KR870001285A - 폴리 실록산-그래프트 공중합체 릴리이스 피복물을 함유한 시이트 물질 및 접착제 테이프 - Google Patents

폴리 실록산-그래프트 공중합체 릴리이스 피복물을 함유한 시이트 물질 및 접착제 테이프 Download PDF

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KR870001285A
KR870001285A KR1019860005799A KR860005799A KR870001285A KR 870001285 A KR870001285 A KR 870001285A KR 1019860005799 A KR1019860005799 A KR 1019860005799A KR 860005799 A KR860005799 A KR 860005799A KR 870001285 A KR870001285 A KR 870001285A
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엠. 클레멘스 라우렌스
클레멘스 라우렌스엠.
에스. 칸트너 스티븐
에이치. 마주레크 믹지슬라우
에이치 마주레크 믹지슬라우
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미네소타 마이닝 앤드 매뉴팩츄어링 컴패니
도날드 밀러 셀
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Abstract

내용 없음.

Description

폴리 실록산-그래프트 공중합체 릴리이스 피복물을 함유한 시이트 물질 및 접착제 테이프
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (27)

  1. 릴리이스 피복 조성물은 약 -20℃이상의 Tg 또는 Tm을 지닌 비닐 공중합성 벡본을 지녔으며, 약 1,000이상의 수평균 분자량을 지닌 1가의 실록산 중합체성 부를 상기 백본에 그래프트한 공중합체로 구성되며, 상기 공중합체에 그래프트된 부의 수 및 조성은 약 50N/100mm이하의 표면 릴리이스 값을 상기 공중합체에 제공할 수 있도록 조절되는 것을 특징으로 하는 가요성 시이트 및 적어도 한 표면을 덮고 있는 릴리이스 피복물로 구성된 피복 시이트 물질.
  2. 제1항에 있어서, 상기 공중합체는 A단량체 및 C단량체의 반복 단위 및 임의의 B단량체로 구성되며, 상기 A는 적어도 하나의 자유 라디칼성 중합성 비닐 단량체이며, B의 사용시 B는 A와 공중합 될수 있는 적어도 하나의 극성 단량체로서, B단량체는 모든 단량체의 충 중량에 대해 30%이하로 함유되어 있으며, C는 하기 구조식을 갖는 단량체이며, 상기 단량체들은 공중합화되어 그래프트된 C단량체를 지닌 중합체성 벡본을 형성하며 공중합체중의 C단량체의 함량 및 조성은 약 50N/100mm이하의 표면 릴리이스 값을 지닌 릴리이스 조성물이 제공되도록 선택되는 것을 특징으로 하는 피복 시이트 물질
    상기식에서, X는 A 및 B단량체와 공중합될 수 있는 비닐기이며; Y는 n이 0 또는 1일때 2가의 결합기이며; m은 1 내지 3의 정수이며; R은 수소, 저급알킬(예 : 메틸, 에틸 또는 프로필), 아릴(예 : 페닐 또는 치환 페닐)또는 알콕시이며; Z는 약 1000이상의 수평군 분자량을 갖는 1가의 실록산 중합체성 부로서, 실질적으로 공중합 조건하에서 비반응성이다.
  3. 제2항에 있어서, 상기 A단량체는 스티렌, 비닐 아세테이트, 비닐 클로라이드, 비닐리덴 클로라이드, 아크릴니트릴, 1 내지 18의 탄소원자를 지닌 비-3차 알콜의 아크릴산 또는 메타아크릴산 에스테르로 구성되는 그룹으로부터 선택되는 것을 특징으로 하는 피복 시이트 물질.
  4. 제3항에 있어서, 상기 비-3차 알콜은 메탄올, 에탄올, 프로판올, 이소프로판올, 부탄올, 이소부탄올 시클로헥산올, 벤젠 알콜, 도데칸올, 헥사데칸올 및 옥타데칸올으로 구성되는 그룹으로부터 선택되는 것을 특징으로 하는 피복 시이트 물질.
  5. 제1항에 있어서, 상기 중합체성 벡본은 폴리(메틸 메타아크릴레이트), 폴리(부틸 메타아크릴레이트), 폴리(비닐아세테이트), 부분적으로 가수 분해된 폴리(비닐 아세테이트) 및 폴리(옥소데실 아크릴레이트)로 구성되는 그룹으로부터 선택되는 것을 특징으로 하는 피복 시이트 물질.
