SU576923A3 - Способ получени имидокарбонатных производных - Google Patents
Способ получени имидокарбонатных производныхInfo
- Publication number
- SU576923A3 SU576923A3 SU721851051A SU1851051A SU576923A3 SU 576923 A3 SU576923 A3 SU 576923A3 SU 721851051 A SU721851051 A SU 721851051A SU 1851051 A SU1851051 A SU 1851051A SU 576923 A3 SU576923 A3 SU 576923A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- imidocarbonate
- derivatives
- preparing
- solution
- mol
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Description
Раствор 5,6 г (0,1 мол ) гидроокиси в 100мл метанола перемешивают при 15°С с 25,1 г (0,1 мол ) S - (4 - метилциклогексил) - f - (3 -пиридил ) тйонокарбамата до образовани гомоген ного раствора. В этот раствор по капл м добавл ют при 15-20°С 22,7 г (0,1 мол ) п трет бутилбензилбромида . Полученный раствор выдерживают при 25° С в течение 3 ч и затем реакщюную смесь выливают в 400 мл охлажденной на льду воды.
Вьшавшее масл нистое вещество экстрагируют 200 мл этилацетата. Экстракт промывают один раз 200 мл воды и сушат над безводным сульфатом натри . Затем растворитель отгон ют в вакууме и получают 33,9 г светло-желтого масл нистого соединени , выход 85,5%.
Аналогично примеру 1 можно получить указанные в таблице соединени .
J NV
$сн У с-с Из
«vO
/ .„
,(i /-
,
3
Г / $tH,/ У«1-СН,
(И,
/YL/.to, 81,1 ,5336
t J ,(.Hi
iHj55
/- / Нз89,7 по 1,5530
Ы™) «У -.
71,0 т.пл. 78-79°
72,20 7,92 7,32 8,38 71,93 7,90 7,25 8,43 енз
72,67 8,15 7,06 8,08 72,58 8,30 7,18 8,01
40
if,5
72,67 8,15 7,06 8,08 85,5 по 1,5597 72,33 8,31 7,03 8,10
73,11 8,36 6,82 7,81 73,32 8,45 6jT 7,36
73 Л1 8,36 6,82 7,81 73,01 8,21 6,98 7,90
V /Сп
/ W . .
/
СН,
16,08
69,29 7,60
7,03
по 1,5830 16,18
68,91 7,57
7,25
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9387471A JPS5039125B2 (ru) | 1971-11-22 | 1971-11-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU576923A3 true SU576923A3 (ru) | 1977-10-15 |
Family
ID=14094596
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU721851051A SU576923A3 (ru) | 1971-11-22 | 1972-11-21 | Способ получени имидокарбонатных производных |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS5039125B2 (ru) |
| AU (1) | AU449798B2 (ru) |
| CA (1) | CA975781A (ru) |
| CH (1) | CH577971A5 (ru) |
| ES (1) | ES408791A1 (ru) |
| FR (1) | FR2160908B1 (ru) |
| GB (1) | GB1380099A (ru) |
| IT (1) | IT973662B (ru) |
| NL (1) | NL153529B (ru) |
| SU (1) | SU576923A3 (ru) |
-
1971
- 1971-11-22 JP JP9387471A patent/JPS5039125B2/ja not_active Expired
-
1972
- 1972-11-06 AU AU48543/72A patent/AU449798B2/en not_active Expired
- 1972-11-15 GB GB5283472A patent/GB1380099A/en not_active Expired
- 1972-11-20 ES ES408791A patent/ES408791A1/es not_active Expired
- 1972-11-21 IT IT5418372A patent/IT973662B/it active
- 1972-11-21 SU SU721851051A patent/SU576923A3/ru active
- 1972-11-21 NL NL7215730A patent/NL153529B/xx not_active IP Right Cessation
- 1972-11-21 CA CA157,115A patent/CA975781A/en not_active Expired
- 1972-11-21 FR FR7241309A patent/FR2160908B1/fr not_active Expired
- 1972-11-22 CH CH1701972A patent/CH577971A5/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| IT973662B (it) | 1974-06-10 |
| JPS4858139A (ru) | 1973-08-15 |
| DE2257052A1 (de) | 1973-06-07 |
| NL7215730A (ru) | 1973-05-24 |
| GB1380099A (en) | 1975-01-08 |
| DE2257052B2 (de) | 1975-05-28 |
| ES408791A1 (es) | 1976-03-01 |
| AU449798B2 (en) | 1974-06-20 |
| FR2160908A1 (ru) | 1973-07-06 |
| CA975781A (en) | 1975-10-07 |
| FR2160908B1 (ru) | 1975-03-28 |
| JPS5039125B2 (ru) | 1975-12-15 |
| NL153529B (nl) | 1977-06-15 |
| CH577971A5 (ru) | 1976-07-30 |
| AU4854372A (en) | 1974-05-09 |
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