RU2009102448A - METHOD FOR PRODUCING 2,4,6-TRIMETHYL- (1,3,5-DITIAZINAN-5-IL) AMINE - Google Patents

METHOD FOR PRODUCING 2,4,6-TRIMETHYL- (1,3,5-DITIAZINAN-5-IL) AMINE Download PDF

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RU2009102448A
RU2009102448A RU2009102448/04A RU2009102448A RU2009102448A RU 2009102448 A RU2009102448 A RU 2009102448A RU 2009102448/04 A RU2009102448/04 A RU 2009102448/04A RU 2009102448 A RU2009102448 A RU 2009102448A RU 2009102448 A RU2009102448 A RU 2009102448A
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trimethyl
amine
hydrogen sulfide
ditiazinan
producing
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RU2009102448/04A
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RU2481337C2 (en
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Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Наталия Наильевна Мурзакова (RU)
Наталия Наильевна Мурзакова
Гузель Ражаповна Хабибуллина (RU)
Гузель Ражаповна Хабибуллина
Райхана Валиулловна Кунакова (RU)
Райхана Валиулловна Кунакова
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
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Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран
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Priority to RU2009102448/04A priority Critical patent/RU2481337C2/en
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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

Способ получения 2,4,6-триметил-(1,3,5-дитиазинан-5-ил)-амина ! , ! заключающийся во взаимодействии предварительно перемешанной при температуре 0°С в течение 15 мин смеси гидразингидрата (60%) и уксусного альдегида с сероводородом до достижения мольного соотношения реагентов гидразин: уксусный альдегид: сероводород = 1:4:2 и последующем перемешивании реакционной массы в течение 1 ч при 0°С. The method of obtaining 2,4,6-trimethyl- (1,3,5-dithiazinan-5-yl) -amine! ! consisting in the interaction of a mixture of hydrazine hydrate (60%) and acetic aldehyde with hydrogen sulfide pre-mixed at a temperature of 0 ° C for 15 min until a molar ratio of hydrazine: acetic aldehyde: hydrogen sulfide = 1: 4: 2 is reached and the reaction mixture is subsequently stirred for 1 h at 0 ° C.

Claims (1)

Способ получения 2,4,6-триметил-(1,3,5-дитиазинан-5-ил)-аминаThe method of obtaining 2,4,6-trimethyl- (1,3,5-dithiazinan-5-yl) -amine
Figure 00000001
,
Figure 00000001
, заключающийся во взаимодействии предварительно перемешанной при температуре 0°С в течение 15 мин смеси гидразингидрата (60%) и уксусного альдегида с сероводородом до достижения мольного соотношения реагентов гидразин: уксусный альдегид: сероводород = 1:4:2 и последующем перемешивании реакционной массы в течение 1 ч при 0°С. consisting in the interaction of a mixture of hydrazine hydrate (60%) and acetic aldehyde with hydrogen sulfide pre-mixed at a temperature of 0 ° C for 15 min until a molar ratio of hydrazine: acetic aldehyde: hydrogen sulfide = 1: 4: 2 is reached and the reaction mixture is subsequently stirred for 1 h at 0 ° C.
RU2009102448/04A 2009-01-26 2009-01-26 Method of producing 2,4,6-trimethyl-(1,3,5-dithiazinan-5-yl)amine RU2481337C2 (en)

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RU2009102448/04A RU2481337C2 (en) 2009-01-26 2009-01-26 Method of producing 2,4,6-trimethyl-(1,3,5-dithiazinan-5-yl)amine

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RU2009102448/04A RU2481337C2 (en) 2009-01-26 2009-01-26 Method of producing 2,4,6-trimethyl-(1,3,5-dithiazinan-5-yl)amine

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4228278A (en) * 1978-11-17 1980-10-14 International Flavors & Fragrances Inc. Preparation of 2,4,6-tri-isobutyl dihydro-1,3,5-dithiazine
RU2291864C1 (en) * 2005-05-13 2007-01-20 Институт нефтехимии и катализа РАН Method for preparing n-methylene-4h-1,3,5-dithiazinyl-5(6h)-amine

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