US3185162A - Process for making reconstituted sheet tobacco - Google Patents

Process for making reconstituted sheet tobacco Download PDF

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Publication number
US3185162A
US3185162A US73562A US7356260A US3185162A US 3185162 A US3185162 A US 3185162A US 73562 A US73562 A US 73562A US 7356260 A US7356260 A US 7356260A US 3185162 A US3185162 A US 3185162A
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US
United States
Prior art keywords
tobacco
sheet
coating
sheet tobacco
making reconstituted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US73562A
Inventor
Fiore Joseph Vincent
Hooper Harry Allison
Monte Matthew Sallee
Moshy Raymond Joseph
Schmidt Otto Karl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AMF Inc
Original Assignee
AMF Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by AMF Inc filed Critical AMF Inc
Priority to US73562A priority Critical patent/US3185162A/en
Priority to GB43074/61A priority patent/GB940129A/en
Priority to DK483461AA priority patent/DK130134B/en
Priority to DE19611517287 priority patent/DE1517287A1/en
Priority to CH1407161A priority patent/CH437091A/en
Priority to US404198A priority patent/US3185161A/en
Application granted granted Critical
Publication of US3185162A publication Critical patent/US3185162A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/186Treatment of tobacco products or tobacco substitutes by coating with a coating composition, encapsulation of tobacco particles
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco

Definitions

  • This invention relates in general to tobacco processing and, more particularly, to coated reconstituted tobacco sheet.
  • Tobacco sheet may be made by depositing a thin layer of an aqueous or other suspension of finely-divided tobacco and a suitable binder on a flat surface. The thin layer is then dried and removed from the surface as tobacco sheet.
  • tobacco sheet If such tobacco sheet is used as a cigar wrapper, it should exhibit all the features of a natural tobacco leaf cigar wrapper such as good color and sheen, a natural feel, no stickiness in the mouth, no unusual or bitter flavor characteristics, good burn aroma and taste, and a good burn rate, as well as water resistance.
  • tobacco sheet yields a better performance than natural leaf on cigarmaking machines because it has more uniform physical characteristics than do varied natural tobacco leaves, heretofore some tobacco sheet has lacked the aforementioned desired properties.
  • the invention relates to coating manufactured tobacco sheets with a thin layer of protective material on either one or both sides. It may be used on sheets made by a paper-making process, a process where dust is adhered to a sticky film or where dust is mixed with a binder. When the coating is hydrophobic there is a marked increase in resistance to moisture penetration. When coated on both sides, the sheet is waterproof.
  • a coating must have more than useful physical properties. It must not be noxious or toxic in the amounts used; it must have an acceptable taste and appearance and not detract from the tobacco character of a smoking article. Moreover, the coating material and method must be easy and practical to use with delicate tobacco material.
  • the coating is preferably used on the surface of the sheet which is outermost on the smoking article. Both sides of the sheet may be coated when protection against chewing a desired. Also, several successive layers of coating material may be appplied to the sheet, and in particular to the area at the mouth end of a smoking article. Coating may be applied in the course of sheet manufacture or on the finished smoking article.
  • the invention particularly concerns making a moisture resistant tobacco product and includes or comprises forming a sheet of tobacco by mixing a major proportion by weight of finely divided tobacco With a minor proportion by weight of water soluble adhesive, such as a 3,185,162 Patented May 25, 1965 ice cellulose ether, e.g., ethyl hydroxyethyl cellulose, in aqueous solution and drying the sheet so formed. Thereafter the improvement consists of coating the surface of the dried sheet witha solution of ethyl cellulose and iinally drying the coating to produce a thin, flexible surface coating which protects the water soluble adhesive and the tobacco from attack and degradation by external moisture and is compatible with the smoking quality of the tobacco product.
  • water soluble adhesive such as a 3,185,162 Patented May 25, 1965 ice cellulose ether, e.g., ethyl hydroxyethyl cellulose
  • Example 0.5 part locust beam gum is added slowly, with agitation, to a 2.5% suspension of 1 part of highly refined sulfite pulp in water and agitation is continued until solution is complete.
  • To the resulting dispersion is added, with stirring, 0.75 part diethylene glycol humectant, 0.5 part dialdehyde starch wet strength agent (as a 10% solution), 0.7 part diatomaceous earth and 6 parts tobacco dust (screen through mesh) which has been prewetted with water (1 part tobacco to 2 parts Water).
  • 0.5 part ethyl hydroxyethyl cellulose adhesive are blended in carefully and the total solids adjusted to 10%.
  • the resulting dispersion is cast on a moving stainless steel belt. The sheet on the belt is dried and then coated with an alcoholic solution of ethyl cellulose and the coating dried.
  • a hydrophobic coating on the sheet which may be used is ethyl-cellulose. This may be applied in either an alcoholic solution or as an aqueous emulsion.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Description

