamber.

12. Apparatus for drying stacked pieces of wet lumber by solvent extraction including:

a scalable elongate chamber having a first wet lumber entrance end and a second dry lumber exit end; means conveying lumber through said chamber from said entrance end to said exit end;

boiler means directing steam into said chamber at said entrance end such that it moves toward said exit end;

means directing solvent into said chamber at its exit end such that it flows toward said entrance end; means spaced along said elongate chamber wetting said lumber with said solvent in the presence of said steam such that said solvent replaces water within said lumber as said lumber moves toward said exit end; and

means stripping said lumber to remove said solvent therefrom to produce substantially dry lumber.

13. The apparatus of claim 12 wherein said elongate chamber includes baffle means spaced therealong to snugly surround said lumber such that said steam moves from said entrance end toward said exit end between said stacked pieces of lumber.

14. The apparatus of claim 13 including spacer means inserted between said pieces of stacked lumber to form passageways through which said steam travels from said entrance end to said exit end of said chamber.

15. The apparatus of claim 12 wherein said elongate chamber includes substantially airtight outer doors at said entrance and exit ends and substantially airtight inner doors spaced from said outer doors to define heating compartments at each longitudinal end of said chamber.

16. The apparatus of claim 12 wherein said means wetting said lumber with solvent include solvent distribution means spacedly mounted along the top of said elongate chamber, a sump associated with each of said solvent distribution means and positioned therebelow to catch solvent running ofi said lumber; and, pump means associated with each of said sumps to recirculate solvent from said sump to said solvent distribution means thereabove.

17. The apparatus of claim 12 wherein the means directing solvent into the exit end of said chamber includes condenser means withdrawing solvent vapor from said chamber, condensing it to liquid and retuming said liquid solvent to said chamber.

18. Apparatus for drying stacked lumber by solvent extraction including:

an elongate sealable chamber having a cross-section sized to closely surround stacked lumber positioned therein;

stacked lumber conveying means within said elongate chamber moving said lumber from the entrance end of said chamber to its exit end;

a first compartment within said elongate chamber positioned adjacent said entrance end;

means steaming said stacked lumber within said first compartment;

a second compartment within said elongate chamber adjacent said first compartment wherein said stacked lumber is wet by progressively stronger boiling liquid mixtures of solvent and water in the presence of like proportioned vapor mixtures of solvent and water such that said solvent replaces water within said lumber; and

- a third compartment adjacent said exit end of said chamber wherein said stacked lumber is heated to drive off the solvent within said lumber to produce substantially dry lumber.

19. The apparatus of claim 18 including means holding said stacked pieces of lumber at a spaced distance from each other such that steam from first compartment flows between said pieces of stacked lumber through said second compartment toward said third compartment.

20. The apparatus of claim 18 including door means positioned at each end of said compartments such that each of said compartments may be separately sealed.

2l. The apparatus of claim 18 wherein the means wetting said stacked lumber within said second compartment includes a plurality of weir trough distributors spacedly mounted along the top of said compartment; sump means positioned below each of said weir trough distributors to catch solvent runoff from said lumber; and pump means recirculating solvent from said sumps to said weir trough distributors.

22. The apparatus of claim 21 including bafile means surrounding said stacked lumber between each of said w'eir trough distributor means such that steam from said first compartment means flows toward the exit end of said second compartment means between said stacked lumber. I

23. The apparatus of claim 22 including condenser means withdrawing vapor from adjacent the exit end of said second compartment and returning condensed liquid solvent to said weir trough distributor means adjacent said exit-end.

. III =t= UNETED STATES PATENT OFFKCE CERHFICATE 0F CORRECTION Patent NO. 3 M Dated September 11, 1973 Inventor(s) DONALD A. RUNCIMAN It is certified that error appears in the above-identified patent and that said Letters Patent are hereby corrected as shown below:

In the Abstract, third line from the end, change "close to closed Column 1, line M5, change "contant" to content Column 2, line 19, change "of" to in Column 3, line ll, change sitributor" to distributor Column 5 line H6, change "afte" to after line 59, change grater" to greater and, line 65, change "wxit" to exit i Column 6, line 16, change "in" to is Column 7, line Ml, change "rough" to trough Column 9, line 1, change "subqompartment" to. a

subcompartment and, line 30 change "blow" to below Q Column 10 line 50 change "oprerating" to operating 1 Column ll line 67 change "mixtures" to mixture 7 Column 12 line 3 change "solo" to cold --L a v Column 14 line 17 before "first" insert said Signed and sealed this 25th day of December 1973.

(SEAL) Attest:

EDWARD M.PLETCHER,JR. RENE D. TEGTMEYER Attesting Officer Acting Commissioner of Patents USCOMM-DC 60376-P69 1: us GQVERNMFNT PRINTING OFFICE l9" 0-566-334,

