KR880000492A - 블록공중합체 및 이것의 디아민전구체의 제조방법 - Google Patents
블록공중합체 및 이것의 디아민전구체의 제조방법 Download PDFInfo
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- KR880000492A KR880000492A KR1019870006248A KR870006248A KR880000492A KR 880000492 A KR880000492 A KR 880000492A KR 1019870006248 A KR1019870006248 A KR 1019870006248A KR 870006248 A KR870006248 A KR 870006248A KR 880000492 A KR880000492 A KR 880000492A
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- Prior art keywords
- radical
- diisocyanate
- carbon atoms
- alkylene
- phenyl
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
- C08G77/54—Nitrogen-containing linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/61—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/458—Block-or graft-polymers containing polysiloxane sequences containing polyurethane sequences
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
- Polyurethanes Or Polyureas (AREA)
- Adhesive Tapes (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (12)
- (1) 적어도 5,000의 분자량과 하기의 구조식(Ⅱ)으로 표시되는 디아민, (2) 하기의 구조식(Ⅲ)으로 표시되는 적어도 하나의 디이소시 아네이트 및 (3) 디아민, 디히드록시화합물 또는 이들의 혼합물로부터 선택된 95중량%까지의 사슬신장기를 중합시키고, 상기 디이소시아네이트에 대한 디아민의 몰비를 약 1 : 0.95내지 1 : 1.05의 범위내로 유지하는 것을 특징으로하는 하기구조식(Ⅰ)의 반복유닛으로 구성되는 유기폴리실록산-폴리우레아 블록공중합체의 제조방법.OCN-Z-NCO상기식중, 구조식(Ⅰ)에서의 Z는 페닐렌, 알킬렌, 알알킬렌 및 시클로알킬렌에서 선택된 이가라디칼이고, 구조식(Ⅲ)에서의 Z는 헥사메틸렌, 메틸렌 비스-(페닐렌), 테트라메틸렌, 이소포론, 시클로헥실렌 및 메틸렌 디시클로 헥실로 이루어진군에서 선택된 이가라디칼이고, Y는 1내지 10개의 탄소원자를 가지는 알킬렌 라디칼이고, R은 적어도 50%는 메틸이고, 그나머지는 2내지 12개의 탄소원자를 가지는 비닐렌라디칼, 페닐라디칼 또는 치환된 페닐라디칼이고, D는 수소, 1내지 10개의 탄소원자를 가지는 알킬라디칼 또는 Y를 포함하여 고리구조를 이루어 헤테로 사이클을 형성하는 알킬렌 라디칼 또는 페닐이고, B는 알킬렌, 알알킬렌, 시클로알킬렌, 페닐렌, 산화폴리에틸렌, 산화폴 리테트 라메틸렌, 폴리 카프로락톤, 이들의 화합물 등으로부터 선택된 2가 라디칼이고, A는 -O--또는(식중, G는 수소, 1내지 10개의 탄소원자를 가지는 알킬기, 페닐 또는 B를 포함하여 고리구조를 이루어 헤테로 사이클을 형성하는 알킬렌라디칼이다)로부터 선택된 이작용성기이고, n은 50 이상의 수이고, m은 0내지 약 25인 수이다.
- 제1항에 있어서, 상기 디이소시아네이트는 톨루엔 디이소시아테이트 및 P-페닐렌디이소 시아네이트에서 선택된 페닐렌디이소시아 네이트인것을 특징으로 하는 제조방법.
- 제1항에 있어서, 상기 디이소시아네이트는 헥사메틸렌디이소시아 네이트인 것을 특징으로 한는 제조방법.
- 제1항에 있어서, 상기 디이소시아네이트는 메틸렌비스페닐이소 시아네이트 및 테트라메틸크실렌 디이소 시아네이트에서 선택된 알알킬렌디이소 시아네이트인것을 특징으로 하는 제조방법.
