US3548062A - Gas pressure bonding furnace - Google Patents

Gas pressure bonding furnace Download PDF

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US3548062A
US3548062A US832640A US3548062DA US3548062A US 3548062 A US3548062 A US 3548062A US 832640 A US832640 A US 832640A US 3548062D A US3548062D A US 3548062DA US 3548062 A US3548062 A US 3548062A
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furnace
heating
gases
shell
workpiece
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Expired - Lifetime
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US832640A
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Charles W Smith Jr
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Autoclave Engineers Inc
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Autoclave Engineers Inc
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B11/00Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
    • B30B11/001Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a flexible element, e.g. diaphragm, urged by fluid pressure; Isostatic presses
    • B30B11/002Isostatic press chambers; Press stands therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K1/00Soldering, e.g. brazing, or unsoldering
    • B23K1/008Soldering within a furnace
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • C21D1/767Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material with forced gas circulation; Reheating thereof
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D11/00Arrangement of elements for electric heating in or on furnaces
    • F27D11/02Ohmic resistance heating

Definitions

  • This invention pertains primarily to furnaces for gas pressure bonding or welding of metal assemblies.
  • the assemblies are heated in the presence of gases at superatmospheric pressures to temperatures below their melting point.
  • the temperature throughout the furnace be substantially uniform during the heating, holding and cooling 'of the furnace. Often elongated assemblies mustbe positioned vertically in the furnace.
  • Furnaces according to the teachings of my invention have the advantage of providing substantially'uniform temperatures throughout an elongate interior with areduced number of heating elements and a corresponding reduced amount of control equipment. In fact, in some instances, it is possible to eliminate multiple zone heating altogether. It is a further advantage of my-inventionv that the elongate furnace can be heated and cooled more rapidly than prior furnaces thereby increasing the number of assemblies that can be bonded by use of the furnace in a given period of time.
  • a furnace having a shell which is sealable and can contain gases at superatmospheric pressures. Adjacent the shell is a heat insulating lining. Heating means are disposed adjacent to the insulating wall and spaced about it. The. heating means are shielded from the workspace of the furnace and the workpiece by a baffle arranged to channel a flow of gases during heating along the periphery of the furnace and thence through the interior of the furnace.
  • my invention is a drastic departure from the prior art gas bonding furnaces wherein gas flow was as much as possible suppressed.
  • a new method of heating assemblies or workpieces comprising the steps of placing the workpieces in a sealed enclosure with superatmospheric gases, heating said gases within one portion of the enclosure and channeling the heated gases about the workpiece at a rate sufficiently fast such that the gases adjacent the workpiece have substantially uniform temperatures. In this manner the workpiece, while being'heated, will have a substantially uniform temperature.
  • FIG. 1 is a vertical section view of a furnace according to this invention taken along lines A-A in FIG. 2;
  • H0. 2 is a plan view in section of a furnace according to this invention taken along lines B-B in HO. 1;
  • FIG. 3 is a schematic wiring diagram which illustrates a multiple zone heating system.
  • a furnace is shown with an outer metal shell 1 which is cylindrical, closed at the base and open at the top.
  • a flange is provided about the top of the cylindrical shell.
  • a metal cover 2 can be disposed over the opening.
  • Means 3 are provided for securing the cover to the flange of the outer shell whereby the cover and shell will cooperate to provide a scalable furnace which can contain superatmospheric pressures.
  • a gasket (not shown in the drawings) may be disposed between the cover 2 and the shell 1. Within the shell and directly adjacent its inner edge there is an insulating lining 5.
  • the insulating lining and cover may consist of, for example, insulating fire brick, asbestos board and so on.
  • a valve means 8 is provided attached to an orifice 9 leading to the interior of the furnace. Through the orifice and valve the furnace can be evacuated and then filled with gases suitable for gas pressure bonding.
  • Electrical-heating elements 11 are disposed about the interior of the insulating brick lining. They are preferably wrapped circumferentially about the interior of the furnace and may comprise, for example, Nichrome wire.
  • a baffle 13 is placed between the interior of the furnace and the heating means to form a convection channel 14. The channel is in communication at both its upper and lower ends with the workspace of the furnace.
