KR20220049717A - Method of extracting undiluted extract from camellia flower and camellia flower extract of the same - Google Patents
Method of extracting undiluted extract from camellia flower and camellia flower extract of the same Download PDFInfo
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Abstract
Description
본 발명은 저온 고속 추출법을 적용하여, 천연성분 주름개선과 노화방지와 미백과 향균효과를 발휘하는 동백나무 꽃 추출물을 제공하여서, 색소 침착을 방지하는 톤업 및 미백용, 수분층진하는 보습용, 노화방지용 또는 항균용 화장료 조성물, 특히 에센스 조성물을 제공할 수 있는, 동백나무 꽃 추출물 추출 방법 및 이에 의한 동백나무 꽃 추출물에 관한 것이다.The present invention provides a camellia flower extract that exhibits natural ingredient wrinkle improvement, anti-aging, and whitening and antibacterial effects by applying a low-temperature high-speed extraction method, for tone-up and whitening to prevent pigmentation, for moisturizing and aging It relates to a method for extracting a camellia flower extract, which can provide an antibacterial or antibacterial cosmetic composition, particularly an essence composition, and a camellia flower extract thereby.
동백나무(Camellia japonica L)는 동백나무과(Theaceae) 동백속(Camelliae)에 속하는 활엽상록수로 주로 관상수와 같은 원예자원으로, 종실은 고품질 지방이 함유되어 있어 전통적으로 식용유와 화장유의 원료로, 줄기는 고급 숯의 원료로 각각 이용되어 왔다.Camellia japonica L is a broad-leaved evergreen tree belonging to the Camellia family, Theaceae, and is mainly used as a horticultural resource such as ornamental trees. Each has been used as a raw material for high-quality charcoal.
또한, 동백꽃은 사찰에서 화전을 만들기 위해 사용하기도 하였고, 건조된 꽃잎을 토혈과 같은 증상에 처방하거나 이뇨작용을 위해 사용하기도 하였다.In addition, camellia flowers were used in temples to make hwajeon, and dried petals were prescribed for symptoms such as hematemesis or used for diuretic action.
이와 같이 동백은 예로부터 다양한 용도로 사용되었고, 근래 기능성차 및 화장품원료와 오일 등으로 개발된 바 있으나, 지금까지는 잎이나 종실을 이용한 것으로 나머지 부위에 대한 성분분석이나 생리활성에 대한 연구가 거의 전무한 실정이다.As such, camellia has been used for various purposes since ancient times, and has recently been developed as a functional tea, cosmetic ingredient, and oil. the current situation.
이에, 원가절감을 위해 첨가되는 유해성분 또는 합성첨가물의 함유없이, 동백나무 꽃을 추출하여 화장료 조성물을 제공할 수 있는 기술이 요구된다.Accordingly, there is a need for a technology capable of providing a cosmetic composition by extracting a camellia flower without containing harmful ingredients or synthetic additives added to reduce costs.
본 발명의 사상이 이루고자 하는 기술적 과제는, 저온 고속 추출법을 적용하여, 천연성분 주름개선과 노화방지와 미백과 향균효과를 발휘하는 동백나무 꽃 추출물을 제공하여서, 색소 침착을 방지하는 톤업 및 미백용, 수분층진하는 보습용, 노화방지용 또는 항균용 화장료 조성물, 특히 에센스 조성물을 제공할 수 있는, 동백나무 꽃 추출물 추출 방법 및 이에 의한 동백나무 꽃 추출물을 제공하는 데 있다.The technical problem to be achieved by the idea of the present invention is to provide a camellia flower extract that exhibits natural ingredient wrinkle improvement, anti-aging, whitening and antibacterial effects by applying a low-temperature and high-speed extraction method, thereby preventing pigmentation and for tone-up and whitening , To provide a moisturizing, anti-aging, or antibacterial cosmetic composition, especially an essence composition, for providing a moisturizing, anti-aging, or antibacterial cosmetic composition, a method for extracting a camellia flower extract, and a camellia flower extract thereby.
