NO303154B1 - SmalbÕnds-strÕlefilter - Google Patents

SmalbÕnds-strÕlefilter Download PDF

Info

Publication number: NO303154B1
Authority: NO; Norway
Prior art keywords: filter according; weight; comonomer; hydrogel; acrylamide
Prior art date: 1990-10-23

Application number

NO914151A

Other languages

English (en)

Norwegian (no)

Other versions

NO914151D0 (no

NO914151L (no

Inventor

Hans Peter Panzer

Lino Giovanni Magliocco

Martin Leonard Cohen

Wei S Yen

Original Assignee

American Cyanamid Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-10-23

Filing date

1991-10-22

Publication date

1998-06-02

1990-10-23 Priority claimed from US07/601,544 external-priority patent/US5342552A/en

1991-10-22 Application filed by American Cyanamid Co filed Critical American Cyanamid Co

1991-10-22 Publication of NO914151D0 publication Critical patent/NO914151D0/no

1992-04-24 Publication of NO914151L publication Critical patent/NO914151L/no

1998-06-02 Publication of NO303154B1 publication Critical patent/NO303154B1/no

Links

239000013078 crystal Substances 0.000 claims description 37
239000000017 hydrogel Substances 0.000 claims description 30
HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 29
239000000203 mixture Substances 0.000 claims description 24
239000010408 film Substances 0.000 claims description 19
239000003999 initiator Substances 0.000 claims description 18
239000002245 particle Substances 0.000 claims description 18
238000006116 polymerization reaction Methods 0.000 claims description 18
230000005855 radiation Effects 0.000 claims description 14
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
239000003431 cross linking reagent Substances 0.000 claims description 11
239000012736 aqueous medium Substances 0.000 claims description 10
229920001577 copolymer Polymers 0.000 claims description 9
229920000642 polymer Polymers 0.000 claims description 9
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 8
239000010409 thin film Substances 0.000 claims description 5
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 4
150000003254 radicals Chemical class 0.000 claims description 4
235000000346 sugar Nutrition 0.000 claims description 4
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 4
DWHJJLTXBKSHJG-HWKANZROSA-N (e)-5-hydroxy-2-methylpent-2-enoic acid Chemical compound OC(=O)C(/C)=C/CCO DWHJJLTXBKSHJG-HWKANZROSA-N 0.000 claims description 3
XHZPRMZZQOIPDS-UHFFFAOYSA-N 2-Methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(C)(C)NC(=O)C=C XHZPRMZZQOIPDS-UHFFFAOYSA-N 0.000 claims description 3
AGBXYHCHUYARJY-UHFFFAOYSA-N 2-phenylethenesulfonic acid Chemical compound OS(=O)(=O)C=CC1=CC=CC=C1 AGBXYHCHUYARJY-UHFFFAOYSA-N 0.000 claims description 3
WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 claims description 3
229930006000 Sucrose Natural products 0.000 claims description 3
NLVXSWCKKBEXTG-UHFFFAOYSA-M ethenesulfonate Chemical compound [O-]S(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-M 0.000 claims description 3
235000021309 simple sugar Nutrition 0.000 claims description 3
229910052708 sodium Inorganic materials 0.000 claims description 3
239000011734 sodium Substances 0.000 claims description 3
239000005720 sucrose Substances 0.000 claims description 3
GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 2
RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 2
229930091371 Fructose Natural products 0.000 claims description 2
239000005715 Fructose Substances 0.000 claims description 2
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 2
GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 2
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
239000008103 glucose Substances 0.000 claims description 2
239000008101 lactose Substances 0.000 claims description 2
PNOXUQIZPBURMT-UHFFFAOYSA-M potassium;3-(2-methylprop-2-enoyloxy)propane-1-sulfonate Chemical compound [K+].CC(=C)C(=O)OCCCS([O-])(=O)=O PNOXUQIZPBURMT-UHFFFAOYSA-M 0.000 claims description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
125000000185 sucrose group Chemical group 0.000 claims 1
239000000243 solution Substances 0.000 description 35
239000000178 monomer Substances 0.000 description 21
239000004816 latex Substances 0.000 description 14
229920000126 latex Polymers 0.000 description 14
239000007788 liquid Substances 0.000 description 13
239000004005 microsphere Substances 0.000 description 13
239000007787 solid Substances 0.000 description 11
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
238000000862 absorption spectrum Methods 0.000 description 8
239000002609 medium Substances 0.000 description 8
238000000034 method Methods 0.000 description 7
239000000725 suspension Substances 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
239000004793 Polystyrene Substances 0.000 description 6
239000007864 aqueous solution Substances 0.000 description 6
229920002223 polystyrene Polymers 0.000 description 6
239000010453 quartz Substances 0.000 description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
238000006243 chemical reaction Methods 0.000 description 5
