PL3256252T3 - Sposób regeneracji katalizatora na bazie zeolitu tytanowego do epoksydowania propylenu - Google Patents
Sposób regeneracji katalizatora na bazie zeolitu tytanowego do epoksydowania propylenuInfo
- Publication number
- PL3256252T3 PL3256252T3 PL16704206T PL16704206T PL3256252T3 PL 3256252 T3 PL3256252 T3 PL 3256252T3 PL 16704206 T PL16704206 T PL 16704206T PL 16704206 T PL16704206 T PL 16704206T PL 3256252 T3 PL3256252 T3 PL 3256252T3
- Authority
- PL
- Poland
- Prior art keywords
- regeneration
- zeolite catalyst
- titanium zeolite
- propylene epoxidation
- epoxidation
- Prior art date
Links
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title 1
- 229910021536 Zeolite Inorganic materials 0.000 title 1
- 239000003054 catalyst Substances 0.000 title 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title 1
- 238000006735 epoxidation reaction Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 title 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 title 1
- 230000008929 regeneration Effects 0.000 title 1
- 238000011069 regeneration method Methods 0.000 title 1
- 229910052719 titanium Inorganic materials 0.000 title 1
- 239000010936 titanium Substances 0.000 title 1
- 239000010457 zeolite Substances 0.000 title 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/90—Regeneration or reactivation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
- B01J38/12—Treating with free oxygen-containing gas
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
- B01J2229/183—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself in framework positions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
- B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/647—2-50 nm
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
- C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
- C01B39/085—Group IVB- metallosilicates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201562115658P | 2015-02-13 | 2015-02-13 | |
EP15154998 | 2015-02-13 | ||
PCT/EP2016/052983 WO2016128538A1 (en) | 2015-02-13 | 2016-02-12 | Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation |
EP16704206.8A EP3256252B1 (en) | 2015-02-13 | 2016-02-12 | Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation |
Publications (1)
Publication Number | Publication Date |
---|---|
PL3256252T3 true PL3256252T3 (pl) | 2021-10-25 |
Family
ID=52472215
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PL16704206T PL3256252T3 (pl) | 2015-02-13 | 2016-02-12 | Sposób regeneracji katalizatora na bazie zeolitu tytanowego do epoksydowania propylenu |
Country Status (11)
Country | Link |
---|---|
US (1) | US10195598B2 (pl) |
EP (1) | EP3256252B1 (pl) |
JP (1) | JP6685315B2 (pl) |
KR (1) | KR102512661B1 (pl) |
CN (1) | CN107530693A (pl) |
BR (1) | BR112017017269B1 (pl) |
MX (1) | MX2017010402A (pl) |
MY (1) | MY189272A (pl) |
PL (1) | PL3256252T3 (pl) |
SG (1) | SG11201706530RA (pl) |
WO (1) | WO2016128538A1 (pl) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
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US10202324B2 (en) | 2015-05-04 | 2019-02-12 | Basf Se | Process for the preparation of melonal |