  • the bottom of the workspace of the furnace 16 has an opening or openings therein.
  • the bottom in the particular embodiment shown in placed on a bed of particulate refractory aggregate 17.
  • the electrical leads 20 and 21 must pass through gastight bushings 22 and 23.
  • a thermocouple 25 is disposed in the furnace and also passes through gastight bushing 26. The number of thermocouples and electrical leads required vary depending on the size of the furnace. It is, of course, desirable to minimize the number of openings passing through the shell which must be sealed.
  • FIG. 3 is a schematic wiring diagram showing a circuit wherein the heating element is divided into more than one zone. Heat introduced in the upper zone of the furnace is less than the heat introduced in the middle and lower zones.
  • a control apparatus is provided to maintain the current through each of the resistors, R R and R approximately uniform.
  • the resistance in R is, of course, less than R which is, in turn less than R.
  • the baffle means is corrugated. It is also preferred that the outer shell, insulating lining and the baffle be tubular and concentric with the shell.
  • the furnace is filled with gas at superatmospheric pressures.
  • Gas is heated in the channel between the baffle and the insulating wire by the electrical heating elements.
  • the heated gas raises to the top of the channel and enters the top of the furnace workspace through an opening provided over the baffle.
  • This movement starts a continuous flow of gas upwardly through the channel and downwardly through the furnace interior.
  • the gas passes through the furnace interior, it transfers its heat to the workpiece or assembly being bonded.
  • the gas flow is maintained sufficiently rapid so that the upper portions of the workpiece are not heated more rapidly than'the lower portions of the workpiece.
  • Some heating is performed on the workpiece by radiation directly from the baffle.
  • the direction of the gas flow is reversed. l have found that a corrugated baffle in which the corrugations run vertical is especially effective at promoting gas flow through the channel and down through the interior of the furnace during heating.
  • the flow of the superatmospheric gas distributes'the heat more uniformly about the workpiece than could be expected by gas at standard pressure.
  • a furnace in which the temperature in the interior of the furnace can be maintained substantially uniform during heating and cooling consisting of means forisealing the furnace and maintaining gases at superatmospheric pressures therein, means for introducing gas under superatmospheric pressures to said furnace, means for heat insulating the furnace, means furnace interior, means for channeling a draft caused by thermal'buoyancy of gases past theheating means and thence through the central furnace interior.
  • An'exigated furnace for gas pressure bonding metal assemblies having a vertical longitudinal axis in which the temperaturecan be maintained in the workspace of the furnace substantially uniform along the longitudinal axis during heating and cooling consisting of an 'outer metal shell which can be sealed and can contain gases at superatmospheric pressures, means for introducing gas under superatmospheric pressures tothe furnace, an insulating wall disposed within and adjacent the metal, shell,-, heating means disposed'adjacent to the insulatingwall baffle means disposed between the workspace of the furnace andnthe heating means forming a convection channel with the insulatingwall, said convection channel in communication with the workspace of the furnace at both ends of the elongated vertical workspace, whereby during heating of the furnace gases move upwardly-due to thermal buoyancy through the convection channel and downwardly through the workspace distributing the heat introduced by the heating means uniformly throughout said workspace.

Description

g and cooling tially uniform sealable shell pheric pressures. Within the Electrical heating means are rnace. During heating of the 5 move through the convech the interior of the furnace maintaining the temperature throughout the furnace substantially uniform.
