NL2026655B1 - System and method for testing high-temperature tensile anisotropic r-values of metal plate - Google Patents
System and method for testing high-temperature tensile anisotropic r-values of metal plate Download PDFInfo
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/08—Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
- G01N3/18—Performing tests at high or low temperatures
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
- G01N3/06—Special adaptations of indicating or recording means
- G01N3/068—Special adaptations of indicating or recording means with optical indicating or recording means
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0014—Type of force applied
- G01N2203/0016—Tensile or compressive
- G01N2203/0017—Tensile
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0058—Kind of property studied
- G01N2203/0069—Fatigue, creep, strain-stress relations or elastic constants
- G01N2203/0075—Strain-stress relations or elastic constants
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/022—Environment of the test
- G01N2203/0222—Temperature
- G01N2203/0226—High temperature; Heating means
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/026—Specifications of the specimen
- G01N2203/0262—Shape of the specimen
- G01N2203/0278—Thin specimens
- G01N2203/0282—Two dimensional, e.g. tapes, webs, sheets, strips, disks or membranes
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/0641—Indicating or recording means; Sensing means using optical, X-ray, ultraviolet, infrared or similar detectors
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/067—Parameter measured for estimating the property
- G01N2203/0682—Spatial dimension, e.g. length, area, angle
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/067—Parameter measured for estimating the property
- G01N2203/0694—Temperature
Abstract
The invention discloses a system and method for testing high-temperature tensile anisotropic r-values of a metal plate, for accurately measuring the anisotropic r-values of the metal plate at high temperatures. The system comprises a tensile tester, a test sample arranged on the tensile tester, a temperature measurement and control system for controlling the temperature of the test sample, and a strain measurement system for measuring strain data of the test sample. The method comprises: measuring the temperature of the test sample and the maXimum output limit value of direct current, and calculating a limit value of temperature borne by the metal test sample, adjusting temperature control parameters, and adjusting the temperature of the test sample, measuring strain data of the test sample during hightemperature uniaXial tensile test, and determining the anisotropic r-values of the test sample at different temperatures according to the obtained strain data of the test sample.
Description
SYSTEM AND METHOD FOR TESTING HIGH-TEMPERATURE TENSILE ANISOTROPIC R-VALUES OF METAL PLATE Field of the Invention
The present disclosure relates to the field of characterization of mechanical properties of metal plates, and in particular to a system and method for testing tensile anisotropic r-values of a metal plate under high-temperature conditions.
Background of the Invention With the development of lightweight design, high-temperature forming has become an important process for forming aluminum-magnesium alloys and high-strength steels.
Plates usually have the feature of anisotropic, and the accurate characterization of anisotropic r- values of the plates at different temperatures has important guiding significance for hot forming numerical simulation of the plates and optimization of forming process parameters.
In recent years, a non-contact strain measurement method (DIC technology) has been widely used in the mechanical property test of metal plates.
The DIC technology can not only obtain the accurate strain of a metal plate, but also record the strain development history during the deformation of the plate, and then accurately measure uniaxial tensile anisotropic r-values of the plate.
During the research and development process, the inventors found that the existing measurement method has the following problems: (1) When a furnace heating method is used for tensile test, the DIC technology cannot be applied well due to the closed furnace body, the high-temperature air in the furnace and the refraction of light by glass, which will affect the test precision and cannot accurately obtain the anisotropic r-values of the plate. (2) A self-resistance heating method refers to that the current is introduced into a test sample, and Joule heat is generated by means of the resistance of the metal test sample, thereby increasing the temperature of the test sample.
When the test sample is heated by means of self-resistance, the resistance of a heating zone will change in the presence of a thermal inertia and with the deformation during the thermal tensile test, so that the temperature of the test sample cannot be stabilized at an accurate temperature value.
Summary of the Invention In order to overcome the above shortcomings of the prior art, the present disclosure provides a system and method for testing high-temperature tensile anisotropic r-values of a metal plate, which can accurately measure the anisotropic r-values of the metal plate at high temperatures.
