UA80781C2 - Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes - Google Patents

Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes Download PDF

Info

Publication number: UA80781C2
Authority: UA; Ukraine
Prior art keywords: gold; crystals; aqueous solution; ion; single crystals
Prior art date: 2006-03-23

Application number

UAA200603158A

Other languages

English (en)

Ukrainian (uk)

Inventor

Victorio Rafael Estrela-Liopys

Iryna Mykolaivna Yurkova

Tetiana Ivanivna Borodinova

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2006-03-23

Filing date

2006-03-23

Publication date

2007-10-25

2006-03-23 Application filed filed Critical

2006-03-23 Priority to UAA200603158A priority Critical patent/UA80781C2/uk

2007-03-19 Priority to RU2007110162/15A priority patent/RU2358042C2/ru

2007-10-25 Publication of UA80781C2 publication Critical patent/UA80781C2/uk

Links

238000000034 method Methods 0.000 title claims abstract description 50
229910000510 noble metal Inorganic materials 0.000 title claims abstract description 9
150000003839 salts Chemical class 0.000 title claims abstract description 6
238000002360 preparation method Methods 0.000 title description 2
239000013078 crystal Substances 0.000 claims abstract description 77
239000007864 aqueous solution Substances 0.000 claims abstract description 31
238000005286 illumination Methods 0.000 claims abstract description 14
239000003638 chemical reducing agent Substances 0.000 claims abstract description 11
229910001425 magnesium ion Inorganic materials 0.000 claims abstract description 10
238000006722 reduction reaction Methods 0.000 claims abstract description 7
229910052751 metal Inorganic materials 0.000 claims abstract description 6
239000002184 metal Substances 0.000 claims abstract description 6
229920000867 polyelectrolyte Polymers 0.000 claims abstract description 6
150000002500 ions Chemical class 0.000 claims abstract description 4
229920001448 anionic polyelectrolyte Polymers 0.000 claims description 5
229910021645 metal ion Inorganic materials 0.000 claims description 4
150000002736 metal compounds Chemical class 0.000 claims 1
238000012876 topography Methods 0.000 claims 1
230000015572 biosynthetic process Effects 0.000 abstract description 18
238000003786 synthesis reaction Methods 0.000 abstract description 11
-1 metals ions Chemical class 0.000 abstract description 7
150000001875 compounds Chemical class 0.000 abstract description 5
239000003814 drug Substances 0.000 abstract description 2
239000002086 nanomaterial Substances 0.000 abstract description 2
230000005693 optoelectronics Effects 0.000 abstract description 2
150000001450 anions Chemical class 0.000 abstract 1
229910052737 gold Inorganic materials 0.000 description 32
239000010931 gold Substances 0.000 description 32
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 31
229920001282 polysaccharide Polymers 0.000 description 17
239000005017 polysaccharide Substances 0.000 description 17
150000004676 glycans Chemical class 0.000 description 16
239000000243 solution Substances 0.000 description 16
239000006185 dispersion Substances 0.000 description 14
239000000203 mixture Substances 0.000 description 14
CLSUSRZJUQMOHH-UHFFFAOYSA-L platinum dichloride Chemical compound Cl[Pt]Cl CLSUSRZJUQMOHH-UHFFFAOYSA-L 0.000 description 11
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
239000002245 particle Substances 0.000 description 8
HZYWFQBABNUAAP-UHFFFAOYSA-N gold;hydrochloride Chemical compound Cl.[Au] HZYWFQBABNUAAP-UHFFFAOYSA-N 0.000 description 7
239000000126 substance Substances 0.000 description 6
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 5
244000005700 microbiome Species 0.000 description 5
239000002105 nanoparticle Substances 0.000 description 5
SSVFCHUBLIJAMI-UHFFFAOYSA-N platinum;hydrochloride Chemical compound Cl.[Pt] SSVFCHUBLIJAMI-UHFFFAOYSA-N 0.000 description 5
229910052709 silver Inorganic materials 0.000 description 5
239000004332 silver Substances 0.000 description 5
229920002125 Sokalan® Polymers 0.000 description 4
239000011651 chromium Substances 0.000 description 4
238000001000 micrograph Methods 0.000 description 4
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
239000000047 product Substances 0.000 description 4
241000894006 Bacteria Species 0.000 description 3
238000004630 atomic force microscopy Methods 0.000 description 3
239000003153 chemical reaction reagent Substances 0.000 description 3
238000001493 electron microscopy Methods 0.000 description 3
239000012535 impurity Substances 0.000 description 3
238000004452 microanalysis Methods 0.000 description 3
230000000813 microbial effect Effects 0.000 description 3
230000003287 optical effect Effects 0.000 description 3
239000004584 polyacrylic acid Substances 0.000 description 3
239000000523 sample Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
229920002307 Dextran Polymers 0.000 description 2
241000196324 Embryophyta Species 0.000 description 2
239000002253 acid Substances 0.000 description 2
230000001580 bacterial effect Effects 0.000 description 2
210000004027 cell Anatomy 0.000 description 2
CBGUOGMQLZIXBE-XGQKBEPLSA-N clobetasol propionate Chemical compound C1CC2=CC(=O)C=C[C@]2(C)[C@]2(F)[C@@H]1[C@@H]1C[C@H](C)[C@@](C(=O)CCl)(OC(=O)CC)[C@@]1(C)C[C@@H]2O CBGUOGMQLZIXBE-XGQKBEPLSA-N 0.000 description 2
229910052802 copper Inorganic materials 0.000 description 2
239000010949 copper Substances 0.000 description 2
238000000502 dialysis Methods 0.000 description 2
239000003937 drug carrier Substances 0.000 description 2
150000002632 lipids Chemical class 0.000 description 2
239000012528 membrane Substances 0.000 description 2
229940112877 olux Drugs 0.000 description 2
229910052697 platinum Inorganic materials 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
238000010561 standard procedure Methods 0.000 description 2
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
241000282326 Felis catus Species 0.000 description 1
235000010469 Glycine max Nutrition 0.000 description 1
244000068988 Glycine max Species 0.000 description 1
229920002845 Poly(methacrylic acid) Polymers 0.000 description 1
238000007792 addition Methods 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
235000013405 beer Nutrition 0.000 description 1
229920001222 biopolymer Polymers 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
210000000170 cell membrane Anatomy 0.000 description 1
210000002421 cell wall Anatomy 0.000 description 1
KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
229940061607 dibasic sodium phosphate Drugs 0.000 description 1
BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000002003 electron diffraction Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000001963 growth medium Substances 0.000 description 1
125000005843 halogen group Chemical group 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
230000003834 intracellular effect Effects 0.000 description 1
239000002502 liposome Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000011159 matrix material Substances 0.000 description 1
239000000155 melt Substances 0.000 description 1
238000001465 metallisation Methods 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000013081 microcrystal Substances 0.000 description 1
239000002159 nanocrystal Substances 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
238000010899 nucleation Methods 0.000 description 1
230000006911 nucleation Effects 0.000 description 1
238000000399 optical microscopy Methods 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 1
ACVYVLVWPXVTIT-UHFFFAOYSA-M phosphinate Chemical compound [O-][PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-M 0.000 description 1
229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
239000001267 polyvinylpyrrolidone Substances 0.000 description 1
235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000011084 recovery Methods 0.000 description 1
230000011514 reflex Effects 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
230000006641 stabilisation Effects 0.000 description 1
238000011105 stabilization Methods 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000000108 ultra-filtration Methods 0.000 description 1
238000005199 ultracentrifugation Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Crystallography & Structural Chemistry (AREA)
Materials Engineering (AREA)
Metallurgy (AREA)
Organic Chemistry (AREA)
Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Catalysts (AREA)
Crystals, And After-Treatments Of Crystals (AREA)