PROCESS FOR MAKING RECONSTITUTED SHEET TOBACCO Joseph Vincent Flore, Fairfield, Conn., Harry Allison Hooper, Larchmont, N.Y., and Matthew Sailee Monte,
Stratford, Raymond Joseph Moshy, Westport, and Otto Karl Schmidt, Springdale, Conn., assignors to American Machine & Foundry Company, a corporation of New Jersey Filed Dec. 5, 1960, Ser. No. 73,562
No Drawing.
1 Claim. (Cl. 131140) This invention relates in general to tobacco processing and, more particularly, to coated reconstituted tobacco sheet.
Tobacco sheet may be made by depositing a thin layer of an aqueous or other suspension of finely-divided tobacco and a suitable binder on a flat surface. The thin layer is then dried and removed from the surface as tobacco sheet.
If such tobacco sheet is used as a cigar wrapper, it should exhibit all the features of a natural tobacco leaf cigar wrapper such as good color and sheen, a natural feel, no stickiness in the mouth, no unusual or bitter flavor characteristics, good burn aroma and taste, and a good burn rate, as well as water resistance. Although tobacco sheet yields a better performance than natural leaf on cigarmaking machines because it has more uniform physical characteristics than do varied natural tobacco leaves, heretofore some tobacco sheet has lacked the aforementioned desired properties.
It is, therefore, an object of this invention to provide tobacco sheets, which may be used for cigar wrappers and in other smoking articles, which look, feel and taste like natural tobacco leaf.
This and other objects, advantages and features of invention will become apparent from the following description.
The invention relates to coating manufactured tobacco sheets with a thin layer of protective material on either one or both sides. It may be used on sheets made by a paper-making process, a process where dust is adhered to a sticky film or where dust is mixed with a binder. When the coating is hydrophobic there is a marked increase in resistance to moisture penetration. When coated on both sides, the sheet is waterproof.
Clearly a coating must have more than useful physical properties. It must not be noxious or toxic in the amounts used; it must have an acceptable taste and appearance and not detract from the tobacco character of a smoking article. Moreover, the coating material and method must be easy and practical to use with delicate tobacco material.
Many tobacco sheets have been made from water soluble adhesives which are limited in use by a tendency to disintegrate in the mouth. Mouth pieces have been used to overcome this and reinforcing tapes have also been used. However, a flexible, non-brittle coating is a far more elegant solution to this problem.
When the sheet is used as a wrapper on a cigar, for example, the coating is preferably used on the surface of the sheet which is outermost on the smoking article. Both sides of the sheet may be coated when protection against chewing a desired. Also, several successive layers of coating material may be appplied to the sheet, and in particular to the area at the mouth end of a smoking article. Coating may be applied in the course of sheet manufacture or on the finished smoking article.
The invention particularly concerns making a moisture resistant tobacco product and includes or comprises forming a sheet of tobacco by mixing a major proportion by weight of finely divided tobacco With a minor proportion by weight of water soluble adhesive, such as a 3,185,162 Patented May 25, 1965 ice cellulose ether, e.g., ethyl hydroxyethyl cellulose, in aqueous solution and drying the sheet so formed. Thereafter the improvement consists of coating the surface of the dried sheet witha solution of ethyl cellulose and iinally drying the coating to produce a thin, flexible surface coating which protects the water soluble adhesive and the tobacco from attack and degradation by external moisture and is compatible with the smoking quality of the tobacco product. i