One aspect of the present disclosure provides a technical solution of a system for testing high- temperature tensile anisotropic r-values of a metal plate: A system for testing high-temperature tensile anisotropic r-values of a metal plate includes a tensile tester, a test sample arranged on the tensile tester, a temperature measurement and control system for controlling the temperature of the test sample, and a strain measurement system for measuring strain data of the test sample.
Another aspect of the present disclosure provides a technical solution of a method for testing high-temperature tensile anisotropic r-values of a metal plate: A method for testing high-temperature tensile anisotropic r-values of a metal plate includes the following steps: measuring the temperature of a test sample and the maximum output limit value of direct current, and calculating a limit value of temperature borne by the metal test sample; adjusting temperature control parameters, and implementing real-time feedback control on the temperature of the tensile test sample by PLC control; measuring strain data of the test sample during high-temperature uniaxial tensile test; and determining the anisotropic r-values of the test sample at different temperatures according to the obtained strain data of the test sample.
Through the above technical solutions, the beneficial effects of the present disclosure are: (1) The present disclosure can obtain stable temperatures during thermal tensile test by setting heating parameters reasonably, the time required for heating to a predetermined temperature is short, the temperature control is accurate and stable, and the equipment of the present disclosure is simple, easy to implement, and low in cost; (2) The present disclosure realizes on-line strain measurement of mechanical properties of the metal plate under high-temperature conditions, can accurately measure the historical data of strain development of the test sample during the thermal tensile test, eliminates the influence of cooperation of various clamps in the traditional thermal tensile device on the experimental results, and accurately obtains the anisotropic r-values of the metal plate at different temperatures.
Brief Description of the Drawings The accompanying drawings constituting a part of the present disclosure are intended to provide a further understanding of the present disclosure, and the illustrative embodiments of the present disclosure and the descriptions thereof are intended to interpret the present disclosure and do not constitute improper limitations to the present disclosure.
FIG. 1 is a structural diagram of a temperature measurement and control system in Embodiment 1; FIG. 2 is a structural diagram of a strain measurement system in Embodiment 1; FIG. 3 is a structural diagram of a tensile control system in Embodiment 1; FIG. 4 is a flowchart of a method for testing high-temperature tensile anisotropic r-values of a metal plate in Embodiment 2; FIGS. 5(a) and 5(b) are schematic diagrams of middle temperature distribution of a test sample in a strain analysis zone of a central area of the test sample.
Detailed Description of Embodiments The present disclosure will be further illustrated below in conjunction with the accompanying drawings and embodiments.
It should be noted that the following detailed descriptions are exemplary and are intended to provide further descriptions of the present disclosure. All technical and scientific terms used herein have the same meanings as commonly understood by those of ordinary skill in the technical filed to which the present disclosure belongs, unless otherwise indicated.
It should be noted that the terms used here are merely used for describing specific embodiments, but are not intended to limit the exemplary embodiments of the present application. As used herein, the singular form is also intended to comprise the plural form unless otherwise indicated in the context. In addition, it should be understood that when the terms “contain” and/or “comprise” are used in the description, they are intended to indicate the presence of features, steps, operations, devices, components and/or combinations thereof.
Embodiment 1 This embodiment provides a system for testing high-temperature tensile anisotropic r-values of a metal plate. The system includes a temperature measurement and control system, a strain measurement system and a tensile control system.
Referring to FIG. 1, the temperature measurement and control system includes an embedded touch display screen 1, a control module 2, a temperature sensor 3 and a low-voltage high- current adjustable DC power supply 4. The control module 2 includes a PLC (Programmable Logic Controller) 6, a CPU (Central Processing Unit) 7, a thermocouple 8 and a power module. The low-voltage high-current adjustable DC power supply 4 is connected to both ends of a test sample 5, the temperature sensor 3 is connected to the thermocouple 8, and the thermocouple 8 is connected to the test sample, welded to the surface of the test sample, and used to collect the temperature of the test sample and output the temperature to the thermocouple 8; the CPU 7 is connected to the embedded touch display screen 1 and the thermocouple 8, the thermocouple 8 transmits the collected temperature data of the test sample to the CPU 7, the CPU 7 processes the temperature data of the test sample, and the embedded touch display screen 1 displays the real-time temperature of the test sample; the CPU 7 is also connected to the PLC 6, an output end of the PLC 6 is connected to the low- voltage high-current adjustable DC power supply 4, the CPU 7 transmits the processed data to the PLC 6, and the PLC 6 uses its PID function to output a control signal from the output port of the PLC to the low-voltage high-current adjustable DC power supply 4 in an automatic mode, thus controlling the output value of the low-voltage high-current adjustable DC power supply 4 to automatically adjust and control the temperature of the test sample.
