TW201343596A

TW201343596A - Adjustable high yield manufacturing method for pitch and equipment thereof

Info

Publication number: TW201343596A
Application number: TW101114302A
Authority: TW
Inventors: Hsin-Ping Chang; Chuen-Ming Gee; Pai-Lu Wang; Yi-Cheng Cheng; Ching-Jang Lin; Ting-Yu Chang
Original assignee: Chung Shan Inst Of Science
Priority date: 2012-04-23
Filing date: 2012-04-23
Publication date: 2013-11-01

Abstract

The present invention relates to an adjustable high yield manufacturing method for pitch and equipment thereof, including: collecting vaporized low molecular weight pitch or vaporized gas in a thermal treatment procedure, and mixing it with the pitch that does not satisfy product specification and requirement from other processes to form another pitch solution. By this way, this invention can prepare a pitch product having pitch component with proper properties and satisfying the requirements of different specifications and promote pitch yield in the whole manufacturing procedure. Therefore, the manufacturing procedure of this invention can reduce the production of pitch waste, promote the pitch yield in the whole manufacturing procedure, sufficiently achieve the purpose of recycling and reusing resources, and reducing the production of pitch waste. The main purpose of the present invention is to obtain an adjustable high yield manufacturing method for pitch and the equipment thereof for collecting low molecular weight pitch and reduceing the production of pitch waste and the costs of the manufacturing procedure.

Description

一種可調式高產率瀝青之製作方法及其設備Method for preparing adjustable high-yield asphalt and equipment thereof

本發明特別著重操作便利、安全性高、節省能量、減少操作成本等優點的一種可調式高產率瀝青之製作方法及其設備。The invention particularly focuses on a method for manufacturing adjustable high-yield asphalt and an apparatus thereof, which are convenient to operate, high in safety, energy saving, and low in operating cost.

瀝青(pitch)原料來源豐富且價值低廉，為石油與煤化工業的副產物，其來源是石油精制殘渣油、石油渣油、煤渣油、煤瀝青及溶劑精製煤及一些純芳香烴(如萘、蔥)所構成，瀝青經過適當的純化或改質處理後，可提高芳香度和減少雜質、金屬離子和灰分後，亦可稱為精製瀝青(refined pitch)。由於瀝青擁有高碳化率及易石墨化特色，能使最終產物具有高模數、高導熱、高導電及低膨脹率性質，可廣泛應用於鋰電池負極、核反應電極、航太、軍武及運動器材與雷達的吸波材料上。Pitch raw materials are rich in source and low in value. They are by-products of the petroleum and coal chemical industries. The sources are petroleum refined residue oil, petroleum residue, coal residue oil, coal pitch and solvent refined coal and some pure aromatic hydrocarbons (such as naphthalene, It is composed of onion. After the asphalt is properly purified or modified, it can improve the aromaticity and reduce impurities, metal ions and ash. It can also be called refined pitch. Due to its high carbonization rate and easy graphitization, asphalt can make the final product have high modulus, high thermal conductivity, high conductivity and low expansion rate. It can be widely used in lithium battery anode, nuclear reaction electrode, aerospace, military and sports. Equipment and radar absorbing materials.

由於瀝青成分由多種環芳香烴所組成，在各分子的邊緣有不同形式之脂肪鍵、環烷烴和一些金屬、非金屬原子。當瀝青加熱到350℃以上，較弱的氫分子鍵會先被打斷，與低分子量成分同時被揮發排出外界，亦可以稱為熱裂解(heat cracking)反應。殘留下來的瀝青以一定型式鍵結成更大更穩定的縮合芳香烴，各種脂肪族化合物會逐漸芳香化和聚合為芳香烴或環烷烴大分子，亦可以稱為熱縮聚(heat polymerization)反應。同時大分子會聚合為另一種新相，在表面張力作用之下形成介相球體(mesophase sphere)。Since the asphalt component is composed of a plurality of cyclic aromatic hydrocarbons, there are different forms of aliphatic bonds, cycloalkanes, and some metal and non-metal atoms at the edges of each molecule. When the asphalt is heated above 350 ° C, the weak hydrogen molecular bonds are first broken, and the low molecular weight components are simultaneously volatilized out of the outside, which may also be called a heat cracking reaction. The remaining bitumen is bonded to a larger and more stable condensed aromatic hydrocarbon in a certain type, and various aliphatic compounds are gradually aromatized and polymerized into an aromatic hydrocarbon or a cycloalkane macromolecule, which may also be referred to as a heat polymerization reaction. At the same time, the macromolecules will polymerize into another new phase, forming a mesophase sphere under the action of surface tension.