7 Example 0.5 part locust beam gum is added slowly, with agitation, to a 2.5% suspension of 1 part of highly refined sulfite pulp in water and agitation is continued until solution is complete. To the resulting dispersion is added, with stirring, 0.75 part diethylene glycol humectant, 0.5 part dialdehyde starch wet strength agent (as a 10% solution), 0.7 part diatomaceous earth and 6 parts tobacco dust (screen through mesh) which has been prewetted with water (1 part tobacco to 2 parts Water). Finally, 0.5 part ethyl hydroxyethyl cellulose adhesive are blended in carefully and the total solids adjusted to 10%. The resulting dispersion is cast on a moving stainless steel belt. The sheet on the belt is dried and then coated with an alcoholic solution of ethyl cellulose and the coating dried.
Since a coating which is hydrophilic will tend to remove moisture from the lips of a smoker and then cause a coated tobacco sheet wrapper to tend to stick to the lips as does a'cigarette paper, a hydrophobic coating on the sheet which may be used is ethyl-cellulose. This may be applied in either an alcoholic solution or as an aqueous emulsion.
What is claimed is:
In the process of making a moisture resistant tobacco product comprising the steps of:
(A) forming a sheet of tobacco by mixing a major proportion of finely divided tobacco by weight with a minor proportion by weight of water soluble adhesive in aqueous solution and (B) drying said sheet, the improvement consisting of the steps of (I) coating the surface of said dried sheet with a solution of ethyl cellulose, and (II) finally drying the coating on the sheet to produce a thin, flexible surface coating which (a) protects the water soluble adhesive and the tobacco from attack and degradation by external moisture and (b) is compatible with the smoking quality of the tobacco product.
References Cited by the Examiner UNITED STATES PATENTS 126,698 5/72 Harris 131-12 X 303,493 8/84 .Culp 131-12X 864,948 9/07 Butler 13112 1,338,827 5/20 Goodfellow 131-17 1,671,182 5/28 Eberlein 13l-12 1,750,835 3/30 Chamberlain 68244 2,158,565 5/39 Andrews 13l17 2,443,221 6/48 Burgstein 117--l58 X 2,613,672 10/52 Sartoretto et a1. 13117 2,613,673 10/52 Sartoretto et al. 131l7 2,708,175 5/55 Samfield et al 131-l7 2,734,509 2/ 56 lurgensen 131-17 2,734,510 2/56 Hungerford et a1. 13117 2,734,513 2/56 Hungerford et a1. 2,769,734 11/56 Handel 13l17 2,797,689 5/57 Frankenburg 13l--l7 (References on following page) 3 i o 4 Detert 131140 FOREIGN PATENTS samfield et a1 131--140 Ro e g e a fir-- 131*17 1,451 1882 Great Britain. Carmellini et a1 131 17 OTHER REFERENCES C0 1ton 131 140 5 The Condensed Chemical Dictionary, pages 28 and Phll -2 131-140 451; published 1956 by Reinhold Publishing Corp., New Howard 131-17 k 7 Rosenberg 131-140 Rosenbsrg et a 4 131 17 ABRAHAM G. STONE, Puma) Exammer. Detert eta1. 13117 10, F. RAY CHAPPELL, Examiner.
US73562A 1960-12-05 1960-12-05 Process for making reconstituted sheet tobacco Expired - Lifetime US3185162A (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
US73562A US3185162A (en) 1960-12-05 1960-12-05 Process for making reconstituted sheet tobacco
GB43074/61A GB940129A (en) 1960-12-05 1961-12-01 Tobacco manufacture
DK483461AA DK130134B (en) 1960-12-05 1961-12-04 Method for applying a water-repellent coating to at least one of the sides of an artificial tobacco leaf.
DE19611517287 DE1517287A1 (en) 1960-12-05 1961-12-05 Tobacco foil that has the same properties as a natural wrapper through a coating
CH1407161A CH437091A (en) 1960-12-05 1961-12-05 Artificial tobacco leaf and process for its manufacture
US404198A US3185161A (en) 1960-12-05 1964-09-09 Tobacco manufacture

