KR910002935A - 폴리이소시아네이트 (Polyisocyanate)의 제조방법 - Google Patents
폴리이소시아네이트 (Polyisocyanate)의 제조방법 Download PDFInfo
- Publication number
- KR910002935A KR910002935A KR1019890010397A KR890010397A KR910002935A KR 910002935 A KR910002935 A KR 910002935A KR 1019890010397 A KR1019890010397 A KR 1019890010397A KR 890010397 A KR890010397 A KR 890010397A KR 910002935 A KR910002935 A KR 910002935A
- Authority
- KR
- South Korea
- Prior art keywords
- isocyanurate
- diisocyanate
- producing
- polyisocyanate
- diol
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/62—Polymers of compounds having carbon-to-carbon double bonds
- C08G18/6216—Polymers of alpha-beta ethylenically unsaturated carboxylic acids or of derivatives thereof
- C08G18/622—Polymers of esters of alpha-beta ethylenically unsaturated carboxylic acids
- C08G18/6225—Polymers of esters of acrylic or methacrylic acid
- C08G18/6229—Polymers of hydroxy groups containing esters of acrylic or methacrylic acid with aliphatic polyalcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
- C07D251/34—Cyanuric or isocyanuric esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
- C08G18/4081—Mixtures of compounds of group C08G18/64 with other macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/791—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups
- C08G18/792—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups formed by oligomerisation of aliphatic and/or cycloaliphatic isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
- C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
- C08G18/8009—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203
- C08G18/8012—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203 with diols
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyurethanes Or Polyureas (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
내용 없음.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- 헥사메틸렌 디이소시아네이트를 주성분으로 하는 지방족 또는 지환식 디이소시아네이트 화합물을, 일반식단, 식중의 R1,R2및 R3는 각각 탄소원자수가 1~20인 탄화수소기, 또는 1개 이상의 복소원자를 함유하는 탄화 수소기를 표시하고, 또한 R1,R2및 R3중의 적어도 2개가 서로 연결된 것이어도 좋으며, 또한 R4는 수소원자 또는 탄소원자수가 1~20인 탄화수소기를 표시하고, R5,R6및 R7은, 각각 탄소원자수가 1~20인 탄화수소기를 표시함으로써 나타내어진 이소시아누레이트화 촉매의 존재하에 반응시키는 것을 특징으로 하는 이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제1항에 있어서, 상기 이소시아누레이트화 촉매는 투여된 디이소시아네이트 화합물의 투입증량에 대하여 20~200ppm의 범위 내에서 사용되는 것을 특징으로 하는 이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제1항에 있어서, 지방족 디이소시아네이트 화합물이 2,2,4-트리메틸헥사메틸렌 디이소시아네이트 및 도데카메틸렌 디이소시아네이트로 이루어진 군에서 선택되어진 적어도 1종의 화합물인 이소시아누레이트 폴리이소시아네이트의 제조방법.
- 제1항에 있어서, 상기 지환식 디이소시아네이트 화합물이, 1,4-시클로헥산디이소시아네이트 및 1,3-비스(이소시아네토메틸)-시클로헥산으로 이루어진 군에서 선택되어진 적어도 1종의 화합물인 이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제1항에 있어서, 상기 이소시아누레이트형 폴리이소시아네이트가 적어도 65 중량 %의 1핵체 폴리이소시아네이트를 함유하는 것인 이소시아네이트형 폴리이소시아네이트의 제조방법.
- 헥사메틸렌 디이소시아네이트를 주성분으로 하는 지방족 또는 지환족 디이소시아네이트 화합물을, (a)일반식 [1]단, 식중의 R1,R2및 R3는 각각 탄소원자수가 1~20인 탄화수소기, 또는 1개 이상의 복소원자를 함유하는 탄화 수소기를 표시하고, 또한 R1,R2및 R3중의 적어도 2개가 서로 연결된 것이어도 좋으며, 또한 R4는 수소원자 또는 탄화수소가 1~20인 탄화수소기를 표시하고, R5,R6및 R7은, 각각 탄소원자수가 1~20인 탄화수소기를 표시함. (b)탄화수소디올의 존재하에 반응시키는 것을 특징으로 하는 디올변성 이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제6항에 있어서, 상기 이소시아누레이트화 촉매는 투여된 디이소시아네이트 화합물의 투입중량에 대하여 20~200ppm의 범위내에서 사용되는 것을 특징으로 하는 디올변성 이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제6항에 있어서, 지방족 디이소시아네이트 화합물이 2,2,4-트리메틸헥사메틸렌 디이소시아네이트 및 도데카 메틸렌 디이소시아네이트로 이루어진 군에서 선택되어진 적어도 1종의 화합물인 디올 변성이소시아누레이트형 폴리이소시아네이트의 제조방법.
- 제6항에 있어서, 지환식 디이소시아네이트 화합물이, 1,4-시클로헥산 디이소시아네이트 및 1,3-비스(이소시아네이토메틸)-시클로헥산으로 이루어진 군에서 선택되어진 적어도 1종의 화합물인 디올변성 이소시아네이트형 폴리이소시아네이트의 제조방법.