當瀝青軟化點愈高時，瀝青成型溫度勢必得比軟化點更高，使得後端加工變得更加不易。同時過高的成型溫度不但可能使瀝青再次熱縮聚成固態游離碳，同時裂解出揮發氣體存在於加工成型的產品內，形成氣泡或裂紋。因此調整瀝青軟化點到適當的黏度，儘可能呈現非觸變特性，同時如何有效地抑制或降低熱處理後中高分子量成分，使得瀝青軟化點達到適當的範圍，將是成為高品質瀝青關鍵條件之一，如何提高整體製程產率，勢必可以降低運轉成本費用，最終增加改質瀝青的附加價值。When the softening point of the asphalt is higher, the asphalt forming temperature tends to be higher than the softening point, making the back end processing more difficult. At the same time, too high molding temperature may not only cause the asphalt to be thermally polycondensed into solid free carbon, but also the volatile gas is cracked in the processed product to form bubbles or cracks. Therefore, adjusting the softening point of the asphalt to the appropriate viscosity, and exhibiting non-thixotropic characteristics as much as possible, and how to effectively suppress or reduce the medium and high molecular weight components after heat treatment, so that the softening point of the asphalt reaches an appropriate range, it will become one of the key conditions for high quality asphalt. How to improve the overall process yield, it is bound to reduce operating costs, and ultimately increase the added value of modified asphalt.

一般習知瀝青改質的製作方法，例如美國發明專利US7220348，實施例是將蒸餾器(vaporizer)上層之揮發產品(volatile product)或上層輕成分(overhead lighter)回收後，經由風扇冷卻後，再導入到熱分離筒槽(hot separator vessel)，再將低分子量瀝青排除，該製程回收過熱蒸氣(superheated steam)繼續後端使用。美國發明專利US7318891，實施例是將筒槽(vessel)上層之蒸氣(低分子量瀝青)，經過加熱器與風扇冷卻器後，回收到上層容器(overhead receiver)後儲存再使用。上述美國發明專利US7220348與US7318891的實施例，熱處理製程內所產生的低分子量，都沒有回收再導入原來製程內，用以增加整體製程瀝青的產率，以及瀝青並沒有透過混合方法達到最佳條件。美國發明專利US4231857將蒸氣與催化分餾時所分別得到之副產物予以混合，得到比單一原料較好之性質。美國發明專利US6350637將高碳產率瀝青與一種芳香族溶劑混合來降低軟化點。上述美國發明專利US4231857與US6350637的實施例，使用兩種不同來源的瀝青進行混合達到改質效果，以及沒有考慮改質瀝青的產率。A conventional method for producing a modified asphalt, for example, U.S. Patent No. 7,220,348, in which the volatile product or the overhead lighter of the upper layer of the vaporizer is recovered, cooled by a fan, and then cooled. It is introduced into a hot separator vessel and the low molecular weight bitumen is removed. The process recovers superheated steam and continues to be used at the back end. U.S. Patent No. 7,318,891, in which the vapor (low molecular weight bitumen) of the upper layer of the vessel is passed through a heater and a fan cooler, recovered to an overhead receiver, and stored for use. In the examples of the above-mentioned U.S. Patent Nos. 7,220,348 and 7,311,891, the low molecular weight produced in the heat treatment process is not recovered and introduced into the original process to increase the yield of the overall process asphalt, and the asphalt is not optimally mixed by the mixing method. . U.S. Patent No. 4,231,857 combines vapors with by-products obtained separately during catalytic fractionation to provide better properties than a single feedstock. U.S. Patent No. 6,350,637 combines high carbon yield bitumen with an aromatic solvent to reduce the softening point. Examples of the above-mentioned U.S. Patent Nos. 4,231,857 and 6,350,637, each of which uses two different sources of bitumen for mixing to achieve a upgrading effect, and which does not consider the yield of the modified bitumen.