  6. 제2항에 있어서, 상기 B단량체는 아크릴산, 메타아크릴산, 이타콘산, 아크릴아미드, 메타아크릴아미드, N,N-디메틸 아크릴아미드, 메타아크릴로니트릴, 및 말레인산 무수물로 구성되는 그룹으로부터 선택되는 것을 특징으로 하는 피복 시이트 물질.
  7. 제2항에 있어서, 상기 단량체는 상기 공중합체의 충중량에 대해 약 1 내지 10%로 포함되어 있는 것을 특징으로 하는 피복 시이트 물질.
  8. 제2항에 있어서, 상기 C단량체의 X기는 하기 구조식을 갖는 것을 특징으로 하는 피복 시이트 물질.
    상기식에서, R1은 수소원자 또는 COOH기이며, R2는 수소원자, 메틸기 또는 CH2COOH기이다.
  9. 제2항에 있어서, 상기 C단량체의 Z기는 하기 구조식을 갖는 것을 특징으로 하는 피복 시이트 물질.
    상기식에서, R3및 R5는 각각 저급알킬, 아릴 또는 플루오로알킬이며, R4는 알킬, 알콕시, 알킬아미노, 아릴, 히드록실 또는 플루오로알킬이며, r은 약 5 내지 700의 정수이다.
  10. 제2항에 있어서, 상기 C단량체는 하기 그룹으로부터 선택된 구조식을 갖는 것을 특징으로 하는 피복 시이트 물질.
    (p=0 또는 1, q=2-6의 정수);
    (p=0 또는 1, q=0-2의 정수);
    (q=2-6의 정수, R″=수소 또는 알킬);
    (R″=는 수소 또는 알킬)
    (q=2-6의 정수, R″=수소 또는 알킬).
  11. 제2항에 있어서, 상기 C단량체는 약 1,000 내지 50,000의 수 평균 분자량을 갖는 것을 특징으로 하는 피복 시이트 물질.
  12. 제2항에 있어서, 상기 C단량체는 약 5,000 내지 25,000의 수 평균 분자량을 갖는 것을 특징으로 하는 피복 시이트 물질.
  13. 제2항에 있어서, 상기 공중합체는 약 0.1 내지 20중량%의 C단량체를 함유하는 것을 특징으로 하는 피복 시이트 물질.
  14. 제2항에 있어서, 상기 공중합체는 약 0.01 내지 50중량%의 (B단량체+C단량체)를 함유하는 것을 특징으로 하는 피복 시이트 물질.
  15. 제1항에 있어서 가요성 시이트는 페이퍼, 패브릭, 필름-형성 중합체, 금속, 고무 및 세라믹으로 구성되는 그룹으로 부터 선택된 물질로 헝성되는 것을 특징으로 하는 피복 시이트 물질.
  16. 제1항에 있어서, 상기 피복물은 상기 가요성 시이트중 적어도 하나의 주 표면상에 피복되는 것을 특징으로 하는 피복 시이트 물질.
  17. (a) 가요성 베킹재; (b) 상기 베킹재의 하나의 구 표면을 피복하는 감압 접착제 피복물; (c) 약 -20。C이상의 Tg또는 Tm을 지닌 비닐 중합성 벡본을 지녔으며, 약 1,000이상의 수 평균 분자량을 지닌 1가의 실록산 중합체성 부가 상기 벡본에 그래프트된 공중합체로 구성되며, 공중합체에서 그래프트 부의 수 및 조성은 약 50N/10mm이하의 표면 릴리이스 값을 상기 공중합체에 제공하도록 조정된, 상기 베킹재의 반대편 표면에 피복된 릴리이스 피복물로 구성된, 로울형태의 감압 접착제 피복 테이프.
  18. 제17항에 있어서, 상기 공중합체는 공중합성의 반복성 A 및 C단량체와 임의의 B단량체로 구성되며 상기 A는 적어도 하나의 자유 라디칼성 중합성 비닐 단량체이며, B의 사용시 B는 A와 공중합 될수 있는 적어도 하나의 극성 단량체로서, B단량체는 모든 단량체의 총 중량에 대해 30% 이하로 함유되어 있으며, C는 하기 구조식을 갖는 단량체이며, 상기 단량체들은 공중합되어 그래프트된 C단량체를 지닌 증합체성 벡본을 형성하며 공중합체중의 C단량체의 함량 및 조성은 약 50N/100mm이하의 표면 릴리이스 값을 지닌 릴리이스 조성물이 제공되도록 선택되는 것을 특징으로 하는 로울형태의 감압 접착제 테이프
    상기식에서, X는 A 및 B단량체와 공중합 될수 있는 비닐기이며; Y는 n이 0 또는 1일때 2가의 결합기이며; m은 1 내지 3이 정수이며; R은 수소, 저급알킬(예 : 메틸, 에틸 또는 프로필), 아릴(예 : 페닐 또는 치환 페닐)또는 알콕시이며; Z는 약 1,000이상의 수 평균 분자량을 갖는 1가의 실록산 중합체성 부로서, 실질적으로 공중합 조건하에서 비반응성이다.
  19. (a) 가요성 베킹재; (b) 상기 베킹재의 하나의 주 표면을 피복하는 감압 접착제 피복물; (c) 약 -20℃이상의 Tg또는 Tm을 지닌 비닐 중합성 벡본을 지녔으며, 약 1,000이상의 수 평균 분자량을 지닌 1가의 실록산 중합체성 부가 상기 벡분이 그래프트된 공중합체로 구성되며, 공중합체서 그래프트 부의 수 및 조성은 약 50N/l00mm이하의 표면 릴리이스 값을 상기 공중합체에 제공하도록 조정된 릴리이스 피복물로 상기 감압 접착제 피복물이 부착된 주 표면상에 피복한 가요성 시이트로 구성된 릴리이스 라이너로 구성된 테이프.