UAA200603158A 2006-03-23 2006-03-23 Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes UA80781C2 (en)

Priority Applications (2)

Application Number	Priority Date	Filing Date	Title
UAA200603158A UA80781C2 (en)	2006-03-23	2006-03-23	Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes
RU2007110162/15A RU2358042C2 (ru)	2006-03-23	2007-03-19	Способ получения монокристаллов благородного металла или его соли нано- и/или микроразмеров

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
UAA200603158A UA80781C2 (en)	2006-03-23	2006-03-23	Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes

Publications (1)

Publication Number	Publication Date
UA80781C2 true UA80781C2 (en)	2007-10-25

Family

ID=39016654

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
UAA200603158A UA80781C2 (en)	2006-03-23	2006-03-23	Process for preparation of monocrystals of noble metal or salt thereof of nano-and/or microsizes

Country Status (2)

Country	Link
RU (1)	RU2358042C2 (ru)
UA (1)	UA80781C2 (ru)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
RU2516153C2 (ru) *	2012-03-20	2014-05-20	Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Юго-Западный государственный университет" (ЮЗГУ)	Способ получения наночастиц золота из сырья, содержащего железо и цветные металлы
RU2566240C1 (ru) *	2014-04-25	2015-10-20	Федеральное государственное бюджетное учреждение науки Институт проблем химической физики Российской академии наук (ИПХФ РАН)	Способ получения наночастиц золота

2006
- 2006-03-23 UA UAA200603158A patent/UA80781C2/uk unknown
2007
- 2007-03-19 RU RU2007110162/15A patent/RU2358042C2/ru not_active IP Right Cessation

Also Published As

Publication number	Publication date
RU2358042C2 (ru)	2009-06-10
RU2007110162A (ru)	2008-09-27

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