Claims

2. The method of claim 1 including the step of simultenaeously distilling said solvent within said closed chamber.
3. A method of drying wet lumber by solvent extraction comprising the steps of: steaming said lumber to raise its temperature to near the boiling point of water; wetting said lumber with a boiling liquid mixture of water and a minor amount of solvent in the presence of a vapor mixture of water and solvent to cause said solvent to replace a minor portion of the water in said lumber; progressively increasing the amount of solvent in said liquid and vapor mixtures till said solvent comprises a major portion of said mixtures while maintaining said liquid mixture at its boiling point to cause said solvent to replace a major portion of the water in said lumber; and heating said lumber to raise its temperature above the boiling point of said solvent to clean said lumber.
4. A method of drying stacked wet lumber in a methanol distillation column having a relatively cold end wherein liquid methanol at its boiling temperature enters said column and a hot end wherein steam enters said column, including the steps of: conveying said stacked lumber into the hot end of said distillation column such that said lumber substantially fills the cross sectional area of said column and acts as the packing therefor; steaming said lumber; wetting the surface areas of said stacked lumber with a boiling liquid mixture of water and a small amount of methanoL in the presence of said steam to replace a small portion of the water in said wood with methanol; moving said stacked lumber progressively from said hot end toward said cold end of said distillation column while continually wetting said lumber with a boiling liquid mixture of water and methanol in the presence of a steam and methanol vapor mixture; increasing the methanol content of said lumber wetting mixtures as said lumber moves toward said cold end of said column to replace substantially all of the water in said wood with methanol; and removing said stacked lumber from the relatively solc end of said distillation column and stripping the methanol from said lumber to produce substantially dry lumber.
5. The method of claim 4 including the step of distilling said methanol within said column as said stacked lumber moves toward the relatively cold end of said column.
6. The method of claim 4 including the step of withdrawing and condensing the vapor mixture from the cold end of said column to produce substantially pure methanol.
7. A method of drying wet lumber by solvent extraction comprising the steps of: moving said wet lumber into a first end of a sealable longitudinal chamber and sealing said chamber; directing steam into said chamber at its first end such that said stem surrounds said lumber and migrates toward the second end of said chamber; directing a boiling liquid solvent having a boiling point below 212*F. into said chamber at its second end in a manner such that said solvent wets said lumber and is prgressively distilled by contact with said steam as it flows toward said first end; progressively moving said lumber from said first end toward said second end to allow said solvent to replace the water within said lumber; and steaming said lumber to strip substantially all of said solvent therefrom to produce substantially dry lumber.
8. The method of drying wet lumber of claim 7 including the steps of: withdrawing liquid from the first end of said longitudinal chamber; reboiling said liquid to produce steam; and directing said steam into said first end of said chamber.
9. The method of drying wet lumber of claim 7 including the steps of: withdrawing vapor from the second end of said longitudinal chamber; condensing said vapor to produce substantially pure, boiling solvent; and directing said boiling solvent into the second end of said chamber.
10. The method of drying lumber of claim 9 including the step of adding additional solvent to said boiling solvent leaving said condenser to make up for solvent losses.
11. The method of claim 7 including the steps of periodically monitoring the water content of said lumber as it moves through said longitudinal chamber.
12. Apparatus for drying stacked pieces of wet lumber by solvent extraction including: a sealable elongate chamber having a first wet lumber entrance end and a second dry lumber exit end; means conveying lumber through said chamber from said entrance end to said exit end; boiler means directing steam into said chamber at said entrance end such that it moves toward said exit end; means directing solvent into said chamber at its exit end such that it flows toward said entrance end; means spaced along said elongate chamber wetting said lumber with said solvent in the presence of said steam such that said solvent replaces water within said lumber as said lumber moves toward said exit end; and means stripping said lumber to remove said solvent therefrom to produce substantially dry lumber.
13. The apparatus of claim 12 wherein said elongate chamber includes baffle means spaced therealong to snugly surround said lumber such that said steam moves from said entrance end toward said exit end between said stacked pieces of lumber.
14. The apparatus of claim 13 including spacer means inserted between said pieces of stacked lumber to form passageways through which said steam travels from said entrance end to said exit end of said chamber.
15. The apparatus of claim 12 wherein said elongate chamber includes substantially airtight outer doors at said entrance and exit ends and substantially airtight inner doors spaced from said outer doors to define heating compartments at each longitudinal end of said chamber.
16. The apparatus of claim 12 wherein said means wetting said lumber with solvent include solvent distribution means spacedly mounted along the top of said elongate chamber, a sump associated with each of said solvent distribution means and positioned therebelow to catch solvent running off said lumber; and, pump means associated with each of said sumps to recirculate solvent from said sump to said solvent distribution means thereabove.
17. The apparatus of claim 12 wherein the means directing solvent into the exit end of said chamber includes condenser means withdrawing solvent vapor from said chamber, condensing it to liquid and returning said liquid solvent to said chamber.
18. Apparatus for drying stacked lumber by solvent extraction including: an elongate sealable chamber having a cross-section sized to closely surround stacked lumber positioned therein; stacked lumber conveying means within said elongate chamber moving said lumber from the entrance end of said chamber to its exit end; a first compartment within said elongate chamber positioned adjacent said entrance end; means steaming said stacked lumber within said first compartment; a second compartment within said elongate chamber adjacent said first compartment wherein said stacked lumber is wet by progressively stronger boiling liquid mixtures of solvent and water in the presence of like proportioned vapor mixtures of solvent and water such that said solvent replaces water within said lumber; and a third compartment adjacent said exit end of said chamber wherein said stacked lumber is heated to drive off the solvent within said lumber to produce substantially dry lumber.
19. The apparatus of claim 18 including means holding said stacked pieces of lumber at a spaced distance from each other such that steam from first compartment flows between said pieces of stacked lumber through said second compartment toward said third compartment.
20. The apparatus of claim 18 including door means positioned at each end of said compartments such that each of said compartments may be separately sealed.
21. The apparatus of claim 18 wherein the means wetting said stacked lumber within said second compartment includes a plurality of weir trough distributors spacedly mounted along the top of said compartment; sump means positioned below each of said weir trough distributors to catch solvent runoff from said lumber; and pump means recirculating solvent from said sumps to said weir trough distributors.
22. The apparatus of claim 21 including baffle means surrounding said stacked lumber between each of said weir trough distributor means such that steam from said first compartment means flows toward the exit end of said second compartment means between said stacked lumber.
23. The apparatus of claim 22 including condenser means withdrawing vapor from adjacent the exit end of said second compartment and returning condensed liquid solvent to said weir trough distributor means adjacent said exit end.