Inventor Charles W. Smith,Jr. 2,791,418 5/1957 Edelmann Erie, Pa. 3,017,262 1/1962 Fegan......... [21] Appl. No. 832,640 3,097,837 7/1963 Jacob........................... t d 3222 Primary ExaminerBernard A. Gilheany 73 B A l E I Assistant Examiner-RoyN.Enval1,.lr. I sslgnee z ngmeers Attorney-Webb, Burden, Robinson & Webb a corporation of Pennsylvania ABSTRACT: A furnace and process for heatin assemblies while maintaining them at substan temperatures. The furnace comprises an outer 7 Claims, 3 Drawing Figs capable of containing superatmos shell there IS an insulating wall. [52] US. 13/20, disposed adjacent the insulating wa|| A b ffl is disposed 13/31 between the workspace of the furnace and the heating means F279 7/06 forming a convection channel with the insulating wall. The Fleld 219/390, convection channel is in communication with the workspace 400; 31; 263/49 at the top and bottom of the fu furnace, superatmospheric gase References Cited tion channel and thence throug UNITED STATES PATENTS 3/1957 McAllister,et a1. 13/20 United States Patent [54] GAS PRESSURE BONDING FURNACE G. wf 1 11 1 11 1 /11 1/ r Q 'LB l l l fl 6 oooooooooooooooo \\1 11 11 1 I! I! I 1 I, 11 11 1/ 11 1 1/ 1 11 11 11 11 I 11 .1 1/ 11 l/ 1/ I 1 PATENTED nun 5 rem Zone Lower INVENTOR. Charles W Smith, Jr:
WM, Ila/Mam i WW H/S ATTORNEYS GAS PRESSURE BONDING FURNACE This invention pertains primarily to furnaces for gas pressure bonding or welding of metal assemblies. In these furnaces, the assemblies are heated in the presence of gases at superatmospheric pressures to temperatures below their melting point. To avoid warping causedby differential thermal expansion of the assemblies or workpieces, it is essential that the temperature throughout the furnace be substantially uniform during the heating, holding and cooling 'of the furnace. Often elongated assemblies mustbe positioned vertically in the furnace. Hence, it is necessary to have elongate furnace chambers having a long vertical axis.'lt is extremely'difticult to provide substantially uniform temperatures in these furnaces because of the tendency of the hotter gases to rise to the upper end of the elongate furnace chamber.
In the past, every effort was made to reduce the gas circulation around the workpiece and the temperature of the furnace interior was controlled by a plurality of individually controllable electric-heating elements spaced in zones vertically along the furnace walls. The multiple-heating elements required extensive control equipment and also required numerous electrical leads each of which had to pass through'the shell of the furnace making sealing more difficult. Notwithstanding the elaborate heating and controlling equipment, the prior art furnaces had to be heated and cooled very slowly 'in order to maintain the temperature substantially uniform throughout the workpiece or assembly.
Furnaces according to the teachings of my invention have the advantage of providing substantially'uniform temperatures throughout an elongate interior with areduced number of heating elements and a corresponding reduced amount of control equipment. In fact, in some instances, it is possible to eliminate multiple zone heating altogether. It is a further advantage of my-inventionv that the elongate furnace can be heated and cooled more rapidly than prior furnaces thereby increasing the number of assemblies that can be bonded by use of the furnace in a given period of time.
Briefly, according to this invention, there is provideda furnace having a shell which is sealable and can contain gases at superatmospheric pressures. Adjacent the shell is a heat insulating lining. Heating means are disposed adjacent to the insulating wall and spaced about it. The. heating means are shielded from the workspace of the furnace and the workpiece by a baffle arranged to channel a flow of gases during heating along the periphery of the furnace and thence through the interior of the furnace. Hence, my invention is a drastic departure from the prior art gas bonding furnaces wherein gas flow was as much as possible suppressed.
Also according to this invention, there is provided a new method of heating assemblies or workpieces comprising the steps of placing the workpieces in a sealed enclosure with superatmospheric gases, heating said gases within one portion of the enclosure and channeling the heated gases about the workpiece at a rate sufficiently fast such that the gases adjacent the workpiece have substantially uniform temperatures. In this manner the workpiece, while being'heated, will have a substantially uniform temperature. t
FIG. 1 is a vertical section view of a furnace according to this invention taken along lines A-A in FIG. 2;
H0. 2 is a plan view in section of a furnace according to this invention taken along lines B-B in HO. 1; and
FIG. 3 is a schematic wiring diagram which illustrates a multiple zone heating system.