In this embodiment, the temperature measurement and control system has two control modes, respectively open-loop control and closed-loop control.
(1) Open-loop control. The CPU is used as a host, and the thermocouple 1s expanded. The thermocouple is connected to the temperature sensor. The thermocouple obtains the temperature data of the test sample collected by the temperature sensor and transmits the temperature data to the CPU for processing, and the CPU transmits the processed data to the embedded touch display screen for displaying the real-time temperature of the test sample. In this process, the low-voltage high-current adjustable DC power supply adjusts the output value of the current in a manual mode to control the temperature of the test sample.
In a switch control state, the temperature measurement and control system measures a limit value of temperature borne by the metal test sample 5 and a maximum output limit parameter of direct current allowed by the metal test sample, so as to provide reference data for parameter setting of a closed-loop system. The output value of the direct current is manually controlled through a current control knob of the low-voltage high-current adjustable DC power supply, so that the current flowing through the test sample 5 gradually increases till the temperature of the test sample rises and the test sample fuses. The temperature of the test sample and the output value A of the direct current, displayed by the embedded touch display screen when the test sample fuses, are recorded. The temperature limit value of the test 5 sample is the recorded fusing temperature of the test sample; a calculation formula for the maximum output limit parameter M of the direct current is: M = 4 x 27648
Q Wherein, A is the maximum DC output limit value of the low-voltage high-current adjustable DC power supply when the test sample fuses, and Q is the range of the temperature sensor. (2) Closed-loop control. The CPU is used as a host, and the thermocouple is expanded. The thermocouple 1s connected to the temperature sensor. The temperature data of the test sample collected by the temperature sensor is processed, the thermocouple obtains the temperature data of the test sample collected by the temperature sensor and transmits the temperature data to the CPU for processing, the CPU transmits the processed data to the PLC, and the PLC outputs a control signal to the low-voltage high-current adjustable DC power supply in the automatic mode, thus controlling the output value of the low-voltage high-current adjustable DC power supply to automatically adjust and control the temperature of the test sample. A working process of the temperature measurement and control system proposed in this embodiment is: In the open-loop control state, the temperature measurement and control system measures the temperature limit value of the test sample and the maximum output limit parameter M of the direct current. Before the closed-loop control of the temperature measurement and control system is used, the temperature control parameters of the PLC need to be set. The control parameters include proportional gain, integral time, differential time, etc. First, the temperature limit value of the metal test sample, the temperature measurement range of the temperature sensor, and the maximum output limit parameter M of the direct current are input through the embedded touch display. Then, the temperature control parameters in the PLC are automatically set by using TIA Portal software to obtain the parameters such as proportional gain, integral time, and differential time required for the temperature control of the test sample, and the temperature control parameters are uploaded and saved to the PLC after the setting.
The PLC compares the collected real-time temperature of the test sample with a given temperature to obtain an error value between the real-time temperature and the given temperature, an output value proportional to the error value is calculated by proportional control of the PID function in the PLC, a steady-state error caused by the proportional control output value is eliminated by integral control, the future change trend of the error value is predicted by differential control and advanced control is implemented to suppress hysteresis errors of the proportional control and integral control output values in temperature adjustment, and then a control signal obtained by the combined action of proportional control, integral control and differential control is output from the output port of the PLC to the low- voltage high-current adjustable DC power supply in the automatic mode, to control the output value of the low-voltage high-current adjustable DC power supply, thereby realizing an automatic adjustment and control function on the temperature of the test sample.
In this embodiment, the temperature measurement and control system further includes a safety protection system.
The safety protection system is an emergency stop button.
The emergency stop button of the PLC realizes an instantaneous current output stop function of the low-voltage and high-current adjustable DC power supply, which can realize safety protection of the system in emergencies.
