KR960704707A - 다층 차단 필름(Multilayer barrier film) - Google Patents
다층 차단 필름(Multilayer barrier film)Info
- Publication number
- KR960704707A KR960704707A KR1019960701307A KR19960701307A KR960704707A KR 960704707 A KR960704707 A KR 960704707A KR 1019960701307 A KR1019960701307 A KR 1019960701307A KR 19960701307 A KR19960701307 A KR 19960701307A KR 960704707 A KR960704707 A KR 960704707A
- Authority
- KR
- South Korea
- Prior art keywords
- barrier film
- multilayer barrier
- multilayer
- copolymer
- film
- Prior art date
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F5/00—Orthopaedic methods or devices for non-surgical treatment of bones or joints; Nursing devices; Anti-rape devices
- A61F5/44—Devices worn by the patient for reception of urine, faeces, catamenial or other discharge; Portable urination aids; Colostomy devices
- A61F5/445—Colostomy, ileostomy or urethrostomy devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/30—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
- B32B27/304—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl halide (co)polymers, e.g. PVC, PVDC, PVF, PVDF
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/40—Layered products comprising a layer of synthetic resin comprising polyurethanes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D65/00—Wrappers or flexible covers; Packaging materials of special type or form
- B65D65/38—Packaging materials of special type or form
- B65D65/40—Applications of laminates for particular packaging purposes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/31—Heat sealable
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/724—Permeability to gases, adsorption
- B32B2307/7242—Non-permeable
- B32B2307/7244—Oxygen barrier
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/724—Permeability to gases, adsorption
- B32B2307/7242—Non-permeable
- B32B2307/7246—Water vapor barrier
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2327/00—Polyvinylhalogenides
- B32B2327/06—PVC, i.e. polyvinylchloride
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2375/00—Polyureas; Polyurethanes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2535/00—Medical equipment, e.g. bandage, prostheses, catheter
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/13—Hollow or container type article [e.g., tube, vase, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
- Y10T428/31515—As intermediate layer
- Y10T428/31522—Next to metal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31573—Next to addition polymer of ethylenically unsaturated monomer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31573—Next to addition polymer of ethylenically unsaturated monomer
- Y10T428/31587—Hydrocarbon polymer [polyethylene, polybutadiene, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31786—Of polyester [e.g., alkyd, etc.]
- Y10T428/31797—Next to addition polymer from unsaturated monomers
Landscapes
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Nursing (AREA)
- Biomedical Technology (AREA)
- Heart & Thoracic Surgery (AREA)
- Vascular Medicine (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Orthopedic Medicine & Surgery (AREA)
- Veterinary Medicine (AREA)
- Mechanical Engineering (AREA)
- Laminated Bodies (AREA)
- Materials For Medical Uses (AREA)
- Orthopedics, Nursing, And Contraception (AREA)
- Prostheses (AREA)
- Medicinal Preparation (AREA)
- Wrappers (AREA)
Abstract
본 발명은 비닐리덴 클로라이드의 단독중합체, 비닐리덴 클로라이드와 비닐 클로라이드와의 공중합체 또는 비닐리덴 클로라이드와 메틸 메타클리레이트와의 공중합체를 함유하는 차단층(12)을 포함하는 산소 및 수분 불투과성 다층 차단 필름(10)에 관한 것이다. 차단층은 열가소성 폴리우레탄, 에틸렌과 α-올레핀과의 사실상 선형 공중합체 또는 균질하게 측쇄된 선형 올레핀 수지를 함유하는 하나 이상의 열 밀봉가능한 표층(14)과 함께 동시 압출되거나 이에 적층되어 다층 차단 필름을 형성한다. 다층 필름은 재사용 가능한 개구 수술 백(24), 약제의 피하운반용 시스템 및 포장시에 사용된 열 밀봉가능한 백에 사용할 수 있다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1도는 본 발명의 다층 차단 필름의 한 가지 양태의 개략적인 단면도이다,
제 2도는 본 발명의 다층 차단 필름의 또 다른 양태의 개략적인 단면도이다,
제 3도는 본 발명에 따르는 피하 약제 운반 시스템의 한 가지 양태의 개략적인 단면도이다,
제 4도는 본 발명에 따르는 피하 약제 운반 시스템의 또 다른 양태의 개략적인 단면도이다,
제 5도는 본 발명의 제1도 또는 제2도의 다층 차단 필름으로부터 형성된 개구 수술 백 또는 파우치의 정면도필.