US10308580B2 (en) | 2015-07-15 | 2019-06-04 | Basf Se | Process for preparing an arylpropene |
CN108137523B (zh) | 2015-07-22 | 2022-07-26 | 巴斯夫欧洲公司 | 制备呋喃-2,5-二甲酸的方法 |
EP3170828A1 (de) | 2015-11-23 | 2017-05-24 | Basf Se | Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten |
ES2765740T3 (es) | 2015-11-27 | 2020-06-10 | Basf Se | Síntesis ultrarápida de elevado rendimiento-espacio-tiempo de armazones orgánicos-metal |
EP3178788A1 (en) | 2015-12-08 | 2017-06-14 | Basf Se | A tin-containing zeolitic material having a bea framework structure |
WO2017097806A1 (en) | 2015-12-08 | 2017-06-15 | Basf Se | A tin-containing zeolitic material having a bea framework structure |
WO2017133995A1 (de) | 2016-02-01 | 2017-08-10 | Basf Se | Verfahren zur herstellung von c4-c15-lactamen |
MX2018016297A (es) | 2016-06-29 | 2019-09-16 | Basf Se | Proceso para la preparacion de aldehidos alfa, beta insaturados mediante oxidacion de alcoholes en presencia de una fase liquida. |
JP6986063B2 (ja) | 2016-07-08 | 2021-12-22 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 有機スルホンの製造方法 |
US10544116B2 (en) | 2016-07-20 | 2020-01-28 | Basf Se | Process for purifying propylene oxide |
CA3030687A1 (en) | 2016-07-29 | 2018-02-01 | Basf Corporation | Process for the preparation of a zeolitic material having a fau-type framework structure and use thereof in the selective catalytic reduction of nox |
US11529618B2 (en) | 2016-11-28 | 2022-12-20 | Basf Se | Catalyst composite comprising an alkaline earth metal containing CHA zeolite and use thereof in a process for the conversion of oxygenates to olefins |
US11091425B2 (en) | 2016-11-30 | 2021-08-17 | Basf Se | Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst |
US11104637B2 (en) | 2016-11-30 | 2021-08-31 | Basf Se | Process for the conversion of monoethanolamine to ethylenediamine employing a copper-modified zeolite of the MOR framework structure |
US10981796B2 (en) | 2016-12-13 | 2021-04-20 | Basf Se | Process for the preparation of a titanium-containing zeolite |
JP2021506870A (ja) * | 2017-12-21 | 2021-02-22 | ビーエイエスエフ・ソシエタス・エウロパエアBasf Se | 液相の存在下でのアルコールの酸化によるα,β不飽和アルデヒドの製造方法 |
EP3604222A1 (en) * | 2018-07-30 | 2020-02-05 | Evonik Operations GmbH | Process for the purification of hydrogen cyanide |
EP3862082A4 (en) * | 2018-11-15 | 2021-10-20 | Dalian Institute Of Chemical Physics, Chinese Academy Of Sciences | METHOD OF MANUFACTURING A HIERARCHICAL POROUS TITANOSILICATE TS-1 MOLECULAR SCREEN |
TW202045484A (zh) * | 2019-02-08 | 2020-12-16 | 德商贏創運營有限公司 | 有機化合物的氧化 |
CN110252393A (zh) * | 2019-05-21 | 2019-09-20 | 江西农业大学 | 一种用于合成环氧大豆油的钛硅沸石负载镉催化剂、制备方法及应用 |
CN110075914A (zh) * | 2019-05-28 | 2019-08-02 | 江苏扬农化工集团有限公司 | 一种hppo工艺失活钛硅分子筛催化剂器内再生的方法 |
EP3812375A1 (en) * | 2019-10-21 | 2021-04-28 | Evonik Operations GmbH | Process for the epoxidation of propene |
CN112354557B (zh) * | 2020-11-16 | 2023-03-24 | 华东师范大学 | 一种整体式钛沸石催化剂制备方法及其应用 |
CN112678866B (zh) * | 2020-12-24 | 2023-07-04 | 中国石油化工股份有限公司 | 一种烯烃聚合工业废酸渣资源化处理方法 |
CN112844468A (zh) * | 2021-01-19 | 2021-05-28 | 中国科学院大连化学物理研究所 | 一种用于丙烯气相环氧化制环氧丙烷的催化剂及其制备方法 |
CN113368895B (zh) * | 2021-07-13 | 2023-09-29 | 福州大学 | 一种具有高转化率的丙烯气相环氧化催化剂的制备方法 |