238000004132 cross linking Methods 0.000 description 5
239000000839 emulsion Substances 0.000 description 5
125000000129 anionic group Chemical group 0.000 description 4
230000008901 benefit Effects 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 4
239000011521 glass Substances 0.000 description 4
230000014759 maintenance of location Effects 0.000 description 4
239000012071 phase Substances 0.000 description 4
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 3
239000004971 Cross linker Substances 0.000 description 3
230000000712 assembly Effects 0.000 description 3
238000000429 assembly Methods 0.000 description 3
239000006185 dispersion Substances 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
239000003456 ion exchange resin Substances 0.000 description 3
229920003303 ion-exchange polymer Polymers 0.000 description 3
ZIUHHBKFKCYYJD-UHFFFAOYSA-N n,n'-methylenebisacrylamide Chemical compound C=CC(=O)NCNC(=O)C=C ZIUHHBKFKCYYJD-UHFFFAOYSA-N 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
229920005862 polyol Polymers 0.000 description 3
150000003077 polyols Chemical class 0.000 description 3
150000008163 sugars Chemical class 0.000 description 3
239000011837 N,N-methylenebisacrylamide Substances 0.000 description 2
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
239000008346 aqueous phase Substances 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
210000004027 cell Anatomy 0.000 description 2
230000008859 change Effects 0.000 description 2
230000000694 effects Effects 0.000 description 2
238000001914 filtration Methods 0.000 description 2
230000008014 freezing Effects 0.000 description 2
238000007710 freezing Methods 0.000 description 2
239000006194 liquid suspension Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
239000004033 plastic Substances 0.000 description 2
229920003023 plastic Polymers 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000000376 reactant Substances 0.000 description 2
230000000717 retained effect Effects 0.000 description 2
230000035939 shock Effects 0.000 description 2
ZANRHLGMHYOWQU-UHFFFAOYSA-N 1,5-bis[4-(2-hydroxyethoxy)phenyl]-2,4-dimethylpentan-3-one Chemical compound C=1C=C(OCCO)C=CC=1CC(C)C(=O)C(C)CC1=CC=C(OCCO)C=C1 ZANRHLGMHYOWQU-UHFFFAOYSA-N 0.000 description 1
TURITJIWSQEMDB-UHFFFAOYSA-N 2-methyl-n-[(2-methylprop-2-enoylamino)methyl]prop-2-enamide Chemical compound CC(=C)C(=O)NCNC(=O)C(C)=C TURITJIWSQEMDB-UHFFFAOYSA-N 0.000 description 1
MKTOIPPVFPJEQO-UHFFFAOYSA-N 4-(3-carboxypropanoylperoxy)-4-oxobutanoic acid Chemical compound OC(=O)CCC(=O)OOC(=O)CCC(O)=O MKTOIPPVFPJEQO-UHFFFAOYSA-N 0.000 description 1
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
230000009471 action Effects 0.000 description 1
230000004913 activation Effects 0.000 description 1
238000013019 agitation Methods 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
210000002421 cell wall Anatomy 0.000 description 1
238000001246 colloidal dispersion Methods 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
238000007334 copolymerization reaction Methods 0.000 description 1
229920006037 cross link polymer Polymers 0.000 description 1
239000008367 deionised water Substances 0.000 description 1
229910021641 deionized water Inorganic materials 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
230000001066 destructive effect Effects 0.000 description 1
125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 1
230000005684 electric field Effects 0.000 description 1
239000003792 electrolyte Substances 0.000 description 1
239000000499 gel Substances 0.000 description 1
239000011491 glass wool Substances 0.000 description 1
239000012535 impurity Substances 0.000 description 1
230000003993 interaction Effects 0.000 description 1
238000005259 measurement Methods 0.000 description 1
239000012528 membrane Substances 0.000 description 1
239000011859 microparticle Substances 0.000 description 1
QYZFTMMPKCOTAN-UHFFFAOYSA-N n-[2-(2-hydroxyethylamino)ethyl]-2-[[1-[2-(2-hydroxyethylamino)ethylamino]-2-methyl-1-oxopropan-2-yl]diazenyl]-2-methylpropanamide Chemical compound OCCNCCNC(=O)C(C)(C)N=NC(C)(C)C(=O)NCCNCCO QYZFTMMPKCOTAN-UHFFFAOYSA-N 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
150000002825 nitriles Chemical class 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
229920006254 polymer film Polymers 0.000 description 1
229920005597 polymer membrane Polymers 0.000 description 1
239000011148 porous material Substances 0.000 description 1
FBSOFCDJBBJYKT-UHFFFAOYSA-M potassium;2-methyl-6-sulfohex-2-enoate Chemical compound [K+].[O-]C(=O)C(C)=CCCCS(O)(=O)=O FBSOFCDJBBJYKT-UHFFFAOYSA-M 0.000 description 1
230000008569 process Effects 0.000 description 1
235000013772 propylene glycol Nutrition 0.000 description 1
238000000746 purification Methods 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
239000011550 stock solution Substances 0.000 description 1
238000005728 strengthening Methods 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
238000010257 thawing Methods 0.000 description 1
239000012780 transparent material Substances 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1

