TWI262110B - Method of making porous structure - Google Patents

Method of making porous structure Download PDF

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Publication number
TWI262110B
TWI262110B TW094106550A TW94106550A TWI262110B TW I262110 B TWI262110 B TW I262110B TW 094106550 A TW094106550 A TW 094106550A TW 94106550 A TW94106550 A TW 94106550A TW I262110 B TWI262110 B TW I262110B
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TW
Taiwan
Prior art keywords
powder
porous structure
raw material
sintering
structure according
Prior art date
Application number
TW094106550A
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Chinese (zh)
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TW200631696A (en
Inventor
Chu-Wan Hong
Chang-Ting Lo
Ching-Tai Cheng
Jung-Yuan Wu
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Foxconn Tech Co Ltd
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Priority to TW094106550A priority Critical patent/TWI262110B/en
Priority to US11/306,061 priority patent/US20060198753A1/en
Publication of TW200631696A publication Critical patent/TW200631696A/en
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Publication of TWI262110B publication Critical patent/TWI262110B/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/10Sintering only
    • B22F3/1035Liquid phase sintering
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05Metallic powder characterised by the size or surface area of the particles
    • B22F1/052Metallic powder characterised by the size or surface area of the particles characterised by a mixture of particles of different sizes or by the particle size distribution
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/10Sintering only
    • B22F3/11Making porous workpieces or articles
    • B22F3/1103Making porous workpieces or articles with particular physical characteristics
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D15/00Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies
    • F28D15/02Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies in which the medium condenses and evaporates, e.g. heat pipes
    • F28D15/04Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies in which the medium condenses and evaporates, e.g. heat pipes with tubes having a capillary structure
    • F28D15/046Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies in which the medium condenses and evaporates, e.g. heat pipes with tubes having a capillary structure characterised by the material or the construction of the capillary structure

Abstract

A method of preparing powder for making a porous structure of predetermined capability by sintering. The preparing of the powder includes: separating an amount of raw powder into a number of groups according to particle size of the powder; selecting one or more groups of the separated powder to be sintered according to the predetermined capability of the porous structure.