- 제1항에 있어서, 상기 디이소시아네이트는 이소포론디이소시아네이트 및 메틸렌 디시클로헥실 디이소시아네이트에서부터 선택된 시클로 알킬렌 디이소 시아네이트인 것을 특징으로 하는 제조방법.
- (1) 반응조건하에서, (a) 하기의 구조식(Ⅴ)로 표시되는 아민작용성 엔드블록커, (b) 충분한 고리형실록산을 상기 아민작용성 엔드블록커와 반응시켜서 제조한 약 2,000미만의 분자량과 하기의 구조식(Ⅵ)를 가지는 저분자량의 유기폴리실록산디아민, (c) 촉매량의 테트라메틸암모늄 3-아미노프로필디메틸 실라놀레이트를 합성하고, (2) 상기 반응을 거의 모든 아민작용성엔드 블록커가 소비될때까지 계속하고, (3) 하기구조식(Ⅱ)로 표시되는 신규의 유기폴리실록산 디아민이 얻어질때까지 부가의 고리형 실록산을 첨가하는 것을 특징으로하는 적어도 5000의 분자량을 가지는 하기구조식(Ⅱ)의 유기폴리실록산디아민의 제조방법.상기식중, Y는 1내지 10개의 탄소원자를 가지는 알킬렌라디칼이고, R은 적어도 50%는 메틸이고, 그 나머지는 2내지 12개의 탄소원자를 가지는 비닐렌라디칼, 페닐라디칼, 또는 치환된 페닐라디칼이고, D는 수소, 1내지 10개의 탄소원자를 가지는 알킬라디칼 또는 Y를 포함하여 고리구조를 이루어 헤테로 사이클을 형성하는 알킬렌 라디칼 또는 페닐이고, X는 약 4내지 40의 수이다.
- 제6항에 있어서, 상기 촉매량은 얻어지는 상기 유기폴리실록산디아민의 약 0.05중량% 미만인것을 특징으로 하는 제조방법.
- 제6항에 있어서, 상기 촉매량은 얻어지는 상기 유기폴리실록산디아민의 약 0.005내지 약 0.03중량%인 것을 특징으로 하는 제조방법.
- 제6항에 있어서, 상기반응조건은 약 80℃ 내지 약 90℃의 반응온도범위, 약 5내지 7시간의 반응시간 및 상기부가의 고리형 실록산의 적가로 이루어지는 것을 특징으로 하는 제조방법.
- 제1항에서 제조된 블록공중합체를 포함하는 릴리이즈제.
- 제10항에 있어서, 상기 블록공중합체는 약 15%내지 약 70%의 경질분절체를 포함하는 것을 특징으로 하는 릴리이즈제.
- 전면과 후면을 가지는 이면부재, 상기 전면상의 압감접착제매스 및 제10항의 릴리이즈제를 포함하는 이면부재후면상의 저접착력이면 판으로 구성되는 것을 특징으로 하는 압감접착재.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR96017982A KR960009691B1 (en) | 1986-06-20 | 1996-05-27 | Organopolysiloxane-diamine precursors and method for producing the same |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US87691886A | 1986-06-20 | 1986-06-20 | |
US876,918 | 1986-06-20 | ||
US876918 | 1986-06-20 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR880000492A true KR880000492A (ko) | 1988-03-26 |
KR960009692B1 KR960009692B1 (ko) | 1996-07-23 |
Family
ID=25368825
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019870006248A KR960009692B1 (ko) | 1986-06-20 | 1987-06-19 | 블록 공중합체 및 이의 제조방법 |
Country Status (12)
Country | Link |
---|---|
EP (2) | EP0250248B1 (ko) |
JP (5) | JP2784761B2 (ko) |
KR (1) | KR960009692B1 (ko) |
AR (1) | AR244729A1 (ko) |
AU (1) | AU591989B2 (ko) |
BR (1) | BR8703101A (ko) |
CA (2) | CA1339226C (ko) |
DE (1) | DE3752135T2 (ko) |
ES (1) | ES2110391T3 (ko) |
HK (1) | HK1011036A1 (ko) |
TR (1) | TR24305A (ko) |
ZA (1) | ZA874414B (ko) |
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-
1987
- 1987-06-18 EP EP87305431A patent/EP0250248B1/en not_active Expired - Lifetime
- 1987-06-18 ZA ZA874414A patent/ZA874414B/xx unknown
- 1987-06-18 EP EP96107085A patent/EP0737700A3/en not_active Withdrawn