本發明是回收熱處理製程中所揮發出去低分子量瀝青或揮發氣體，再加入欲改質的瀝青內，用以調整出適當性質的瀝青，滿足各種不同規格要求之瀝青產品，同時提升整體製程瀝青產率。有鑑於此，本發明係為一種操作便利、安全性高、節省能量、減少操作成本等優點的一種可調式高產率瀝青之製作方法及其設備。The invention recovers the low molecular weight bitumen or volatile gas which is volatilized in the heat treatment process, and then adds it to the bitumen to be modified to adjust the asphalt of suitable nature, meets the asphalt products of various specifications, and improves the overall process asphalt production. rate. In view of this, the present invention is a method and a device for manufacturing an adjustable high-yield asphalt which are convenient in operation, high in safety, energy saving, and low in operating cost.

鑒於上述習知技術之缺點，本發明之主要目的是回收熱處理製程所揮發的低分子量瀝青或揮發氣體，依照一定比例加入欲改質的瀝青內，用以調整出適當性質的瀝青，滿足各種不同規格要求之瀝青產品，同時亦可以提升整體製程瀝青之產率。本發明係以提供一瀝青粉末，將惰性氣體(氮氣與氬氣)加入熱處理裝置內，主要目的是為了保護瀝青在熱處理製程中，避免與外界空氣接觸而形成氧化交聯反應。並提供一氣氛壓力於瀝青溶液內並進行加熱攪拌處理，收集熱處理製程所揮發的低分子量瀝青或揮發氣體。量測熱處理製程內一瀝青溶液之成分性質，針對其瀝青性質，添加不同比例之回收低分子量瀝青於欲改質的瀝青內，量測並判斷是否符合產品規格與需求，若是的話，便成為最終瀝青產品，若不是的話，迴流到製程前端再進行加熱攪拌處理製程。本發明製程是回收熱處理製程中所揮發之低分子量瀝青或揮發氣體，並可提升整體製程瀝青產率，另藉由回收低分子量瀝青調整欲改質的瀝青性質，以滿足各種不同規格要求之瀝青產品。同時提升整體製程瀝青產率。In view of the above disadvantages of the prior art, the main object of the present invention is to recover the low molecular weight bitumen or volatile gas volatilized by the heat treatment process, and add it to the bitumen to be modified according to a certain ratio, in order to adjust the asphalt of appropriate properties to meet various differences. Asphalt products with specifications can also increase the yield of the overall process asphalt. The invention provides an asphalt powder, and an inert gas (nitrogen and argon) is added into the heat treatment device, and the main purpose is to protect the asphalt from the contact with the outside air to form an oxidative crosslinking reaction during the heat treatment process. An atmosphere pressure is applied to the asphalt solution and heated and agitated to collect low molecular weight bitumen or volatile gas volatilized by the heat treatment process. Measure the composition properties of a bitumen solution in the heat treatment process, add different proportions of recycled low molecular weight bitumen to the bitumen to be modified, measure and judge whether it meets the product specifications and requirements, and if so, become the final The asphalt product, if not, is returned to the front end of the process and then heated and agitated. The process of the invention recovers the low molecular weight bitumen or volatile gas volatilized in the heat treatment process, and can improve the overall process asphalt yield, and adjusts the asphalt property to be modified by recovering the low molecular weight asphalt to meet various specifications of the asphalt. product. At the same time, the overall process asphalt yield is improved.

本發明主要目的是得到一種可調式高產率瀝青之製作方法及其設備，回收低分子量瀝青再加以利用，避免廢棄物排放與後續處理問題。The main object of the present invention is to obtain a method and a device for preparing a high-yield asphalt with adjustable high-yield asphalt, and then recycling the low-molecular-weight asphalt to avoid waste discharge and subsequent treatment problems.

本發明提供一種可調式高產率瀝青之製作方法及其設備，創造更高的瀝青產率與滿足不同規格之瀝青產品，同時達到瀝青揮發物再度回收利用的效益，可以運用於人工石墨與碳/碳複合材料之黏著劑、人工石墨與碳/碳複合材料之浸滲材料與碳纖維前端材料等碳材料領域。為了讓熟悉該項技術人員能夠詳細地瞭解本發明之宗旨、目的、特徵及功能，茲藉由下述最佳具體實施例來加以說明。The invention provides an adjustable high-yield asphalt production method and equipment thereof, which can create higher asphalt yield and meet different specifications of asphalt products, and at the same time achieve the benefits of re-recycling of asphalt volatiles, and can be applied to artificial graphite and carbon/ Adhesives for carbon composites, impregnated materials for artificial graphite and carbon/carbon composites, and carbon fiber front-end materials. The objectives, objects, features, and functions of the present invention will be described in detail in the claims.