Description

1262110 九、發明說明: 【發明所屬之技術領域】 本發明係關於—鮮孔賴的製造方法,尤係_ 結構之粉末的篩選方法。 【先前技術】 現階段,對於發熱錄高之電子辑,人們f遍採祕管、散軌 鰭片及散熱風扇結合之方式進行散熱。彻熱㈣部紐之 : 1 乍液體在發熱電子元件處(蒸發端)賴蒸發,向散熱鰭片移動,,,在 政熱韓片處(冷凝端)將發熱電子元件產生之熱量傳遞 利用散熱風扇將產生之熱量帶走,完成對電子元件之散埶。=後之 工作液體在冷凝微熱,凝軸,職财熱 ==回流至蒸發端,進人下_玉作循環。該熱管具有較高之;= 率和傳熱速度,在電子元件散熱領域發揮著重要作用。 ' 熱管之毛細結_影響熱管性能之重要因素,習知之熱管毛細结 構二般係贿末混合物放人高溫射燒結—段時間,使諸末連贴 形成。惟’該财法製造毛崎構時,由_粉末混合物含 夕種不同粒徑之粉末,且各粒徑範圍粉末之含量 (Surface Energy) , ^ 里不& ’進而使該粉末混合物燒結時所需之溫度範圍不明確,及 =個,度範圍停留之時·_定,令燒結溫度及燒結時間不易控 、_,、、ό/γ度過低或燒結時間過短,各粉末之間不能有效結合。若 3溫度過高錢結時間過長,該粉末混合物將產生钱、緻密化, 、:、4成之毛細結構内部僅存在少數不互相連通之較大孔隙,進而 ^毛細結構錢滿足高錢率及高毛細力之需求。故,業界希望尋 結溫纽燒結時間料控制之毛細結構。 本發明之目的係提供一種燒結溫度及燒結時間較易控制之多孔結 l262li〇 法:該方法係先篩分出不_徑大小之粉末,將該等粉末 ΐ 複數等份,再按照實際所需L«多個_ 多L*構。接燒結或按照—定比例搭配後燒結,以加工*滿足需求之 佔數製造多孔結構時,由於各等份粉末之粒徑大小及其所 時所:厶二:,燒結時所需減少之表面能較為明確,從而使燒結 守厅而之/皿度及日守間較易控制。 【實施方式】 下面參附圖結合貫施例對本發明作進一步說明。 用該毛細結構。利 4芩閱第一圖,該多孔結構的製造方法,包括如下步驟: 圍為原料包括複數粒徑大小不等之粉末,該等粉末之粒徑範 ^ ^ 粒徑範圍根據機械加卫精度之不。 中,原料之粒徑範圍為2〇至22〇篩目(Mesh)。“篩目” 孔的^目業界多用標準筛之筛目表示通過該標準筛 77 、;:徑大小。篩目越大,表示之粉末的粒徑越小。 數法篩取原料,使原料依次通過篩目相差較小之複 旱師’將不同粒叙粉末區分開來,並確定各粒徑之粉 所佔比例,得職原料各組份之正態分 二" π,次通過筛目由小到大之剛,搖動ί二:i 過,遠在師子上之粉末即為該標準篩所代表粒徑之粉末。’、 =區:請繼續參閱第二圖,根據所需加工熱管功率的大小及功率 數寺份。本貫施例中,將其分為a、b、c、d、e 广複 ^Mesh、140Mesh、100Mesh 及傷灿為區隔點使 a、^ =固,之粒徑範別為〜2纖esh、⑽〜2⑻驗 〇1262110 IX. DESCRIPTION OF THE INVENTION: TECHNICAL FIELD OF THE INVENTION The present invention relates to a method for producing fresh pores, and more particularly to a method for screening powders. [Prior Art] At this stage, for the electronic series of the high-temperature recording, people use the combination of the secret tube, the loose-angle fin and the cooling fan to dissipate heat. The heat (four) part of the New Zealand: 1 乍 liquid in the heating electronic components (evaporation end) depends on evaporation, moving to the heat sink fins, at the political hot Korean (condensing end) heat generated by the heating electronic components to use heat The fan takes away the heat generated and completes the divergence of the electronic components. = After the working liquid is in the condensation heat, the condensation axis, the occupational heat == reflux to the evaporation end, into the next _ jade cycle. The heat pipe has a high ratio; the rate and the heat transfer rate play an important role in the heat dissipation of electronic components. 'The thinness of the heat pipe _ is an important factor affecting the performance of the heat pipe. The conventional heat pipe capillary structure is the second type of bribe mixture that is placed in a high-temperature shot sintering period for a period of time. However, when the method of manufacturing the Mazaki structure, the powder mixture contains powders of different particle sizes, and the content of the powder in each particle size range (Surface Energy), ^ does not & 'and then the powder mixture is sintered. The required temperature range is not clear, and = one, the range of time stays _, so that the sintering temperature