Referring to FIG. 2, the strain measurement system is a DIC three-dimensional digital speckle strain measurement system.
The three-dimensional digital speckle strain measurement system includes an adjustable measuring head 9, a control box 10 and a PC 11. The control box is connected to the adjustable measuring head 9 to control the adjustable measuring head, and camera power is triggered externally.
The control box 10 is connected to the PC 11, and the PC 11 is connected to the adjustable measuring head 9 by a cable.
The adjustable measuring head 9 includes a bracket, and a camera, a laser and an LED arranged on the bracket.
A working process of the strain measurement system proposed in this embodiment is: Before measurement, the surface of the test sample is sprayed with random speckles by using a high-temperature and oxidation resistant spray paint, and then the measurement distance between the measuring head and the test sample is adjusted according to the breadth parameters of the camera.
During measurement, the setting parameters are initialized at the PC, the cross central line of the camera is corrected, and images are captured.
After the images are captured, a patch area and seed points are created, and measurement results are automatically calculated.
Speckle images on the test sample are captured by the camera, deformation points on the surface are matched by using a digital image correlation algorithm (DIC), and a strain field of the thermal tensile test sample is calculated through the changes of three-dimensional coordinates of each point.
As an optical non-contact three-dimensional strain measuring system, it has the advantages of rapidness, simplicity, flexibility and high precision, and can achieve non-contact measurement, obtain real strain data of the test sample during the high- temperature uniaxial tensile process, and then determine anisotropic r-values of the plate at different temperatures.
Referring to FIG. 3, the tensile control system includes a tensile tester, the tensile tester includes a workbench 14, two clamps 12 arranged on the workbench and a test sample 5 held between the two clamps, the two clamps 12 are respectively provided with a terminal 15, one end of each of the terminals 15 is connected to the low-voltage high-current adjustable DC power supply 4 through a high current-carrying wire 16, and the low-voltage high-current adjustable DC power supply 4, the high current-carrying wires 16, the terminals 15, the clamps 12 and the test sample 5 form a current loop; the PLC 6 is connected to the low- voltage high-current adjustable DC power supply 4 to automatically control the low-voltage high-current adjustable DC power supply.
In this embodiment, each clamp 12 is provided with an insulating gasket 13, and the insulating gasket is used to reliably insulate the current loop and the tensile tester.
The tensile control system proposed in this embodiment implements thermal stretch of the metal test sample by means of the self-resistance heating of the metal test sample and the uniaxial tensile function of the tensile tester, and the tensile tester records a force-time curve of the test sample during the thermal tensile test process.
A working process of the tensile control system is: Positive and negative poles of the low-voltage high-current adjustable DC power supply 4 are respectively connected to the upper and lower clamps 12 of the tester through the high current-carrying wires 16 and the terminals 15. The direct current output by the low-voltage high-current adjustable DC power supply 4 flows through the test sample 5 held by the clamps via the high current-carrying wires 16, the terminals 15 and the clamps 12, the metal test sample 5 is thermally stretched by means of the self-resistance heating of the metal test sample and the uniaxial tensile function of the tester, and the force-time curve of the test sample 5 during the thermal tensile test process is recorded by the tensile tester and combined with a strain-time curve obtained by the strain measurement system to obtain accurate strain data of the test sample.
Referring to FIGS. 5(a) and 5(b), the temperature of the self-resistance electric heating test sample is in a gradient distribution, and a temperature constant zone in the middle area is selected for strain measurement. Although the self-resistance heating will reduce the elongation of the tensile test sample, when anisotropic r-values are measured, the data at small strain can be selected for obtaining accurate anisotropic r-values.
The system for testing high-temperature tensile anisotropic r-values of a metal plate according to this embodiment implements on-line strain measurement of mechanical properties of the metal plate under high-temperature conditions, and can accurately measure the historical data of strain development of the test sample during the thermal tensile test process, eliminate the influence of cooperation between various clamps in the traditional thermal tensile device on the experimental results, and accurately obtain the anisotropic r-values of the metal plate at different temperatures.