以上之概述與接下來的詳細說明及附圖，皆是為了能進一步說明本發明達到預定目的所採取的方式、手段及功效。而有關本發明的其他目的及優點，將在後續的說明及圖示中加以闡述。The above summary, the following detailed description and the accompanying drawings are intended to further illustrate the manner, the Other objects and advantages of the present invention will be described in the following description and drawings.

以下係藉由特定的具體實例說明本創作之實施方式，熟悉此技藝之人士可由本說明書所揭示之內容輕易地瞭解本發明之其他優點與功效。The embodiments of the present invention are described below by way of specific examples, and those skilled in the art can readily appreciate other advantages and effects of the present invention from the disclosure herein.

請參考第1圖及第2圖，係分別為本發明一種可調式高產率瀝青之製作方法流程示意圖及本發明一種可調式高產率瀝青之製作設備實施例示意圖。Please refer to FIG. 1 and FIG. 2 , which are respectively a schematic diagram of a process for preparing a tunable high-yield asphalt according to the present invention and a schematic diagram of an embodiment of a tunable high-yield asphalt production apparatus according to the present invention.

如第1圖所示，本發明為一種可調式高產率瀝青之製作方法，步驟(a)提供一瀝青粉末s11。步驟(b)提供一氣氛壓力於一瀝青溶液中並進行加熱攪拌處理s12，氣氛主要目的是為了保護瀝青在熱處理製程中，避免與外界空氣接觸而形成氧化交聯反應，其中氣氛可以是氮氣、氬氣氣源或其組合，一氣氛壓力控制在0.1~15 atm、最佳氣氛壓力控制在1~10 atm，該溫度控制在250~500℃，最佳的溫度控制在300~450℃，攪拌時間控制在0.5~10小時，最佳攪拌時間在1~8小時，攪拌速度控制在0~1000轉/分，其最佳攪拌速度在60~500轉/分。使得瀝青由固體(常溫狀態)熔融成液體(超過軟化點的狀態)並且持續加熱攪拌製程，步驟(c)收集熱處理製程所揮發的低分子量瀝青s13或揮發氣體。步驟(d)量測一瀝青溶液之成分性質s14，得知熱處理後瀝青之軟化點(SP)性質。步驟(e)添加不同比例之步驟(h)副產品s18回收低分子量瀝青，混合成一瀝青溶液s15。步驟(f)是判斷是否符合產品規格與需求，改質瀝青性質符合軟化點範圍在70~180℃與最佳軟化點在90~130℃，步驟(g)最終瀝青產品，若無法符合上述規格時，迴流到步驟(b)，進行加熱攪拌處理製程。As shown in Fig. 1, the present invention is a process for producing a tunable high-yield pitch, and step (a) provides an asphalt powder s11. Step (b) provides an atmosphere pressure in a bitumen solution and performs a heating and agitation treatment s12. The main purpose of the atmosphere is to protect the bitumen during the heat treatment process, avoiding contact with outside air to form an oxidative cross-linking reaction, wherein the atmosphere may be nitrogen, Argon gas source or a combination thereof, an atmosphere pressure is controlled at 0.1~15 atm, the optimal atmosphere pressure is controlled at 1~10 atm, the temperature is controlled at 250~500 °C, and the optimal temperature is controlled at 300~450 °C, stirring The time is controlled at 0.5~10 hours, the optimal stirring time is 1~8 hours, the stirring speed is controlled at 0~1000 rpm, and the optimal stirring speed is 60~500 rpm. The pitch is melted from a solid (normal temperature state) into a liquid (a state exceeding a softening point) and the heating and agitating process is continued, and the step (c) collects the low molecular weight asphalt s13 or a volatile gas volatilized by the heat treatment process. Step (d) measures the compositional property s14 of a bituminous solution, and knows the softening point (SP) property of the bitumen after heat treatment. Step (e) adding a different ratio of step (h) by-product s18 to recover the low molecular weight bitumen and mixing into a bituminous solution s15. Step (f) is to determine whether the product specifications and requirements are met. The modified asphalt properties meet the softening point range of 70-180 ° C and the optimum softening point is 90-130 ° C. Step (g) final asphalt product, if the above specifications are not met At the time, it is refluxed to the step (b) to carry out a heating and agitation treatment process.