and sintering time are not easy to control, _,, ό / γ degree is too low or the sintering time is too short, between the powder Can not be effectively combined. If the temperature is too high and the carbonation time is too long, the powder mixture will produce money and densification, and: 40% of the capillary structure has only a few large pores that are not connected to each other, and then the capillary structure money satisfies the high money rate. And the demand for high capillary strength. Therefore, the industry hopes to find the capillary structure controlled by the temperature sintering time. The object of the present invention is to provide a porous junction l262li method which is easy to control in sintering temperature and sintering time: the method first screens out the powder of the size of the diameter, and the powder is aliquoted in plurals, and then according to actual needs. L« multiple _ multiple L* structure. Sintering or sintering according to the ratio of the ratio of the sintering to the processing of * to meet the demand of the production of the porous structure, due to the particle size of each aliquot of the powder and its time: 厶 2: the surface required to reduce the sintering Can be more clear, so that the sintering of the hall and the degree and the day is easier to control. [Embodiment] The present invention will be further described below with reference to the accompanying drawings. Use this capillary structure. Referring to the first figure, the method for manufacturing the porous structure comprises the following steps: the raw material comprises a plurality of powders having different particle sizes, and the particle size range of the powders is based on mechanical precision. Do not. The raw material has a particle size ranging from 2 Å to 22 Å mesh. The mesh of the "mesh" hole is mostly used in the standard sieve mesh to indicate the passage through the standard sieve 77;;: diameter. The larger the mesh size, the smaller the particle size of the powder. The method of screening the raw materials by the number method, so that the raw materials are successively passed through the re-grading divisions with small differences in mesh size, and the different granules are separated, and the proportion of the powders of each particle size is determined, and the normal components of the components of the raw materials are obtained. Two " π, the second pass through the mesh from small to large, shake ί 2: i too, the powder far from the division is the powder of the particle size represented by the standard sieve. ', = area: Please continue to refer to the second picture, according to the size and power of the heat pipe required to process the temple. In this example, it is divided into a, b, c, d, e, Guangfu ^Mesh, 140Mesh, 100Mesh, and wounded can be a compartmentalized point, a, ^ = solid, the particle size range is ~2 fiber Esh, (10) ~ 2 (8) test