Before describing the drawings in detail, it should be understood that they illustrate one furnace embodying the concepts of this invention, and are given by way of explanation and not by way of limitation. ln'FlGS. land 2, a furnace is shown with an outer metal shell 1 which is cylindrical, closed at the base and open at the top. A flange is provided about the top of the cylindrical shell. A metal cover 2 can be disposed over the opening. Means 3 are provided for securing the cover to the flange of the outer shell whereby the cover and shell will cooperate to provide a scalable furnace which can contain superatmospheric pressures. A gasket (not shown in the drawings) may be disposed between the cover 2 and the shell 1. Within the shell and directly adjacent its inner edge there is an insulating lining 5. There is also a removable insulating cover 6. The insulating lining and cover may consist of, for example, insulating fire brick, asbestos board and so on. A valve means 8 is provided attached to an orifice 9 leading to the interior of the furnace. Through the orifice and valve the furnace can be evacuated and then filled with gases suitable for gas pressure bonding. Electrical-heating elements 11 are disposed about the interior of the insulating brick lining. They are preferably wrapped circumferentially about the interior of the furnace and may comprise, for example, Nichrome wire. A baffle 13 is placed between the interior of the furnace and the heating means to form a convection channel 14. The channel is in communication at both its upper and lower ends with the workspace of the furnace. The bottom of the workspace of the furnace 16 has an opening or openings therein. The bottom in the particular embodiment shown in placed on a bed of particulate refractory aggregate 17. The electrical leads 20 and 21 must pass through gastight bushings 22 and 23. A thermocouple 25 is disposed in the furnace and also passes through gastight bushing 26. The number of thermocouples and electrical leads required vary depending on the size of the furnace. It is, of course, desirable to minimize the number of openings passing through the shell which must be sealed.
FIG. 3 is a schematic wiring diagram showing a circuit wherein the heating element is divided into more than one zone. Heat introduced in the upper zone of the furnace is less than the heat introduced in the middle and lower zones. A control apparatus is provided to maintain the current through each of the resistors, R R and R approximately uniform. The resistance in R is, of course, less than R which is, in turn less than R Actually because of the advantages of this invention, simple single zone heating elements can be used. According to a preferred aspect of this invention, the baffle means is corrugated. It is also preferred that the outer shell, insulating lining and the baffle be tubular and concentric with the shell.
During heating, the furnace is filled with gas at superatmospheric pressures. Gas is heated in the channel between the baffle and the insulating wire by the electrical heating elements. The heated gas raises to the top of the channel and enters the top of the furnace workspace through an opening provided over the baffle. This movement starts a continuous flow of gas upwardly through the channel and downwardly through the furnace interior. As the gas passes through the furnace interior, it transfers its heat to the workpiece or assembly being bonded. The gas flow is maintained sufficiently rapid so that the upper portions of the workpiece are not heated more rapidly than'the lower portions of the workpiece. Some heating, of course, is performed on the workpiece by radiation directly from the baffle. During cooling the direction of the gas flow is reversed. l have found that a corrugated baffle in which the corrugations run vertical is especially effective at promoting gas flow through the channel and down through the interior of the furnace during heating.
While I do not completely understand the scientific basis of my invention, I believe the success thereof may have to do with the nature of gases under superatmospheric pressures. As pressures are increased, gases flow more and more like liquids.
The flow of the superatmospheric gas distributes'the heat more uniformly about the workpiece than could be expected by gas at standard pressure.
Having described my invention with the particularity required by the patent laws, what is desired to have protected by letters patent is set forth in the following claims.
I claim:
1. A furnace in which the temperature in the interior of the furnace can be maintained substantially uniform during heating and cooling consisting of means forisealing the furnace and maintaining gases at superatmospheric pressures therein, means for introducing gas under superatmospheric pressures to said furnace, means for heat insulating the furnace, means furnace interior, means for channeling a draft caused by thermal'buoyancy of gases past theheating means and thence through the central furnace interior.
2. An'elorigated furnace for gas pressure bonding metal assemblies having a vertical longitudinal axis in which the temperaturecan be maintained in the workspace of the furnace substantially uniform along the longitudinal axis during heating and cooling consisting of an 'outer metal shell which can be sealed and can contain gases at superatmospheric pressures, means for introducing gas under superatmospheric pressures tothe furnace, an insulating wall disposed within and adjacent the metal, shell,-, heating means disposed'adjacent to the insulatingwall baffle means disposed between the workspace of the furnace andnthe heating means forming a convection channel with the insulatingwall, said convection channel in communication with the workspace of the furnace at both ends of the elongated vertical workspace, whereby during heating of the furnace gases move upwardly-due to thermal buoyancy through the convection channel and downwardly through the workspace distributing the heat introduced by the heating means uniformly throughout said workspace.