Embodiment 2 This embodiment provides a method for testing high-temperature tensile anisotropic r-values of a metal plate. This method is implemented based on the system for testing high- temperature tensile anisotropic r-values of a metal plate as described in Embodiment 1. Referring to FIG. 4, the method for testing high-temperature tensile anisotropic r-values of a metal plate includes the following steps: S101, a limit value of temperature borne by the metal test sample and a maximum output limit parameter of direct current allowed by the metal test sample are measured.
Specifically, in the open-loop control state of the temperature measurement and control system, the DC output value of the low-voltage high-current adjustable DC power supply is manually controlled, so that the current flowing through the test sample 5 gradually increases till the temperature of the test sample rises and the test sample fuses. The temperature data of the test sample collected by the temperature sensor is obtained by the thermocouple, and transmitted to the CPU for processing to obtain a temperature of the test sample and a maximum output limit value A of the direct current, and the limit value of temperature borne by the metal test sample is calculated by using the maximum output limit value A of the direct current and the range of the sensor.
S102, temperature control parameters in the PLC are set to obtain the parameters such as proportional gain, integral time, and differential time required for the temperature control of the test sample.
S103, the output value of the low-voltage high-current adjustable DC power supply 1s controlled by a PID control method, so as to automatically adjust and control the temperature of the test sample.
Specifically, in the closed-loop control state of the temperature measurement and control system, the PLC compares the collected real-time temperature of the test sample with a given temperature to obtain an error value between the real-time temperature and the given temperature, an output value proportional to the error value is calculated by proportional control of the PID function in the PLC, a steady-state error caused by the proportional control output value is eliminated by integral control, the future change trend of the error value is predicted by differential control and advanced control is implemented to suppress hysteresis errors of the proportional control and integral control output values in temperature adjustment, and then a control signal obtained by the combined action of proportional control, integral control and differential control is output from the output port of the PLC to the low- voltage high-current adjustable DC power supply in the automatic mode, to control the output value of the low-voltage high-current adjustable DC power supply, thereby realizing an automatic adjustment and control function on the temperature of the test sample.
S104, a high-temperature uniaxial tensile test is performed on the test sample, and strain data of the test sample during the high-temperature uniaxial tensile test is measured.
Positive and negative poles of the low-voltage high-current adjustable DC power supply 4 are respectively connected to the upper and lower clamps 12 of the tester through the high current-carrying wires 16 and the terminals 15. The direct current output by the low-voltage high-current adjustable DC power supply 4 flows through the test sample 5 held by the clamps via the high current-carrying wires 16, the terminals 15 and the clamps 12, and the metal test sample 5 is thermally stretched by means of the self-resistance heating of the metal test sample 5 and the uniaxial tensile function of the tester.
Before measurement, the surface of the test sample is sprayed with random speckles by using a high-temperature and oxidation resistant spray paint, and then the measurement distance between the measuring head and the test sample is adjusted according to the breadth parameters of the camera.
During measurement, the setting parameters are initialized at the PC, the cross central line of the camera is corrected, and images are captured.
After the images are captured, a patch area and seed points are created, speckle images on the test sample are captured by the camera, deformation points on the surface are matched by using a digital image correlation algorithm (DIC), and a strain field of the thermal tensile test sample is calculated through the changes of three-dimensional coordinates of each point.
S105, the anisotropic r-values of the test sample at different temperatures are determined according to the obtained strain data of the test sample during the high-temperature uniaxial tensile process.
In this embodiment, the test sample is a metal plate.
The method for testing high-temperature tensile anisotropic r-values of a metal plate according to this embodiment implements on-line strain measurement of mechanical properties of the metal plate under high-temperature conditions, and can accurately measure the historical data of strain development of the test sample during the thermal tensile test process, eliminate the influence of cooperation between various clamps in the traditional thermal tensile device on the experimental results, and accurately obtain the anisotropic r- values of the metal plate at different temperatures.
Although the specific embodiments of the present disclosure are described above in combination with the accompanying drawings, the protection scope of the present disclosure is not limited thereto.
It should be understood by those skilled in the art that various modifications or variations could be made by those skilled in the art based on the technical solution of the present disclosure without any creative effort, and these modifications or variations shall fall into the protection scope of the present disclosure.
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