Mesh、40〜100 Mesh、20〜40 Mesh。 140 選取··按照所需熱管功率的大小即所需毛細結構的 :將所選粉末按照4比例搭配。對於大功率熱管 透率及毛細力均較大讀末進行賊。對於小神熱管,可 7 1262110 後滲透率或毛細力相對較小之粉末。 燒結:將所選粉末進行焯4 ^ ^ ^ , 結構。 退仃燒〜,以形成滿足该熱管功率需求之毛細 本發明可選擇一個或多個等#p P 阿於古式R、Γ、n r , 寻,之叔末如廷擇C區粉末或β、0 〃 區粉末等。當選擇多個等份的粉末時,需按昭-定 比例進灯搭配。下面以選擇B、D區粉末4、2為例進^介^.·、疋 及徑範圍分別棒 _ B、D [i +彳致小與B祕末4妹軸比較大, 粉末堆::D弟Η:斤不’該B、D區粉末4、2混合時’ B區小粒徑 泰末堆積在D £大粒徑粉末 (Surface Energy)較大,1瞌从士 匕』祖仏物禾之表面月匕 溫产對於覃獨栋用η π、Γ 乂、、Ό日守所需減小之表面能較少,故,其燒結 時區於東4 粉末2之燒結溫度而言,相對較低。進行燒結 縮(NeCJng'並料了2溫度下即可將D 11粉末2連接在—起形成頸 、' 、’’失,同呀增加相鄰D區粉末2之頸部面積,在燒社後 6 ? 6 ° 2 ^ 二ΐ有較高之滲透力及毛細力,使該混合粉末較易在 較低服度下控峰結戦具魏高滲透力及毛細力之毛細結構。 上等份之粉末時,可在較低溫度下控制形成不同孔隙 ,使該毛細結構具有一定之毛細梯度,令該毛細結構 ’、、乂同透力及毛細力,有利於熱管性能之提高。 、聋接2單—等份之粉末時,各粉末在燒結過程中同樣會產生頸縮而 .、3八之'死"成之毛細結構的滲透力或毛細力與含有該等份粒徑粉 末之‘,相比有所下降,適合於較低功率之熱管。如第五及第六圖 d不為單獨選擇C區粉末燒結前後之示意圖,單獨選擇C區粉末燒 、M曼’在各粉末間形成一比第四圖孔隙6略大之孔隙6,,使燒結後形 成之毛細結構的毛細力與選擇B、D區粉末*、2形成之毛細結構的毛 細力相比有所下降。 >等份粉末之粒徑較大,燒結時所需之溫度較高,但由於 i等份粉末之粒徑大小及數量較為確定,使燒結時所需減少之表 面能較為明確,故,燒結時所需之溫度及時間仍較易控制。 1262110 確,從而使其燒έ士溫戶及吏ff時發生變化之粉末的表面能較為明 不同功率熱官之毛細結構時 ^錢相同或 使原料得到咖用,節省熱;=:末一不同的選擇, 把F ^例之原料係單一材料之粉末,本發明也可、把 料之妹’如選取銅,、獨鋼、m粉末。、取不同持 【圖式簡單說明】 ,一圖為本發明多孔結構製造方法之流程圖; Φ 第二圖為本發明原料各組份之正態分佈圖; 第三圖為本發明第一實施例燒結前之示意圖 第四圖為本發明第一實施例燒結後之示意圖 第五圖為本發明第二實施例燒結前之示意圖 第六圖為本發明第二實施例燒結後之示意圖 【主要元件符號說明】 〜Mesh, 40~100 Mesh, 20~40 Mesh. 140 Select · According to the required heat pipe power, that is, the required capillary structure: Match the selected powder in 4 scales. For the high-power heat pipe permeability and capillary force are relatively large, read the end of the thief. For the Xiaoshen heat pipe, the powder with a relatively small permeability or capillary force after 7 1262110 can be used. Sintering: The selected powder was subjected to 焯4 ^ ^ ^ , structure.仃 仃 , , , , , , , , , , , , 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本〃 Area powder, etc. When selecting multiple aliquots of powder, it is necessary to match the lamps in a proportional-to-scale ratio. In the following, the powders 4 and 2 in the B and D areas are selected as examples. The diameters of the rods are respectively _ B, D [i + 彳 小 小 小 小 B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B B D Η Η 斤 斤 斤 斤 斤 斤 斤 斤 斤 斤 斤 斤 斤 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该 该The surface temperature of the surface of the grass is less than that of the η π, Γ 乂, Ό Ό 所需 所需 所需 所需 所需 , , , , , , , , , , , , , , , , , , , 。 。 。 。 东 东 东 东 东 东 东 东 东Sintering shrinkage (NeCJng' can be combined with 2 temperatures to connect D 11 powder 2 to form a neck, ', '' lost, and increase the neck area of adjacent D powder 2, after burning 6 ? 6 ° 2 ^ Diterpenes have higher penetrating power and capillary force, making the mixed powder easier to control the capillary structure of Wei high permeability and capillary force under lower service. In the case of powder, it is possible to control the formation of different pores at a lower temperature, so that the capillary structure has a certain capillary gradient, so that the capillary structure', the same permeability and the capillary force are beneficial to the improvement of the performance of the heat pipe. In the case of a single-aliquot of powder, each powder will also be necked during the sintering process, and the 'dead' of the capillary structure or the capillary force of the capillary structure and the powder containing the particle size, Compared with the lower heat pipe, it is suitable for the lower power heat pipe. For example, the fifth and sixth graphs d are not separately selected before and after the sintering of the C zone powder, and the C zone powder is burned separately, and the Mman' is formed between the powders. a pore 6 which is slightly larger than the pores 6 of the fourth figure, so that the capillary structure formed after sintering The fine force is lower than the capillary force of the capillary structure formed by selecting the powders * and 2 in the B and D regions. > The particle size of the aliquot powder is larger, and the temperature required for sintering is higher, but due to the i aliquot The particle size and quantity of the powder are relatively certain, so that the surface energy required for sintering is relatively clear, so the temperature and time required for sintering are still relatively easy to control. 1262110 Indeed, so that it burns the gentleman and the 吏The surface energy of the powder that changes when ff is different. When the capillary structure of the power is different, the money is the same or the raw material is used for coffee, saving heat; =: the last different choice, the raw material of the F ^ example is a single material Powder, the invention can also be used as the material of the sister 'such as copper, single steel, m powder. Take different holdings [simple description of the drawing], a picture is a flow chart of the manufacturing method of the porous structure of the present invention; Φ second The figure is a normal distribution diagram of the components of the raw material of the present invention; the third diagram is a schematic diagram of the first embodiment of the present invention before sintering. The fourth diagram is a schematic diagram of the first embodiment of the present invention after sintering. Example 6 before the sintering Main reference numerals schematic DESCRIPTION - after sintering the second embodiment of the present invention embodiment