Claims (15)
- 차단층과 하나 이상의 열 밀봉가능한 표층[여기서, 열가소성 중합체를 함유하는 표층은, 2% 시컨트 모듈러스가 종방향과 횡방향 모두 15,000psi미만이다]을 함유하는, 열 밀봉 강도가 필름 너비(in)당 1.01ℓb이상이고, 0.45Hz에서 65°각도로 굴곡시키는 경우 소음도가 85dB미만인 산소 및 수분 불투과성 다층 차단 필름.
- 제1항에 있어서, 표층이 열가소성 폴리우레탄, 밀도가 0.87 내지 0.95gm/cc의 범위이고 장쇄 측쇄(long chain branch)가 중합체 주쇄를 따라 탄소원자 1000개당 0.01내지 3개인 에틸렌과 α-올레핀 수지와의 사실상 선형 공중합체 또는 균질하게 측쇄된 선형 올레핀 수지를 함유하는 다층 차단 필름.
- 제1항에 있어서, 열 밀봉가능한 표층이 열가소성 폴리우레탄을 함유하고 에틸렌과 비닐 아세테이트와의 공중합체를 0 내지 10중량%포함하는 다층 차단 필름.
- 제1항에 있어서, 차단층이 비닐리덴 클로라이드의 단독 중합체, 비닐리덴 클로라이드와 비닐 클로라이드와의 공중합체 및 비닐리덴 클로라이드와 메틸 메타크릴레이트와의 공중합체로 이루어진 그룹으로부터 선택되는 다층 차단 필름.
- 제1항에 있어서, 산소 투과도가 90cc/㎡/dayㆍatm미만인 다층 차단 필름.
- 제1항에 있어서, 차단층이 2개의 열 밀봉가능한 표층들 사이에 위치하는 다층 차단 필름.
- 제6항에 있어서, 표층이 필름의 70중량%를 구성하고 수분 차단층이 필름의 30중량%를 구성하는 다층 차단 필름.
- 제1항에 있어서, 표층이 슬립 첨가제(slip additive)/차단방지제 패키지를 0.5 내지 5중량% 포함하는 다층 차단 필름.
- 제3항에 있어서, 표층이 에틸렌과 비닐 아세테이트와의 공중합체를 1 내지 10중량%포함하는 다층 차단 필름.
- 제1항에 있어서, 표층이, 밀도 범위가 0.87 내지 0.92gm/cc이고 장쇄 측쇄가 중합체 주쇄를 따라 탄소 원자 1,000개당 0.01 내지 3개인 에틸렌과 α-올레핀과의 사실상 선형 공중합체인 다층 차단 필름.
- 제10항에 있어서, 차단층과 표층 사이에 에틸렌과 비닐 아세테이트와의 공중합체의 중간 연결층을 포함하는 다층 차단 필름.
- 제1항에 있어서, 차단층이 비닐 클로라이드의 단독 중합체, 비닐리덴 클로라이드와 비닐 클로라이드와의 공중합체 또는 비닐리덴 클로라이드와 메틸 메타크릴레이트와의 공중합체 및 에틸렌과 비닐 아세테이트와의 공중합체 1 내지 6%를 함유하는 다층 차단 필름.
- 제1항에 있어서, 차단 필름이 차단 필름의 하나의 표면에 부착된 활성 약재를 함유하는 접착제(a)와 이러한 접착제에 인접해 있고 활성 약제가 환자의 피부로 조절되어 방출되도록 채택된 조절된 이형 막(release membrane)(b)을 추가로 포함하는 다층 차단 필름.