  20. 제19항에 있어서, 상기 공중합체는 공중합체성의 반복성 A 및 C단량체와 임의의 B단량체로 구성되며, 상기 A는 적어도 하나의 자유 라디칼성 중합성 비닐 단량체이며, B의 사용시 B는 A와 공중합될 수 있는 적어도 하나의 극성 단량체로서, B단량체는 모든 단량체의 총 중량에 대해 30%이하로 함유되어 있으며, C는 하기 구조식을 갖는 단량체이며, 상기 단량체들은 공중합화되어 그래프트된 C단량체를 지닌 중합체성 벡분을 헝성하며 공중합체중의 C단량체의 함량 및 조성은 약 50N/100mm이하의 표면 릴리이스 값을 지닌 릴리이스 조성물이 제공되도록 선택되는 것을 특징으로 하는 테이프.
    상기식에서, X는 A 및 B단량체와 공중합될수 있는 비닐기이며; Y는 n이 0 또는 1일때 2가의 결합기이며; m은 1 내지 3의 정수이며; R은 수소, 저급 알킬(예 : 메틸, 에틸 또는 프로필), 아릴(예 : 페닐 또는 치환 페닐)또는 알콕시이며; Z는 약 1,000이상의 수 평균 분자량을 갖는 1가의 실록산 중합체성 부로서, 실질적으로 공중합 조건하에서 비반응성이다.
  21. 제1항에 있어서, 상기 공중합체는 교차 결합되는 것을 특징으로 하는 피복 시이트 물질.
  22. 제l7항에 있어서, 상기 공중합체는 교차 결합되는 것을 특징으로 하는 로울 형태의 감압 접착제 피복 테이프.
  23. 제19항에 있어서, 상기 공중합체는 교차 결합되는 젓을 특징으로 하는 테이프.
  24. 약 -20。C이상의 Tg또는 Tm을 지닌 비닐 공중합성 벡본을 지녔으며, 약 1,000이상의 수 평균 분자량을 지닌 1가의 실록산 중합체성 부를 상기 벡본이 그래프트한 공중합체로 구성되며, 상기 공중합체에 그래프트된 부의 수 및 조성은 약 50N/100mm이하의 표면 릴리이스 값을 상기 공중합체에 제공할 수 있도록 조절된 릴리이스 피복물로 피복된 적어도 하나의 릴리이스 라이너를 가지는 것을 특징으로 하는 릴리이스 라이너들 사이에 감압 접착제 필름을 포합한 트랜스퍼 테이프.
  25. 제24항에 있어서, 상기 공중합체는 공증합성의 반복성 A 및 C단량체와 임의의 B단량체로 구성되며, 상기 A는 적어도 하나의 극성단량체로서, B단량체는 모든 단량체의 총 중량에 대해 30%이하로 함유되어 있으며, C는 하기 구조식을 갖는 단량체이며, 상기 단량체들은 공중합화되어 그래프트된 C단량체를 지닌 중합체성 벡분을 형성하며 공중합체중의 C단량체의 함량 및 소정은 약 50N/100mm이하의 표면 릴리이스 값을 지닌 릴리이스 조성물이 제공되도톡 선택되는 것을 특징으로 하는 트랜스퍼 테이프.
    상기식에서, X는 A 및 B단량체와 공중합될수 있는 비닐기이며; Y는 n이 0 또는 1일때 2가의 결합기이며; m은 1 내지 3의 정수이며; R은 수소, 저급알킬(예 : 메틸, 에틸 또는 프로필), 아릴(예 : 페닐 또는 치환 페닐) 또는 알콕시이며; Z는 약 1,000이상의 수 평균 분자량을 갖는 1가의 실록산 중합체성 부로서, 실질적으로 공중합 조건하에서 비반응성이다.
  26. 제24항에 있어서, 상기 공중합체는 교차 결합되는 것을 특징으로 하는 트랜스퍼 테이프.
  27. 제1항에 있어서, 상기 릴리이스 피복물은 상기 공중합체와 또다른 중합체의 혼합물로 구성되는 것을 특징으로 하는 피복 시이트 물질.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019860005799A 1985-07-19 1986-07-18 폴리실록산-그래프트 공중합체 박리 피복물이 피복된 시이트 물질 및 접착 테이프 KR950009039B1 (ko)

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US4728571A (en) 1988-03-01
JP2537806B2 (ja) 1996-09-25
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EP0210041B1 (en) 1992-03-11
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