UA109136C2 - method for growing single crystals of copper (I) hexathiophosphate Cu7PS6 - Google Patents

method for growing single crystals of copper (I) hexathiophosphate Cu7PS6

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Publication number
UA109136C2
UA109136C2 UAA201214055A UAA201214055A UA109136C2 UA 109136 C2 UA109136 C2 UA 109136C2 UA A201214055 A UAA201214055 A UA A201214055A UA A201214055 A UAA201214055 A UA A201214055A UA 109136 C2 UA109136 C2 UA 109136C2
Authority
UA
Ukraine
Prior art keywords
single crystals
copper
hexathiophosphate
cu7ps6
carried out
Prior art date
Application number
UAA201214055A
Other languages
Russian (ru)
Ukrainian (uk)
Inventor
Артем Ігорович Погодін
Олександр Павлович Кохан
Дмитро Володимирович Севрюков
Ігор Петрович Студеняк
Original Assignee
Державний Вищий Навчальний Заклад "Ужгородський Національний Університет"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Державний Вищий Навчальний Заклад "Ужгородський Національний Університет" filed Critical Державний Вищий Навчальний Заклад "Ужгородський Національний Університет"
Priority to UAA201214055A priority Critical patent/UA109136C2/en
Publication of UA109136C2 publication Critical patent/UA109136C2/en

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  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

This invention relates to inorganic chemistry and inorganic material science. A method for growing single crystals of copper (I) hexathiophosphate Cu7PS6 is claimed. The single crystals are grown by a method of directional crystallization from the melt, which includes stage heating of the vacuumized quartz vessels containing raw ingredients copper, phosphorus, sulfur in the desired stoichiometric ratio. The heating is carried out to a peak temperature and the vessels are held for 24 hours. The growth of single crystals is carried out at a maximum temperature of +1380 K at a rate of 3 mm/day in double beveled end ampoules. The proposed method allows to produce single crystals of large dimensions and can be realized using standard equipment.
UAA201214055A 2012-12-10 2012-12-10 method for growing single crystals of copper (I) hexathiophosphate Cu7PS6 UA109136C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
UAA201214055A UA109136C2 (en) 2012-12-10 2012-12-10 method for growing single crystals of copper (I) hexathiophosphate Cu7PS6

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
UAA201214055A UA109136C2 (en) 2012-12-10 2012-12-10 method for growing single crystals of copper (I) hexathiophosphate Cu7PS6

Publications (1)

Publication Number Publication Date
UA109136C2 true UA109136C2 (en) 2015-07-27

Family

ID=53721153

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA201214055A UA109136C2 (en) 2012-12-10 2012-12-10 method for growing single crystals of copper (I) hexathiophosphate Cu7PS6

Country Status (1)

Country Link
UA (1) UA109136C2 (en)

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