如第2圖所示，本發明為一種可調式高產率瀝青之製作設備，一種可調式高產率瀝青之製作設備，該設備包括：一爐體23；一供料單元21，係與該爐體連通，提供過程中所需原料；一供氣單元22，係與該爐體23連通，提供過程中所需氣體；一回收單元24，係與該爐體23及混合單元26連通，提供過程中回收容器並提供混合單元26所需之原料；複數個檢測單元25，係與該爐體23及混合單元26連通，檢測該項產品參數；混合單元26，係與該檢測單元A25及回收單元24連通，調整混合其產品參數；複數個流量控制單元，係控制該設備間之流量管控；一收集單元28，係與該檢測單元B27連通收集完成品，提供一容器收集完成品。As shown in FIG. 2, the present invention is an adjustable high-yield asphalt production equipment, an adjustable high-yield asphalt production apparatus, the apparatus comprising: a furnace body 23; a feeding unit 21, and the furnace body Connected to provide the raw materials required in the process; a gas supply unit 22 is connected to the furnace body 23 to provide the gas required in the process; a recovery unit 24 is connected to the furnace body 23 and the mixing unit 26, and is provided in the process. Recovering the container and providing the raw materials required for the mixing unit 26; a plurality of detecting units 25 are connected to the furnace body 23 and the mixing unit 26 to detect the product parameters; the mixing unit 26 is connected to the detecting unit A25 and the recycling unit 24 Connected, adjust and mix its product parameters; a plurality of flow control units control flow control between the devices; a collection unit 28 is connected with the detection unit B27 to collect finished products, and provides a container for collecting finished products.

本發明製程可有效回收熱處理製程中所揮發之低分子量瀝青，並可提升整體製程瀝青產率，另藉由回收揮發之低分子量瀝青調整欲改質瀝青的成分與性質，以滿足各種不同規格要求之瀝青產品。The process of the invention can effectively recover the low molecular weight bitumen volatilized in the heat treatment process, and can improve the overall process asphalt yield, and adjust the composition and properties of the modified bitumen by recovering the volatilized low molecular weight bitumen to meet various specifications. Asphalt products.

本發明研製的一種可調式高產率瀝青經由上述步驟處理後，如下表所示。A tunable high-yield bitumen developed by the present invention is processed as described in the following table.

編號1與編號5分別是欲改質瀝青與低分子量瀝青的軟化點約144℃與65℃，編號2到編號4分別添加10%、30%、50%的低分子量瀝青於欲改質瀝青內，量測到軟點約132.9℃、114.8℃與105.6℃，證實不同比例低分子量瀝青加入欲改質瀝青，可以達到瀝青軟化點調整的功能，以滿足各種不同規格要求之瀝青產品。No. 1 and No. 5 are respectively softening points of modified asphalt and low molecular weight asphalt of about 144 ° C and 65 ° C, and No. 2 to No. 4 are respectively added with 10%, 30%, 50% of low molecular weight asphalt in the modified asphalt. The measured soft points are about 132.9 ° C, 114.8 ° C and 105.6 ° C. It is confirmed that different proportions of low molecular weight asphalt are added to the modified asphalt, and the function of adjusting the softening point of the asphalt can be achieved to meet various asphalt products with different specifications.

本發明乃是一種可調式高產率瀝青之製作方法及其設備，為一種調整熱處理後瀝青性質與高產率之製作說明，亦可用其它之特定方法來實現，皆不脫離本發明之特點與精神所在。上述之實施例僅為例示性說明本創作之特點及其功效，而非用於限制本發明之實質技術內容的範圍，任何熟習此技藝之人士均可在不違背本發明之精神及範疇下，對上述實施例進行修飾與變化。因此，本發明之權利保護範圍，應如後述之申請專利範圍所列。The invention relates to a preparation method and equipment for adjustable high-yield asphalt, which is a production description for adjusting the properties and high yield of asphalt after heat treatment, and can also be realized by other specific methods without departing from the characteristics and spirit of the invention. . The above-described embodiments are merely illustrative of the features and functions of the present invention, and are not intended to limit the scope of the technical scope of the present invention, and those skilled in the art can do without departing from the spirit and scope of the present invention. Modifications and variations of the above embodiments are made. Therefore, the scope of protection of the present invention should be as set forth in the scope of the claims described below.