- 제13항에 있어서, 조절된 이형 막의 한 부분 이상에 부착되어 있는 접착제와 이러한 접착제와 약제의 피하 운반용 시스템을 형성하기 위한 이형 막을 덮는 이형 라이너(release liner)를 추가로 포함하는 다층 차단 필름.
- 제13항에 있어서, 하나 이상의 표층이 이의 가장자리를 따라 열 밀봉되어 백 또는 파우치(pouch)를 형성하는 다층 차단 필름.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12147493A | 1993-09-16 | 1993-09-16 | |
US08/216,903 | 1994-03-23 | ||
US08/216,903 US5567488A (en) | 1993-09-16 | 1994-03-23 | Multilayer barrier film for transdermal drug delivery system and ostomy applications |
US08/121,474 | 1994-03-23 | ||
PCT/US1994/009229 WO1995007816A1 (en) | 1993-09-16 | 1994-08-16 | Multilayer barrier film |
Publications (2)
Publication Number | Publication Date |
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KR960704707A true KR960704707A (ko) | 1996-10-09 |
KR100309363B1 KR100309363B1 (ko) | 2001-12-28 |
Family
ID=26819511
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019960701307A KR100309363B1 (ko) | 1993-09-16 | 1994-08-16 | 다층 차단 필름 |
Country Status (11)
Country | Link |
---|---|
US (1) | US5567488A (ko) |
EP (1) | EP0719210B1 (ko) |
JP (1) | JPH09502671A (ko) |
KR (1) | KR100309363B1 (ko) |
AT (1) | ATE188910T1 (ko) |
AU (1) | AU692179B2 (ko) |
CA (1) | CA2171966C (ko) |
DE (1) | DE69422722T2 (ko) |
DK (1) | DK0719210T3 (ko) |
ES (1) | ES2140556T3 (ko) |
WO (1) | WO1995007816A1 (ko) |
Families Citing this family (37)
Publication number | Priority date | Publication date | Assignee | Title |
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US5681627A (en) * | 1995-07-21 | 1997-10-28 | W. R. Grace & Co.-Conn. | Highly flexible multilayer films for various medical applications |
US5730736A (en) * | 1996-04-30 | 1998-03-24 | Dansac A/S | Ostomy appliance and contoured adhesive wafer therefor |
KR20000052857A (ko) | 1996-10-29 | 2000-08-25 | 크라이오백 인코포레이티드 | 알에프-밀봉가능한 필로우 파우치 |
US6185665B1 (en) * | 1997-02-28 | 2001-02-06 | Matsushita Electric Industrial Co., Ltd. | File management apparatus, file management method, and recording medium containing file management program |
CA2288548A1 (en) | 1998-12-11 | 2000-06-11 | Kimberly-Clark Worldwide, Inc. | Compositions of amorphous polyalphaolefin coatings on water-sensitive substrate |
US7063859B1 (en) | 1999-04-28 | 2006-06-20 | Noven Pharmaceuticals, Inc. | Barrier film lined backing layer composition and method for topical administration of active agents |
US6455161B1 (en) * | 1999-06-30 | 2002-09-24 | Dow Global Technologies Inc. | Essentially amorphous, non-chlorinated polymeric barrier films and method of using such films |
DE10007942A1 (de) * | 2000-02-22 | 2001-09-06 | Lohmann Therapie Syst Lts | Verpackung für wirkstoffhaltige Pflaster |
US20040139705A1 (en) * | 2000-03-14 | 2004-07-22 | Noven Pharmaceuticals, Inc. | Packaging materials for transdermal drug delivery systems |
CN1592704A (zh) * | 2001-11-17 | 2005-03-09 | 艾文蒂斯药品有限公司 | 吸附剂及其使用 |
US7025205B2 (en) * | 2002-06-26 | 2006-04-11 | Aventis Pharma Limited | Method and packaging for pressurized containers |
WO2005025549A2 (en) * | 2003-09-10 | 2005-03-24 | Noven Pharmaceuticals, Inc. | Multi-layer transdermal drug delivery device |