- 제6항에 있어서, 디올변성 이소시아누레이트형 폴리이소시아네이트가 적어도 65중량 %인 1핵체 폴리이소시아네이트를 함유하는 것인 디올변성 이소시아누레이트형 폴리이소시아네이트의 제조방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP63181512A JP2770329B2 (ja) | 1988-07-22 | 1988-07-22 | ポリイソシアネートの製造方法 |
JP63-181512 | 1988-07-22 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR910002935A true KR910002935A (ko) | 1991-02-26 |
KR970009425B1 KR970009425B1 (ko) | 1997-06-13 |
Family
ID=16102058
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019890010397A KR970009425B1 (ko) | 1988-07-22 | 1989-07-22 | 폴리이소시아네이트(Polyisocyanate)의 제조방법 |
Country Status (5)
Country | Link |
---|---|
US (1) | US5070137A (ko) |
EP (1) | EP0351873B1 (ko) |
JP (1) | JP2770329B2 (ko) |
KR (1) | KR970009425B1 (ko) |
DE (1) | DE68924453T2 (ko) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5691440A (en) * | 1995-10-05 | 1997-11-25 | Arco Chemical Technonogy, L.P. | Catalyst and process for producing isocyanate trimers |
FR2770532B1 (fr) * | 1997-11-04 | 2000-01-21 | Rhodia Chimie Sa | Catalyseur de trimerisation d'isocyanates, a base d'un hydrogenocarbonate |
ZA9810038B (en) | 1997-11-04 | 2000-05-03 | Rhodia Chimie Sa | A catalyst and a method for the trimerization of isocyanates. |
DE19944373A1 (de) | 1999-09-16 | 2001-03-22 | Degussa | Katalysator und Verfahren zur Herstellung von farbreduzierten isocyanuratgruppenhaltigen Polyisocyananten |
DE10065176A1 (de) | 2000-12-23 | 2002-06-27 | Degussa | Katalysator und Verfahren zur Herstellung von niedrigviskosen und farbreduzierten isocyanuratgruppenhaltigen Polyisocyanaten |
DE10309432A1 (de) * | 2003-03-05 | 2004-09-16 | Degussa Ag | Verfahren zur Herstellung von geruchsarmen und lagerstabilen monomerhaltigen Polyisocyanuraten auf Basis von Isophorondiisocyanat |
DE10320266A1 (de) * | 2003-05-03 | 2004-11-18 | Degussa Ag | Feste Uretdiongruppenhaltige Polyurethan-Pulverlackzusammensetzungen bei niedriger Temperatur härtbar |
US7504523B2 (en) * | 2006-03-10 | 2009-03-17 | Basf Corporation | Uretonimine-modified isocyanate composition and method of forming the same |
US7541397B2 (en) * | 2006-03-10 | 2009-06-02 | Basf Corporation | Uretonimine-modified isocyanate composition and method of forming the same |
KR101503743B1 (ko) * | 2014-06-26 | 2015-03-19 | 애경화학 주식회사 | 이소시아누레이트형 폴리이소시아네이트의 제조방법 |
WO2020016119A1 (de) | 2018-07-16 | 2020-01-23 | Covestro Deutschland Ag | Verfahren zur oligomerisierung von isocyanaten mit polyedrischen silsesquioxan-katalysatoren |
JP7293762B2 (ja) * | 2019-03-19 | 2023-06-20 | 東ソー株式会社 | ポリイソシアネート組成物およびそれを用いた塗料組成物 |
CN111793182B (zh) * | 2020-07-15 | 2022-04-22 | 万华化学集团股份有限公司 | 一种多异氰酸酯组合物 |
CN115124483B (zh) * | 2022-06-02 | 2023-08-11 | 万华化学集团股份有限公司 | 一种改性异氰酸酯及一种聚脲弹性体 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2616415A1 (de) * | 1976-04-14 | 1977-11-03 | Basf Ag | Verfahren zur polymerisation von organischen diisocyanaten |
DE2916201A1 (de) * | 1979-04-21 | 1980-10-30 | Huels Chemische Werke Ag | Verfahren zur trimerisierung von diisocyanaten |
EP0155559A1 (en) * | 1984-02-29 | 1985-09-25 | Dainippon Ink And Chemicals, Inc. | Process for production of isocyanurate ring-containing polyisocyanate and resin composition for urethane paints comprising said polyisocyanate and acrylic polyol |
JPS61129173A (ja) * | 1984-11-19 | 1986-06-17 | Takeda Chem Ind Ltd | イソシアヌレ−ト環とイソシアナ−ト基とを有する化合物の製造法 |
JPH0678418B2 (ja) * | 1986-03-10 | 1994-10-05 | 大日本インキ化学工業株式会社 | 樹脂組成物 |
-
1988
- 1988-07-22 JP JP63181512A patent/JP2770329B2/ja not_active Expired - Fee Related
-
1989
- 1989-07-21 DE DE68924453T patent/DE68924453T2/de not_active Expired - Fee Related
- 1989-07-21 EP EP89113449A patent/EP0351873B1/en not_active Expired - Lifetime
- 1989-07-21 US US07/382,876 patent/US5070137A/en not_active Expired - Lifetime
- 1989-07-22 KR KR1019890010397A patent/KR970009425B1/ko not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
US5070137A (en) | 1991-12-03 |
EP0351873A3 (en) | 1991-08-28 |
DE68924453T2 (de) | 1996-04-18 |
EP0351873B1 (en) | 1995-10-04 |
JPH0232068A (ja) | 1990-02-01 |
JP2770329B2 (ja) | 1998-07-02 |
KR970009425B1 (ko) | 1997-06-13 |
DE68924453D1 (de) | 1995-11-09 |
EP0351873A2 (en) | 1990-01-24 |
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