1．．．製造流程1. . . Manufacturing process

s11、s12、s13、s14、s15、s16、s17、s18．．．一種可調式高產率瀝青之製作方法流程S11, s12, s13, s14, s15, s16, s17, s18. . . Process for producing adjustable high-yield asphalt

21．．．供料單元twenty one. . . Feed unit

22．．．供氣單元twenty two. . . Gas supply unit

23．．．爐體twenty three. . . Furnace body

24．．．回收單元twenty four. . . Recycling unit

25．．．檢測單元A25. . . Detection unit A

26．．．混合單元26. . . Mixing unit

27．．．檢測單元B27. . . Detection unit B

28．．．收集單元28. . . Collection unit

a-e．．．流量控制單元A-e. . . Flow control unit

第1圖：本發明一種可調式高產率瀝青之製作方法流程示意圖。Fig. 1 is a schematic view showing the flow of a method for producing an adjustable high-yield asphalt according to the present invention.

第2圖：本發明一種可調式高產率瀝青之製作設備實施例示意圖。Fig. 2 is a schematic view showing an embodiment of a manufacturing apparatus for adjustable high-yield asphalt according to the present invention.

1．．．製造流程1. . . Manufacturing process

Claims

一種可調式高產率瀝青之製作方法，該方法包括：(a)　提供一瀝青粉末；(b)　提供氣氛壓力於瀝青溶液中並進行加熱攪拌處理；(c)　收集熱處理製程所揮發的低分子量瀝青進入步驟(h)，其餘瀝青進入步驟(d)；(d)　量測一瀝青溶液之成分性質；(e)　添加不同比例之步驟(h)副產品，混合成一調整瀝青溶液；(f)　判斷步驟(e)的瀝青是否符合產品規格與需求，是，則進入步驟(g)，不是，則是回到步驟(b)；(g)　完成最終瀝青產品；(h)　產生副產品。A method for preparing a tunable high-yield asphalt, the method comprising: (a) providing a bituminous powder; (b) providing an atmosphere pressure in the bitumen solution and performing a heating and agitation treatment; and (c) collecting the low molecular weight bitumen volatilized by the heat treatment process Going to step (h), the remaining bitumen enters step (d); (d) measuring the compositional properties of a bitumen solution; (e) adding a different proportion of the step (h) by-products, mixing into an adjusted bitumen solution; (f) judging step (e) Whether the asphalt meets the product specifications and requirements, if yes, proceed to step (g), if not, return to step (b); (g) complete the final asphalt product; (h) produce by-products.

如申請專利範圍第1項所述一種可調式高產率瀝青之製作方法，其中，該瀝青粉末包括煤焦油、煤焦瀝青、石油瀝青、石油分餾之重質油、軟瀝青、柏油其中之一或其混合物。The method for preparing a tunable high-yield asphalt according to the first aspect of the invention, wherein the asphalt powder comprises one of coal tar, coal tar pitch, petroleum pitch, petroleum fractionated heavy oil, soft asphalt, tar or Its mixture.

如申請專利範圍第1項所述一種可調式高產率瀝青之製作方法，其中，該氣氛壓力控制在0.1~15 atm，最佳氣氛壓力控制在1~10 atm。The method for manufacturing an adjustable high-yield asphalt according to claim 1, wherein the atmosphere pressure is controlled at 0.1 to 15 atm, and the optimal atmosphere pressure is controlled at 1 to 10 atm.

如申請專利範圍第1項所述一種可調式高產率瀝青之製作方法，其中，該氣氛可以是氮氣、氬氣氣源或其組合。The method for producing a tunable high-yield asphalt according to the first aspect of the invention, wherein the atmosphere may be a nitrogen gas, an argon gas source or a combination thereof.

如申請專利範圍第1項所述一種可調式高產率瀝青之製作方法，其中，該加熱攪拌處理係包含一控制溫度、一控制時間及一攪拌速度。The method for producing an adjustable high-yield asphalt according to the first aspect of the invention, wherein the heating and agitating treatment comprises a control temperature, a control time and a stirring speed.

如申請專利範圍第5項所述一種可調式高產率瀝青之製作方法，其中，該控制溫度在250~550℃，最佳的溫度控制在300~450℃。The method for manufacturing an adjustable high-yield asphalt according to claim 5, wherein the control temperature is 250 to 550 ° C, and the optimal temperature is controlled at 300 to 450 ° C.

如申請專利範圍第5項所述一種可調式高產率瀝青之製作方法，其中，該控制時間在0.5~10小時，最佳攪拌時間控制在1~8小時。The method for manufacturing an adjustable high-yield asphalt according to the fifth aspect of the invention, wherein the control time is 0.5 to 10 hours, and the optimal stirring time is controlled within 1 to 8 hours.

