MX2013006190A - Procedimiento mejorado para la preparacion de 2-trifluorometil-5-(1-substituido)alquilpiridinas. - Google Patents
Procedimiento mejorado para la preparacion de 2-trifluorometil-5-(1-substituido)alquilpiridinas.Info
- Publication number
- MX2013006190A MX2013006190A MX2013006190A MX2013006190A MX2013006190A MX 2013006190 A MX2013006190 A MX 2013006190A MX 2013006190 A MX2013006190 A MX 2013006190A MX 2013006190 A MX2013006190 A MX 2013006190A MX 2013006190 A MX2013006190 A MX 2013006190A
- Authority
- MX
- Mexico
- Prior art keywords
- alkylpyridines
- trifluoromethyl
- bstituted
- preparation
- improved process
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D491/00—Heterocyclic compounds containing in the condensed ring system both one or more rings having oxygen atoms as the only ring hetero atoms and one or more rings having nitrogen atoms as the only ring hetero atoms, not provided for by groups C07D451/00 - C07D459/00, C07D463/00, C07D477/00 or C07D489/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
- C07D213/32—Sulfur atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/08—Preparation by ring-closure
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/08—Preparation by ring-closure
- C07D213/09—Preparation by ring-closure involving the use of ammonia, amines, amine salts, or nitriles
- C07D213/12—Preparation by ring-closure involving the use of ammonia, amines, amine salts, or nitriles from unsaturated compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Se producen 2-Trifluorometil-5-(1-sustituido)alquilpiridinas en forma eficiente y en un alto rendimiento a partir de 4-alcoxi-1,1,1-trifluorobut-3-en-2-ona mediante una reacción de condensación y ciclización. Ambas reacciones se realizan en el mismo solvente no polar sin aislamiento y purificación de intermedios.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US41927910P | 2010-12-03 | 2010-12-03 | |
PCT/US2011/061980 WO2012074857A2 (en) | 2010-12-03 | 2011-11-23 | Improved process for the preparation of 2-trifluoromethyl-5-(1-substituted)alkylpyridines |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2013006190A true MX2013006190A (es) | 2013-07-29 |
Family
ID=46162833
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013006190A MX2013006190A (es) | 2010-12-03 | 2011-11-23 | Procedimiento mejorado para la preparacion de 2-trifluorometil-5-(1-substituido)alquilpiridinas. |
Country Status (17)
Country | Link |
---|---|
US (1) | US8742125B2 (es) |
EP (1) | EP2646416B9 (es) |
JP (1) | JP5828004B2 (es) |
KR (1) | KR20130124330A (es) |
CN (1) | CN103814031B (es) |
AR (1) | AR084099A1 (es) |
AU (1) | AU2011336870B2 (es) |
BR (1) | BR112013013290B1 (es) |
CA (1) | CA2818513C (es) |
CO (1) | CO6700894A2 (es) |
IL (1) | IL226660A (es) |
MX (1) | MX2013006190A (es) |
PL (1) | PL2646416T3 (es) |
RU (1) | RU2608317C2 (es) |
UA (1) | UA113281C2 (es) |
WO (1) | WO2012074857A2 (es) |
ZA (1) | ZA201303872B (es) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2012074857A2 (en) | 2010-12-03 | 2012-06-07 | Dow Agrosciences Llc | Improved process for the preparation of 2-trifluoromethyl-5-(1-substituted)alkylpyridines |
JP6242392B2 (ja) * | 2012-06-30 | 2017-12-06 | ダウ アグロサイエンシィズ エルエルシー | ピリジンn−オキシドおよびそれらの製法 |
CN102977005A (zh) * | 2012-11-08 | 2013-03-20 | 安徽国星生物化学有限公司 | 2,3,5-三甲基吡啶的提纯方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NO912475L (no) * | 1990-06-27 | 1991-12-30 | Sankyo Co | Tiazolidinkarboksylsyreamidderivater med antiallergisk aktivitet, og fremgangsmaate til fremstilling derav. |