CN118043136A (zh) * | 2021-09-30 | 2024-05-14 | 巴斯夫公司 | 用于脱氢和其他反应的多孔金属氧化物催化剂的预处理 |
WO2024115737A1 (en) | 2022-12-02 | 2024-06-06 | Basf Se | Process for regeneration of an epoxidation reactor |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
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DE19723751A1 (de) | 1997-06-06 | 1998-12-10 | Basf Ag | Formkörper und Verfahren zu dessen Herstellung |
US6114551A (en) | 1999-10-04 | 2000-09-05 | Mobil Oil Corporation | Olefin epoxidation catalysts |
DE10044798A1 (de) | 2000-09-11 | 2002-04-04 | Basf Ag | Verfahren zur Regenerierung eines Zeolith-Katalysators |
DE50115570D1 (de) | 2001-01-08 | 2010-09-09 | Evonik Degussa Gmbh | Verfahren zur Epoxidierung von Olefinen |
DE10320635A1 (de) * | 2003-05-08 | 2004-11-18 | Basf Ag | Verfahren zur Herstellung von Propylenoxid |
EP1489074A1 (en) | 2003-06-18 | 2004-12-22 | Degussa AG | Process for the epoxidation of propene |
US20050277542A1 (en) * | 2004-06-14 | 2005-12-15 | Kaminsky Mark P | Catalyst regeneration process |
KR101166932B1 (ko) | 2005-07-27 | 2012-07-19 | 에스케이이노베이션 주식회사 | 티타늄 함유 분자체 촉매의 재생방법 |
JP2009233656A (ja) | 2008-03-05 | 2009-10-15 | Sumitomo Chemical Co Ltd | チタノシリケート触媒の再生方法 |
CN101480623B (zh) | 2009-02-24 | 2011-06-08 | 江苏扬农化工集团有限公司 | 一种钛硅分子筛催化剂的再生方法 |
KR20130005269A (ko) * | 2010-03-18 | 2013-01-15 | 스미또모 가가꾸 가부시끼가이샤 | 티타노실리케이트 촉매의 재생 방법 |
EP3216520B1 (en) | 2012-02-07 | 2024-07-17 | Basf Se | Molding containing a zeolitic mww type material containing ti and zn and use thereof as a catalyst |
CN104014365B (zh) * | 2013-02-28 | 2016-08-24 | 中国石油化工股份有限公司 | 一种钛硅分子筛的再生方法 |
RU2673798C9 (ru) * | 2013-07-24 | 2019-04-08 | Басф Се | Регенерация титансодержащего цеолита |
-
2016
- 2016-02-12 EP EP16704206.8A patent/EP3256252B1/en active Active
- 2016-02-12 BR BR112017017269-0A patent/BR112017017269B1/pt active IP Right Grant
- 2016-02-12 JP JP2017542404A patent/JP6685315B2/ja active Active
- 2016-02-12 US US15/550,581 patent/US10195598B2/en active Active
- 2016-02-12 KR KR1020177025695A patent/KR102512661B1/ko active IP Right Grant
- 2016-02-12 PL PL16704206T patent/PL3256252T3/pl unknown
- 2016-02-12 SG SG11201706530RA patent/SG11201706530RA/en unknown
- 2016-02-12 WO PCT/EP2016/052983 patent/WO2016128538A1/en active Application Filing
- 2016-02-12 CN CN201680020837.XA patent/CN107530693A/zh active Pending
- 2016-02-12 MX MX2017010402A patent/MX2017010402A/es unknown
- 2016-02-12 MY MYPI2017001194A patent/MY189272A/en unknown
Also Published As
Publication number | Publication date |
---|---|
US20180036723A1 (en) | 2018-02-08 |
BR112017017269A2 (pt) | 2018-04-17 |
MX2017010402A (es) | 2018-05-28 |
US10195598B2 (en) | 2019-02-05 |
KR102512661B1 (ko) | 2023-03-21 |
MY189272A (en) | 2022-01-31 |
EP3256252A1 (en) | 2017-12-20 |
JP6685315B2 (ja) | 2020-04-22 |
BR112017017269B1 (pt) | 2022-05-24 |
SG11201706530RA (en) | 2017-09-28 |
WO2016128538A1 (en) | 2016-08-18 |
JP2018511459A (ja) | 2018-04-26 |
KR20170117509A (ko) | 2017-10-23 |
EP3256252B1 (en) | 2021-04-07 |
CN107530693A (zh) | 2018-01-02 |
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