- 1987-06-18 ES ES87305431T patent/ES2110391T3/es not_active Expired - Lifetime
- 1987-06-18 AU AU74474/87A patent/AU591989B2/en not_active Expired
- 1987-06-18 DE DE3752135T patent/DE3752135T2/de not_active Expired - Lifetime
- 1987-06-19 JP JP62153199A patent/JP2784761B2/ja not_active Expired - Lifetime
- 1987-06-19 CA CA000540190A patent/CA1339226C/en not_active Expired - Fee Related
- 1987-06-19 BR BR8703101A patent/BR8703101A/pt not_active IP Right Cessation
- 1987-06-19 KR KR1019870006248A patent/KR960009692B1/ko not_active IP Right Cessation
- 1987-06-19 TR TR87/0419A patent/TR24305A/xx unknown
- 1987-06-19 AR AR87307927A patent/AR244729A1/es active
-
1996
- 1996-02-08 JP JP8022759A patent/JP2799381B2/ja not_active Expired - Lifetime
-
1997
- 1997-05-16 CA CA000617075A patent/CA1340655C/en not_active Expired - Fee Related
- 1997-06-10 JP JP9152301A patent/JP3024678B2/ja not_active Expired - Lifetime
-
1998
- 1998-01-14 JP JP10005855A patent/JP3075470B2/ja not_active Expired - Fee Related
- 1998-01-14 JP JP10005854A patent/JP2901236B2/ja not_active Expired - Lifetime
- 1998-11-13 HK HK98112001A patent/HK1011036A1/xx not_active IP Right Cessation
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6540314B1 (en) | 1998-10-27 | 2003-04-01 | Canon Kabushiki Kaisha | Ink tank, cartridge including the ink tank, and printing apparatus using the cartridge |
Also Published As
Publication number | Publication date |
---|---|
BR8703101A (pt) | 1988-03-08 |
JPS633029A (ja) | 1988-01-08 |
JP3075470B2 (ja) | 2000-08-14 |
EP0737700A2 (en) | 1996-10-16 |
DE3752135D1 (de) | 1997-12-11 |
JP2784761B2 (ja) | 1998-08-06 |
JPH10310628A (ja) | 1998-11-24 |
JP3024678B2 (ja) | 2000-03-21 |
TR24305A (tr) | 1991-08-01 |
DE3752135T2 (de) | 1998-04-16 |
EP0737700A3 (en) | 1996-12-18 |
JPH08231726A (ja) | 1996-09-10 |
EP0250248A3 (en) | 1989-04-12 |
JPH1060386A (ja) | 1998-03-03 |
AR244729A1 (es) | 1993-11-30 |
ES2110391T3 (es) | 1998-02-16 |
HK1011036A1 (en) | 1999-07-02 |
CA1339226C (en) | 1997-08-05 |
ZA874414B (en) | 1989-02-22 |
EP0250248A2 (en) | 1987-12-23 |
JPH10279915A (ja) | 1998-10-20 |
KR960009692B1 (ko) | 1996-07-23 |
AU591989B2 (en) | 1989-12-21 |
AU7447487A (en) | 1987-12-24 |
JP2799381B2 (ja) | 1998-09-17 |
CA1340655C (en) | 1999-07-13 |
EP0250248B1 (en) | 1997-11-05 |
JP2901236B2 (ja) | 1999-06-07 |
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