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US73562A US3185162A (en) 1960-12-05 1960-12-05 Process for making reconstituted sheet tobacco

Publications (1)

Publication Number Publication Date
US3185162A true US3185162A (en) 1965-05-25

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Family Applications (1)

Application Number Title Priority Date Filing Date
US73562A Expired - Lifetime US3185162A (en) 1960-12-05 1960-12-05 Process for making reconstituted sheet tobacco

Country Status (5)

Country Link
US (1) US3185162A (en)
CH (1) CH437091A (en)
DE (1) DE1517287A1 (en)
DK (1) DK130134B (en)
GB (1) GB940129A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080006286A1 (en) * 2002-11-19 2008-01-10 John-Paul Mua Reconstituted Tobacco Sheet and Smoking Article Therefrom
US20080078417A1 (en) * 2002-11-19 2008-04-03 Wanna Joseph T Process for making a bandcast tobacco sheet and smoking article therefrom
US20130061861A1 (en) * 2010-03-23 2013-03-14 Alex Hearn Simulated cigarette
EP3263276A4 (en) * 2016-04-20 2018-12-05 China Tobacco Guizhou Industrial Co., Ltd. Method for manufacturing heat-not-burn tobacco substrate containing activated carbon

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4140135A (en) * 1975-12-29 1979-02-20 Gulf & Western Corporation Hydrophobic coating for tobacco sheet material
DE3224416C1 (en) * 1982-06-30 1984-03-15 Tamag Basel AG, 4127 Birsfelden Smokable, coherent film and process for its production

Citations (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US126698A (en) * 1872-05-14 Improvement
US303493A (en) * 1884-08-12 James daeius gulp
US864948A (en) * 1906-11-06 1907-09-03 George P Butler Art of manufacturing cigars and all-tobacco cigarettes.
US1338827A (en) * 1919-05-23 1920-05-04 Willard J Goodfellow Method of making cigar-wrappers
US1671182A (en) * 1926-11-11 1928-05-29 Frederick A Eberlein Cigar
US1750835A (en) * 1928-11-09 1930-03-18 Chamberlain Corp Wringer
US2158565A (en) * 1937-08-27 1939-05-16 Standard Commercial Tobacco Co Process for making harsh tobacco mild and the resultant product thereof
US2443221A (en) * 1944-08-14 1948-06-15 Robert Morris Bergstein Method of making grease- and moistureproof coated paperboard
US2613672A (en) * 1946-07-11 1952-10-14 Int Cigar Mach Co Tobacco sheet material and method of producing the same
US2613673A (en) * 1946-07-11 1952-10-14 Int Cigar Mach Co Tobacco sheet material and method of producing the same
US2708175A (en) * 1954-05-28 1955-05-10 Max M Samfield Composition of matter consisting chiefly of fragmented tobacco and galactomannan plant gum
US2734513A (en) * 1956-02-14 hungerford etal
US2734509A (en) * 1956-02-14 Wetting
US2734510A (en) * 1956-02-14 Preparing
US2769734A (en) * 1955-07-14 1956-11-06 Int Cigar Mach Co Tobacco sheet material and method of forming
US2797689A (en) * 1955-04-11 1957-07-02 Gen Cigar Co Tobacco products and process therefor
US2840085A (en) * 1955-09-28 1958-06-24 Eduard Gerlach G M B H Fa Cigar or the like and method of making the same
US2845933A (en) * 1954-05-28 1958-08-05 Liggett & Myers Tobacco Co Process of converting fragmented tobacco into coherent sheets
US2887414A (en) * 1958-03-06 1959-05-19 American Mach & Foundry Smoking product and method of manufacture
US2949117A (en) * 1959-04-06 1960-08-16 American Mach & Foundry Tobacco product
US2969794A (en) * 1958-04-14 1961-01-31 Raymond R Colton Tobacco processing
US2971517A (en) * 1958-06-30 1961-02-14 Arenco Ab Process for the preparation of an insoluble tobacco sheet or web
US3012915A (en) * 1957-11-21 1961-12-12 Minerals & Chem Philipp Corp Tobacco composition including comminuted solid material affixed thereto
US3016907A (en) * 1959-10-19 1962-01-16 Int Cigar Mach Co Manufacture of tobacco
US3042552A (en) * 1958-05-19 1962-07-03 American Mach & Foundry Tobacco products
US3062688A (en) * 1960-08-18 1962-11-06 Detert Ernst-Rolf Tobacco foils and methods of making the same