MEP23508A (en) * | 2003-10-28 | 2010-06-10 | Noven Pharma | Compositions and methods for comtrolling drug loss and delivery in transdermal drug delivery systems |
US20060122693A1 (en) * | 2004-05-10 | 2006-06-08 | Youssef Biadillah | Stent valve and method of manufacturing same |
US7819849B2 (en) | 2004-06-04 | 2010-10-26 | Hollister Incorporated | Laminated material and body wearable pouch formed therefrom |
JP4765277B2 (ja) * | 2004-07-30 | 2011-09-07 | 東ソー株式会社 | 積層体 |
US8343538B2 (en) * | 2004-10-08 | 2013-01-01 | Noven Pharmaceuticals, Inc. | Compositions and methods for controlling the flux of a drug from a transdermal drug delivery systems |
US7722929B2 (en) | 2005-08-18 | 2010-05-25 | Corning Incorporated | Sealing technique for decreasing the time it takes to hermetically seal a device and the resulting hermetically sealed device |
US20070040501A1 (en) | 2005-08-18 | 2007-02-22 | Aitken Bruce G | Method for inhibiting oxygen and moisture degradation of a device and the resulting device |
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DE3612160A1 (de) * | 1986-04-11 | 1987-10-15 | Wolff Walsrode Ag | Siegelbar, gereckte verbundfolien |
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US5271940A (en) * | 1989-09-14 | 1993-12-21 | Cygnus Therapeutic Systems | Transdermal delivery device having delayed onset |
EP0435792A3 (en) * | 1989-12-28 | 1991-11-06 | American National Can Company | Vinylidene chloride copolymer films |
US5300299A (en) * | 1991-07-22 | 1994-04-05 | Dow Corning Corporation | Silicone pressure sensitive adhesive containing alkylmethylsiloxane wax and related methods and devices |
DE69228827T2 (de) * | 1991-12-18 | 1999-10-21 | Minnesota Mining And Mfg. Co., Saint Paul | Mehrschichtige sperrstrukturen |
-
1994
- 1994-03-23 US US08/216,903 patent/US5567488A/en not_active Expired - Lifetime
- 1994-08-16 CA CA 2171966 patent/CA2171966C/en not_active Expired - Fee Related
- 1994-08-16 AU AU76880/94A patent/AU692179B2/en not_active Ceased
- 1994-08-16 DE DE69422722T patent/DE69422722T2/de not_active Expired - Lifetime
- 1994-08-16 WO PCT/US1994/009229 patent/WO1995007816A1/en active IP Right Grant
- 1994-08-16 AT AT94927172T patent/ATE188910T1/de not_active IP Right Cessation
- 1994-08-16 EP EP94927172A patent/EP0719210B1/en not_active Expired - Lifetime
- 1994-08-16 KR KR1019960701307A patent/KR100309363B1/ko not_active IP Right Cessation
- 1994-08-16 DK DK94927172T patent/DK0719210T3/da active
- 1994-08-16 JP JP50917995A patent/JPH09502671A/ja active Pending
- 1994-08-16 ES ES94927172T patent/ES2140556T3/es not_active Expired - Lifetime
Also Published As
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DK0719210T3 (da) | 2000-06-26 |
EP0719210B1 (en) | 2000-01-19 |
US5567488A (en) | 1996-10-22 |
CA2171966C (en) | 2004-08-31 |
ATE188910T1 (de) | 2000-02-15 |
AU7688094A (en) | 1995-04-03 |
CA2171966A1 (en) | 1995-03-23 |
AU692179B2 (en) | 1998-06-04 |
DE69422722T2 (de) | 2000-07-27 |
ES2140556T3 (es) | 2000-03-01 |
DE69422722D1 (de) | 2000-02-24 |
KR100309363B1 (ko) | 2001-12-28 |
WO1995007816A1 (en) | 1995-03-23 |
JPH09502671A (ja) | 1997-03-18 |
EP0719210A1 (en) | 1996-07-03 |
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