Classifications

- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/20—Filters
- G02B5/203—Filters having holographic or diffractive elements
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/18—Diffraction gratings

Landscapes

Physics & Mathematics (AREA)
General Physics & Mathematics (AREA)
Optics & Photonics (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Compositions Of Macromolecular Compounds (AREA)
Polymerisation Methods In General (AREA)
Optical Filters (AREA)
Diffracting Gratings Or Hologram Optical Elements (AREA)

NO914151A 1990-10-23 1991-10-22 SmalbÕnds-strÕlefilter NO303154B1 (no)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US60197790A	1990-10-23	1990-10-23
US07/601,544 US5342552A (en)	1990-10-23	1990-10-23	Narrow band radiation filter films

Publications (3)

Publication Number	Publication Date
NO914151D0 NO914151D0 (no)	1991-10-22
NO914151L NO914151L (no)	1992-04-24
NO303154B1 true NO303154B1 (no)	1998-06-02

Family

ID=27083890

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO914151A NO303154B1 (no)	1990-10-23	1991-10-22	SmalbÕnds-strÕlefilter

Country Status (9)

Country	Link
EP (1)	EP0482394B1 (de)
JP (1)	JPH04264403A (de)
AR (1)	AR245988A1 (de)
AT (1)	ATE141010T1 (de)
DE (1)	DE69121162T2 (de)
FI (1)	FI104587B (de)
IL (1)	IL99822A (de)
NO (1)	NO303154B1 (de)
RU (1)	RU2085976C1 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP4106435B2 (ja)	2003-07-22	2008-06-25	独立行政法人物質・材料研究機構	コロイド結晶およびコロイド結晶ゲルの作製方法、および、そのための装置
JP5120909B2 (ja) *	2005-07-22	2013-01-16	独立行政法人物質・材料研究機構	コロイド結晶ゲルを製造する方法、コロイド結晶ゲル、および、光学素子
WO2007038219A2 (en) *	2005-09-23	2007-04-05	University Of North Texas	Synthesis of columnar hydrogel colloidal crystals in water-organic solvent mixture
JP5299843B2 (ja) *	2008-12-04	2013-09-25	株式会社豊田中央研究所	ポリマーで固定化されたコロイド結晶及びその製造方法
CN106405709B (zh) *	2016-11-16	2018-12-28	天津津航技术物理研究所	一种宽带截止超窄带滤光片