Patent Citations (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2734513A (en) * 1956-02-14 hungerford etal
US303493A (en) * 1884-08-12 James daeius gulp
US126698A (en) * 1872-05-14 Improvement
US2734510A (en) * 1956-02-14 Preparing
US2734509A (en) * 1956-02-14 Wetting
US864948A (en) * 1906-11-06 1907-09-03 George P Butler Art of manufacturing cigars and all-tobacco cigarettes.
US1338827A (en) * 1919-05-23 1920-05-04 Willard J Goodfellow Method of making cigar-wrappers
US1671182A (en) * 1926-11-11 1928-05-29 Frederick A Eberlein Cigar
US1750835A (en) * 1928-11-09 1930-03-18 Chamberlain Corp Wringer
US2158565A (en) * 1937-08-27 1939-05-16 Standard Commercial Tobacco Co Process for making harsh tobacco mild and the resultant product thereof
US2443221A (en) * 1944-08-14 1948-06-15 Robert Morris Bergstein Method of making grease- and moistureproof coated paperboard
US2613673A (en) * 1946-07-11 1952-10-14 Int Cigar Mach Co Tobacco sheet material and method of producing the same
US2613672A (en) * 1946-07-11 1952-10-14 Int Cigar Mach Co Tobacco sheet material and method of producing the same
US2708175A (en) * 1954-05-28 1955-05-10 Max M Samfield Composition of matter consisting chiefly of fragmented tobacco and galactomannan plant gum
US2845933A (en) * 1954-05-28 1958-08-05 Liggett & Myers Tobacco Co Process of converting fragmented tobacco into coherent sheets
US2797689A (en) * 1955-04-11 1957-07-02 Gen Cigar Co Tobacco products and process therefor
US2769734A (en) * 1955-07-14 1956-11-06 Int Cigar Mach Co Tobacco sheet material and method of forming
US2840085A (en) * 1955-09-28 1958-06-24 Eduard Gerlach G M B H Fa Cigar or the like and method of making the same
US3012915A (en) * 1957-11-21 1961-12-12 Minerals & Chem Philipp Corp Tobacco composition including comminuted solid material affixed thereto
US2887414A (en) * 1958-03-06 1959-05-19 American Mach & Foundry Smoking product and method of manufacture
US2969794A (en) * 1958-04-14 1961-01-31 Raymond R Colton Tobacco processing
US3042552A (en) * 1958-05-19 1962-07-03 American Mach & Foundry Tobacco products
US2971517A (en) * 1958-06-30 1961-02-14 Arenco Ab Process for the preparation of an insoluble tobacco sheet or web
US2949117A (en) * 1959-04-06 1960-08-16 American Mach & Foundry Tobacco product
US3016907A (en) * 1959-10-19 1962-01-16 Int Cigar Mach Co Manufacture of tobacco
US3062688A (en) * 1960-08-18 1962-11-06 Detert Ernst-Rolf Tobacco foils and methods of making the same

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080006286A1 (en) * 2002-11-19 2008-01-10 John-Paul Mua Reconstituted Tobacco Sheet and Smoking Article Therefrom
US20080078417A1 (en) * 2002-11-19 2008-04-03 Wanna Joseph T Process for making a bandcast tobacco sheet and smoking article therefrom
US8136533B2 (en) 2002-11-19 2012-03-20 R.J. Reynolds Tobacco Company Reconstituted tobacco sheet and smoking article therefrom
US20130061861A1 (en) * 2010-03-23 2013-03-14 Alex Hearn Simulated cigarette
US9693585B2 (en) 2010-03-23 2017-07-04 Kind Consumer Limited Simulated cigarette
US9763474B2 (en) * 2010-03-23 2017-09-19 Kind Consumer Limited Simulated cigarette
EP3263276A4 (en) * 2016-04-20 2018-12-05 China Tobacco Guizhou Industrial Co., Ltd. Method for manufacturing heat-not-burn tobacco substrate containing activated carbon

Also Published As

Publication number Publication date
CH437091A (en) 1967-05-31
DK130134B (en) 1974-12-30
GB940129A (en) 1963-10-23
DE1517287A1 (en) 1969-07-10
DK130134C (en) 1975-06-09

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