3. A furnace according to claim 2 in which the shell, insulating wall and baffle means are substantially tubular and concentric. g
4. A furnace according to claim 2 in which the baffle means is corrugated.
5. A furnace according to claim 2 in which the heating means comprises electrical resistance elements wrapped cir curnferentially around the furnace and spaced vertically.
6. A furnace according to claim 5 in which the heating element comprises at least twoindividually controllable sections vertically spaced.
7.- A method of heating a workspace while maintaining sub-' stantially-mniform temperature throughout the workpiece comprising the steps of:
l. placing the workpiece in a sealed enclosure with superatmospheric gases, 2. heatingsaid gases within a portion of said enclosure, and 3. channeling a draft of said heated gases caused by thermal buoyancy about the workpiece at a rate sufficiently fast such that the temperature of the'gases adjacent the workpiece are substantially uniform. 1
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4007325A (en) * 1975-08-13 1977-02-08 National Forge Company Furnace assembly
US4022446A (en) * 1975-10-23 1977-05-10 Autoclave Engineers, Inc. Quenching in hot gas isostatic pressure furnace
US4131419A (en) * 1976-05-25 1978-12-26 Asea Aktiebolag Furnace for the high temperature-high pressure treatment of materials which includes pressure medium circulation channels
US4151400A (en) * 1977-06-15 1979-04-24 Autoclave Engineers, Inc. Autoclave furnace with mechanical circulation
US4247755A (en) * 1978-01-16 1981-01-27 Autoclave Engineers, Inc. High pressure autoclave
US4359336A (en) * 1979-07-16 1982-11-16 Pressure Technology, Inc. Isostatic method for treating articles with heat and pressure
US4471949A (en) * 1982-04-13 1984-09-18 Kabushiki Kaisha Kobe Seiko Sho Hot isostatic pressing system
US4602769A (en) * 1984-05-11 1986-07-29 National Forge Company Apparatus for the cooling of articles which have been subjected to an isostatic pressing process
US4753192A (en) * 1987-01-08 1988-06-28 Btu Engineering Corporation Movable core fast cool-down furnace
EP0330922A1 (en) * 1988-03-02 1989-09-06 Siemens Nixdorf Informationssysteme Aktiengesellschaft Reflow process for circuit boards

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4007325A (en) * 1975-08-13 1977-02-08 National Forge Company Furnace assembly
US4022446A (en) * 1975-10-23 1977-05-10 Autoclave Engineers, Inc. Quenching in hot gas isostatic pressure furnace
US4131419A (en) * 1976-05-25 1978-12-26 Asea Aktiebolag Furnace for the high temperature-high pressure treatment of materials which includes pressure medium circulation channels
US4151400A (en) * 1977-06-15 1979-04-24 Autoclave Engineers, Inc. Autoclave furnace with mechanical circulation
US4247755A (en) * 1978-01-16 1981-01-27 Autoclave Engineers, Inc. High pressure autoclave
US4359336A (en) * 1979-07-16 1982-11-16 Pressure Technology, Inc. Isostatic method for treating articles with heat and pressure
US4471949A (en) * 1982-04-13 1984-09-18 Kabushiki Kaisha Kobe Seiko Sho Hot isostatic pressing system
US4602769A (en) * 1984-05-11 1986-07-29 National Forge Company Apparatus for the cooling of articles which have been subjected to an isostatic pressing process
US4753192A (en) * 1987-01-08 1988-06-28 Btu Engineering Corporation Movable core fast cool-down furnace
EP0330922A1 (en) * 1988-03-02 1989-09-06 Siemens Nixdorf Informationssysteme Aktiengesellschaft Reflow process for circuit boards
US5174020A (en) * 1988-03-02 1992-12-29 Siemens Aktiengesellschaft Remelting process for printed circuit boards

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