D區粉末 孔隙 2、B區粉末6、6, ' 4 9D area powder pores 2, B area powder 6,6, ' 4 9

Claims (1)

1262110 十、申請專利範圍: 1· 一種多孔結構的製造方法,包括如下步驟: 提供原料,該原料包括複數粒徑大小不等之粉末,該等粉末按照不同 之粒徑範圍劃分為複數等份; 選取,選取一個或多個等份之粉末; 燒結,將所選之粉末進行燒結,以加工所需之多孔結構。 2·如申請專利範圍第χ項所述之多孔結構的製造方法,其中該原料包括至 少一種材料之粉末。 3.如申請專利範圍第2項所述之多孔結構的製造方法,其中該原料為銅粉 或鎳粉或不銹鋼粉或陶瓷粉。 4·如申請專利範圍第丄項所述之多孔結構的製造方法,其中該提供原料之 步驟包括統計各粒徑大小之粉末在該原料中所佔比例。 5.如申請專利範圍第χ項所述之多孔結構的製造方法,其中該提供原料之 步驟中係按照所需加工之多孔結構的性能將該原料劃分為複數等份。 6·如申請專利範圍第1項所述之多孔結構的製造方法,其中該選取步驟 中,選取多個等份之粉末時,需按照一定的比例搭配。 7· —種多孔結構的製造方法,包括如下步驟: 原料’提供包括複數粒徑大小不等粉末之原料; 統計,統計該原料中各組份所佔比例; 分區’將該原料按照不同的粒徑範圍劃分為複數等份; 10 1262110 選取,選取一個或多個等份之粉末; 燒結,將所選之粉末進行燒結,以加工所需之多孔結構。 8. 如申請專利範圍第7項所述之多孔結構的製造方法,其中該統計步驟進 一步包括將原料按照不同的粒徑大小區分開來。 9. 如申請專利範圍第7項所述之多孔結構的製造方法,其中該選取步驟 中,選取多個等份之粉末時,需按照一定的比例搭配。 φ 10.如申請專利範圍第7項所述之多孔結構的製造方法,其中該提供原料之 步驟中係按照所需多孔結構的性能將該原料劃分為複數等份。1262110 X. Patent application scope: 1. A method for manufacturing a porous structure, comprising the steps of: providing a raw material comprising a plurality of powders having different particle sizes, and the powders are divided into plural equal parts according to different particle size ranges; Alternatively, one or more aliquots of the powder are selected; sintering, the selected powder is sintered to process the desired porous structure. 2. The method of producing a porous structure according to claim 2, wherein the raw material comprises a powder of at least one material. 3. The method of producing a porous structure according to claim 2, wherein the raw material is copper powder or nickel powder or stainless steel powder or ceramic powder. 4. The method of manufacturing a porous structure according to the above aspect of the invention, wherein the step of providing a raw material comprises counting the proportion of the powder of each particle size in the raw material. 5. The method of producing a porous structure according to the above aspect of the invention, wherein the step of providing the raw material is divided into plural aliquots according to the properties of the porous structure to be processed. 6. The method of manufacturing a porous structure according to claim 1, wherein in the selecting step, when a plurality of aliquots of the powder are selected, they are matched in a certain ratio. 7. A method for manufacturing a porous structure, comprising the steps of: the raw material 'providing a raw material comprising a plurality of powders of different particle sizes; counting and counting the proportion of each component in the raw material; partitioning the raw material according to different grains The diameter range is divided into a plurality of equal parts; 10 1262110 is selected, one or more aliquots of the powder are selected; sintering, the selected powder is sintered to process the desired porous structure. 8. The method of producing a porous structure according to claim 7, wherein the statistical step further comprises separating the raw materials according to different particle size sizes. 9. The method for producing a porous structure according to claim 7, wherein in the selecting step, when a plurality of aliquots of the powder are selected, they are matched in a certain ratio. Φ 10. The method for producing a porous structure according to claim 7, wherein the step of providing the raw material is divided into plural aliquots according to the properties of the desired porous structure.
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