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2519777A1 (fr) *	1982-01-12	1983-07-18	Thomson Csf	Procede de fabrication de structures de phase diffractantes
US4627689A (en) *	1983-12-08	1986-12-09	University Of Pittsburgh	Crystalline colloidal narrow band radiation filter
US4632517A (en) *	1983-12-08	1986-12-30	University Of Pittsburgh	Crystalline colloidal narrow band radiation filter
GB8811894D0 (en) *	1988-05-19	1988-06-22	Secr Defence	Colloid spheres in suspension

1991
- 1991-10-02 EP EP91116835A patent/EP0482394B1/de not_active Expired - Lifetime
- 1991-10-02 DE DE69121162T patent/DE69121162T2/de not_active Expired - Fee Related
- 1991-10-02 AT AT91116835T patent/ATE141010T1/de not_active IP Right Cessation
- 1991-10-22 NO NO914151A patent/NO303154B1/no not_active IP Right Cessation
- 1991-10-22 AR AR91320979A patent/AR245988A1/es active
- 1991-10-22 FI FI914968A patent/FI104587B/fi active
- 1991-10-22 RU SU915001910A patent/RU2085976C1/ru active
- 1991-10-22 JP JP3301191A patent/JPH04264403A/ja active Pending
- 1991-10-23 IL IL9982291A patent/IL99822A/en not_active IP Right Cessation

Also Published As

Publication number	Publication date
ATE141010T1 (de)	1996-08-15
EP0482394A2 (de)	1992-04-29
FI914968A (fi)	1992-04-24
DE69121162T2 (de)	1997-01-16
EP0482394B1 (de)	1996-07-31
NO914151D0 (no)	1991-10-22
IL99822A (en)	1996-06-18
DE69121162D1 (de)	1996-09-05
NO914151L (no)	1992-04-24
FI914968A0 (fi)	1991-10-22
JPH04264403A (ja)	1992-09-21
RU2085976C1 (ru)	1997-07-27
EP0482394A3 (en)	1993-02-24
FI104587B (fi)	2000-02-29
AR245988A1 (es)	1994-03-30

Legal Events

Date	Code	Title	Description
2001-05-28	MM1K	Lapsed by not paying the annual fees	Free format text: LAPSED IN APRIL 2001

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US10358516B2 (en)	2019-07-23	Method for preparing porous hydrogel through freezing-illumination
US5338492A (en)	1994-08-16	Narrow band radiation filter films
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US4184992A (en)	1980-01-22	Cross-linked alkyl methacrylate-N-vinyllactam polymer composition for use in soft contact lenses
CA2054001C (en)	2002-06-11	Narrow band radiation filter films
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KR930008451B1 (ko)	1993-09-04	증대된 입자크기를 가지는 단일분산 중합체 입자의 제조방법
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US5863993A (en)	1999-01-26	Preparation method of polymeric rod and gradient-index rod lens using free radical bulk polymerization with temperature gradient
JPS6166707A (ja)	1986-04-05	新規アクリルアミド系共重合体及びその製造方法
Schulte et al.	2002	Development of non-reactive fluorine-rich biphenyl molecules and their incorporation into a PDLC system
JPH065322B2 (ja)	1994-01-19	光学材料の製造方法
KR19990045094A (ko)	1999-06-25	입자 및 그 제조방법
JPH07159767A (ja)	1995-06-23	エマルジョン組成物および液晶素子
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