RU2083562C1 (ru) * | 1993-02-05 | 1997-07-10 | Исихара Сангио Кайся Лтд. | Производные пиридина, способ их получения, инсектицидная композиция |
ATE223900T1 (de) * | 1995-05-26 | 2002-09-15 | Ishihara Sangyo Kaisha | Verfahren zur herstellung von 4- trifluormethylnicotinsäure |
BRPI0509695B8 (pt) | 2004-04-08 | 2022-06-28 | Dow Agrosciences Llc | Sulfoximinas n-substituídas, composição e método para controlar insetos |
TW201309635A (zh) | 2006-02-10 | 2013-03-01 | Dow Agrosciences Llc | 殺蟲性之n-取代(6-鹵烷基吡啶-3-基)烷基磺醯亞胺(二) |
TWI383973B (zh) | 2006-08-07 | 2013-02-01 | Dow Agrosciences Llc | 用於製備2-取代-5-(1-烷硫基)烷基吡啶之方法 |
TWI387585B (zh) * | 2006-09-01 | 2013-03-01 | Dow Agrosciences Llc | 殺蟲性之n-取代(雜芳基)烷基烴基硫亞胺 |
PL2166851T3 (pl) * | 2007-07-20 | 2012-02-29 | Dow Agrosciences Llc | Zwiększanie żywotności roślin |
MX2011000196A (es) * | 2008-07-01 | 2011-03-24 | Dow Agrosciences Llc | Proceso mejorado para la preparacion de alquilpiridinas 2-trifluorometil-5-(1-sustituidas). |
WO2012074857A2 (en) | 2010-12-03 | 2012-06-07 | Dow Agrosciences Llc | Improved process for the preparation of 2-trifluoromethyl-5-(1-substituted)alkylpyridines |
-
2011
- 2011-11-23 WO PCT/US2011/061980 patent/WO2012074857A2/en active Application Filing
- 2011-11-23 AU AU2011336870A patent/AU2011336870B2/en active Active
- 2011-11-23 JP JP2013542059A patent/JP5828004B2/ja active Active
- 2011-11-23 KR KR1020137014014A patent/KR20130124330A/ko not_active Application Discontinuation
- 2011-11-23 UA UAA201308355A patent/UA113281C2/uk unknown
- 2011-11-23 CA CA2818513A patent/CA2818513C/en active Active
- 2011-11-23 PL PL11844184T patent/PL2646416T3/pl unknown
- 2011-11-23 CN CN201180058142.8A patent/CN103814031B/zh active Active
- 2011-11-23 EP EP11844184.9A patent/EP2646416B9/en active Active
- 2011-11-23 RU RU2013130244A patent/RU2608317C2/ru active
- 2011-11-23 US US13/303,182 patent/US8742125B2/en active Active
- 2011-11-23 MX MX2013006190A patent/MX2013006190A/es active IP Right Grant
- 2011-11-23 BR BR112013013290-6A patent/BR112013013290B1/pt active IP Right Grant
- 2011-12-02 AR ARP110104520A patent/AR084099A1/es active IP Right Grant
-
2013
- 2013-05-28 ZA ZA2013/03872A patent/ZA201303872B/en unknown
- 2013-05-29 CO CO13131752A patent/CO6700894A2/es unknown
- 2013-05-30 IL IL226660A patent/IL226660A/en active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
EP2646416A2 (en) | 2013-10-09 |
AR084099A1 (es) | 2013-04-17 |
BR112013013290B1 (pt) | 2018-02-14 |
RU2608317C2 (ru) | 2017-01-17 |
PL2646416T3 (pl) | 2017-03-31 |
CA2818513C (en) | 2018-07-17 |
WO2012074857A3 (en) | 2014-03-13 |
IL226660A (en) | 2017-05-29 |
EP2646416A4 (en) | 2014-11-05 |
WO2012074857A2 (en) | 2012-06-07 |
BR112013013290A2 (pt) | 2016-07-12 |
EP2646416B1 (en) | 2016-09-07 |
KR20130124330A (ko) | 2013-11-13 |
US20120142933A1 (en) | 2012-06-07 |
AU2011336870B2 (en) | 2016-03-03 |
RU2013130244A (ru) | 2015-01-10 |
US8742125B2 (en) | 2014-06-03 |
CA2818513A1 (en) | 2012-06-07 |
CN103814031A (zh) | 2014-05-21 |
UA113281C2 (xx) | 2017-01-10 |
CN103814031B (zh) | 2016-10-19 |
CO6700894A2 (es) | 2013-06-28 |
ZA201303872B (en) | 2014-08-27 |
AU2011336870A1 (en) | 2013-05-30 |
JP2014514241A (ja) | 2014-06-19 |
EP2646416B9 (en) | 2016-12-21 |
JP5828004B2 (ja) | 2015-12-02 |
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Legal Events
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