如申請專利範圍第5項所述一種可調式高產率瀝青之製作方法，其中，該攪拌速度在0~1000轉/分，最佳攪拌速度控制在100~500轉/分。The method for manufacturing an adjustable high-yield asphalt according to claim 5, wherein the stirring speed is 0 to 1000 rpm, and the optimal stirring speed is controlled at 100 to 500 rpm.

如申請專利範圍第1項所述一種可調式高產率瀝青之製作方法，其中，該判斷是否符合產品規格與需求，改質瀝青性質符合甲苯不溶物及軟化點溫度等特點。The method for preparing an adjustable high-yield asphalt according to the first aspect of the patent application, wherein the determining whether the product meets the product specifications and requirements, and the modified asphalt property conforms to the characteristics of toluene insoluble matter and softening point temperature.

如申請專利範圍第9項所述一種可調式高產率瀝青之製作方法，其中，該甲苯不溶物設定在20~80 wt%，最佳甲苯不溶物在30~70 wt%。The method for preparing a tunable high-yield asphalt according to claim 9, wherein the toluene-insoluble matter is set at 20 to 80 wt%, and the optimum toluene-insoluble matter is at 30 to 70 wt%.

如申請專利範圍第9項所述一種可調式高產率瀝青之製作方法，其中，該軟化點溫度設定在70~200℃，最佳軟化點在90~150℃。The method for preparing an adjustable high-yield asphalt according to claim 9, wherein the softening point temperature is set at 70 to 200 ° C, and the optimum softening point is 90 to 150 ° C.

一種可調式高產率瀝青之製作設備，該設備包括：一爐體；一供料單元，係與該爐體連通，提供過程中所需原料；一供氣單元，係與該爐體連通，提供過程中所需氣體；一回收單元，係與該爐體及混合單元連通，提供過程中回收容器並提供混合單元所需之原料；複數個檢測單元，係與該爐體及混合單元連通，檢測該項產品參數；混合單元，係與該檢測單元及回收單元連通，調整混合其產品參數；複數個流量控制單元，係控制該設備間之流量管控；一收集單元，係與該檢測單元連通收集完成品，提供一容器收集完成品。An adjustable high-yield asphalt production equipment, the equipment comprising: a furnace body; a feeding unit connected to the furnace body to provide raw materials required in the process; and a gas supply unit connected to the furnace body to provide a gas required in the process; a recovery unit is connected to the furnace body and the mixing unit to provide a process for recovering the container and providing the raw materials required for the mixing unit; and a plurality of detecting units connected to the furnace body and the mixing unit for detecting The product parameter; the mixing unit is connected with the detecting unit and the recycling unit to adjust and mix the product parameters; the plurality of flow control units control the flow control between the devices; and a collecting unit is connected with the detecting unit to collect Finished product, providing a container to collect finished products.

如申請專利範圍第12項所述一種可調式高產率瀝青之製作設備，其中，該爐體為不銹鋼、高英鎳、高碳鋼或其組合。The apparatus for manufacturing a tunable high-yield asphalt according to the invention of claim 12, wherein the furnace body is stainless steel, high-nickel nickel, high carbon steel or a combination thereof.

如申請專利範圍第12項所述一種可調式高產率瀝青之製作設備，其中，該檢測單元係包含量測元件、判斷元件及顯示元件。The apparatus for manufacturing an adjustable high-yield asphalt according to claim 12, wherein the detecting unit comprises a measuring component, a determining component and a display component.

如申請專利範圍第12項所述一種可調式高產率瀝青之製作設備，其中，該爐體係包含加熱元件及攪拌元件。The apparatus for manufacturing an adjustable high-yield asphalt according to the invention of claim 12, wherein the furnace system comprises a heating element and a stirring element.

如申請專利範圍第12項所述一種可調式高產率瀝青之製作設備，其中，該爐體更進一步包含一控制器，該控制器係具有控制溫度、攪拌時間或其組合之群組。The apparatus for manufacturing an adjustable high-yield asphalt according to claim 12, wherein the furnace further comprises a controller having a group of controlling temperature, stirring time, or a combination thereof.

如申請專利範圍第16項所述一種可調式高產率瀝青之製作設備，其中，該控制器係控制供氣單元及供料單元流通量。The apparatus for manufacturing an adjustable high-yield asphalt according to claim 16, wherein the controller controls the flow of the gas supply unit and the supply unit.