전술한 목적을 달성하고자, 본 발명은, 동백꽃 생체를 채취하고 동백꽃 시료를 세척하여 선별하는 원료선정 단계; 상기 선별된 동백꽃 시료의 물기를 제거한 후 세절하고 동결 건조하는 단계; 상기 동결 건조된 동백꽃 시료를 분쇄하여 중량부 100에 당류 50 내지 200 중량부를 첨가하여 발효숙성시키는 단계; 상기 발효숙성된 동백꽃 시료를 지방족알코올에 침지하는 단계; 상기 침지된 동백꽃 시료를 저온가압하고 농축하여 동백꽃 추출물을 추출하는 단계; 상기 동백꽃 추출물을 상분리하는 단계; 상기 상분리된 동백꽃 추출물을 여과하여 동백나무 꽃 추출물을 수득하는 단계; 및 화장수, 유액, 크림, 젤 또는 에센스로 이루어진 화장료 조성물 100 중량부에 상기 수득된 동백나무 꽃 추출물 0.001 내지 90 중량부를 혼합하고 포장용기에 주입하여 동백나무 꽃 추출물을 포장하는 단계;를 포함하는, 동백나무 꽃 추출물 추출 방법을 제공한다.In order to achieve the above object, the present invention, the raw material selection step of collecting a camellia flower living body and washing and selecting the camellia flower sample; removing moisture from the selected camellia flower sample, then shredding and freeze-drying; fermenting and aging the freeze-dried camellia flower sample by adding 50 to 200 parts by weight of sugar to 100 parts by weight; immersing the fermented and matured camellia flower sample in aliphatic alcohol; extracting the camellia flower extract by low-temperature pressurizing and concentrating the immersed camellia flower sample; phase-separating the camellia flower extract; filtering the phase-separated camellia flower extract to obtain a camellia flower extract; And 0.001 to 90 parts by weight of the obtained camellia flower extract mixed with 100 parts by weight of a cosmetic composition consisting of lotion, emulsion, cream, gel or essence, and injecting it into a packaging container to package the camellia flower extract; Containing, A method for extracting a camellia flower extract is provided.
여기서, 상기 동백꽃 시료를 10℃ 내지 30℃에서 100일 내지 200일 동안 발효숙성할 수 있다.Here, the camellia flower sample may be fermented and aged at 10° C. to 30° C. for 100 to 200 days.
또한, 상기 당류는 설탕, 과당, 포도당, 유당, 엿류, 당시럽류, 덱스트린 및 올리고당으로 이루어진 군에서 선택될 수 있다.In addition, the sugar may be selected from the group consisting of sugar, fructose, glucose, lactose, malt syrup, sugar syrup, dextrin, and oligosaccharide.
또한, 상기 화장수는, 정제수, 알코올, 보습제, 가용화제, 완충제, 향료, 착색제, 퇴색 방지제, 수렴제, 살균제, 활력제, 소염제 또는 미백제 중 2종 이상을 포함할 수 있다.In addition, the lotion may include two or more of purified water, alcohol, a moisturizing agent, a solubilizer, a buffering agent, a flavoring agent, a colorant, an anti-fading agent, an astringent, a sterilizing agent, an activating agent, an anti-inflammatory agent, or a whitening agent.
또한, 상기 에센스는 유제, 가용화제, 보습제, 물 또는 약제를 포함하고, 상기 유제는 올리브유, 동백유, 참기름, 해바라기유, 스위트아몬드유, 또는 호호바유의 천연 식물유와, 카프린산, 미리스틴산, 올레인산 또는 이소스테아린산의 지방산의 디글리세린 에스테르 또는 트리글리세린 에스테르 중 어느 하나 이상을 포함하고, 상기 가용화제는 글리세린지방산에스테르, 폴리글리세린지방산에스테르, 솔비탄지방산에스테르 및 모노스테아린산프로필렌 글리콜 등의 프로필렌글리콜지방산에스테르류, 글리세린, 디글리세린, 에틸렌글리콜, 프로필렌글리콜 또는 1,3－부틸렌글리콜의 다가알코올 중 어느 하나 이상을 포함하고, 상기 물은 증류수 또는 탈이온수를 포함하고, 상기 약제로는 살균제, 비타민류, 천연 액기스, 색소 또는 향료를 포함할 수 있다.In addition, the essence includes an emulsion, a solubilizer, a moisturizer, water or a pharmaceutical, and the emulsion is olive oil, camellia oil, sesame oil, sunflower oil, sweet almond oil, or natural vegetable oil of jojoba oil, capric acid, myristic acid, Contains at least one of diglycerin esters or triglycerin esters of fatty acids of oleic acid or isostearic acid, and the solubilizing agent is propylene glycol fatty acid esters such as glycerin fatty acid ester, polyglycerin fatty acid ester, sorbitan fatty acid ester, and propylene glycol monostearate contains any one or more of polyhydric alcohols such as glycerin, glycerin, diglycerin, ethylene glycol, propylene glycol, or 1,3-butylene glycol, the water includes distilled water or deionized water, and the drug includes a disinfectant, vitamins , natural extracts, colors or fragrances.
또한, 상기 침지된 동백꽃 시료를 열수추출하여 동백꽃 추출물을 추출하는 단계를 포함할 수 있다.In addition, it may include the step of extracting the camellia flower extract by hot water extraction of the immersed camellia flower sample.
한편, 본 발명은, 앞서 언급한 동백나무 꽃 추출물 추출 방법에 의해 추출된 동백나무 꽃 추출물을 제공한다.On the other hand, the present invention provides a camellia flower extract extracted by the aforementioned camellia flower extract extraction method.
본 발명에 의하면, 저온 고속 추출법을 적용하여, 천연성분 주름개선과 노화방지와 미백과 향균효과를 발휘하는 동백나무 꽃 추출물을 제공하여서, 색소 침착을 방지하는 톤업 및 미백용, 수분층진하는 보습용, 노화방지용 또는 항균용 화장료 조성물, 특히 에센스 조성물을 제공할 수 있는 효과가 있다.According to the present invention, by applying a low-temperature and high-speed extraction method to provide a camellia flower extract that exhibits natural ingredient wrinkle improvement, anti-aging, whitening and antibacterial effects, for tone-up and whitening to prevent pigmentation, and for moisturizing , there is an effect of providing a cosmetic composition for anti-aging or antibacterial, in particular an essence composition.
도 1은 본 발명의 실시예에 의한 동백나무 꽃 추출물 추출 방법의 개략적인 순서도를 도시한 것이다.
도 2는 도 1의 동백나무 꽃 추출물 추출 방법을 예시한 것이다.
도 3은 동백나무 꽃 추출물 추출 방법에 의한 동백나무 꽃 추출물의 효능을 예시한 것이다.1 shows a schematic flowchart of a method for extracting a camellia flower extract according to an embodiment of the present invention.
Figure 2 illustrates the extraction method of the camellia flower extract of Figure 1.
Figure 3 illustrates the efficacy of the camellia flower extract by the camellia flower extract extraction method.
이하, 첨부된 도면을 참조로 전술한 특징을 갖는 본 발명의 실시예를 더욱 상세히 설명하고자 한다.Hereinafter, embodiments of the present invention having the above-described characteristics with reference to the accompanying drawings will be described in more detail.
본 발명의 실시예에 의한 동백나무 꽃 추출물 추출 방법은, 동백꽃 생체를 선별하는 원료선정 단계(S110), 동백꽃 시료를 동결 건조하는 단계(S120), 동결 건조된 동백꽃 시료를 분쇄하고 당류를 첨가하여 발효숙성시키는 단계(S130), 발효숙성된 동백꽃 시료를 지방족알코올에 침지하는 단계(S140), 동백꽃 시료를 저온가압하고 농축하여 동백꽃 추출물을 추출하는 단계(S150), 동백꽃 추출물을 상분리하는 단계(S160), 동백꽃 추출물을 여과하여 동백나무 꽃 추출물을 수득하는 단계(S170), 및 화장료 조성물에 동백나무 꽃 추출물을 혼합하고 포장용기에 주입하여 동백나무 꽃 추출물을 포장하는 단계(S180)를 포함하여, 천연성분 주름개선과 노화방지와 미백과 향균효과를 발휘하는 동백나무 꽃 추출물을 제공하는 것을 요지로 한다.In the method for extracting camellia flower extract according to an embodiment of the present invention, the raw material selection step (S110) for selecting a living body of the camellia flower, the step of freeze-drying the camellia flower sample (S120), the freeze-dried camellia flower sample is crushed and sugar is added. Fermentation and aging (S130), immersing the fermented and matured camellia flower sample in aliphatic alcohol (S140), low-temperature pressurizing and concentrating the camellia flower sample to extract the camellia flower extract (S150), phase-separating the camellia flower extract (S160) ), filtering the camellia flower extract to obtain a camellia flower extract (S170), and mixing the camellia flower extract in a cosmetic composition and injecting it into a packaging container to package the camellia flower extract (S180), including, It aims to provide a camellia flower extract that exhibits natural wrinkle improvement, anti-aging, whitening and antibacterial effects.
이하, 도 1 내지 도 3을 참조하여, 전술한 구성의 동백나무 꽃 추출물 추출 방법을 상술하면 다음과 같다.Hereinafter, with reference to FIGS. 1 to 3 , the method of extracting the camellia flower extract of the above configuration will be described in detail as follows.
우선, 원료선정 단계(S110)에서는, 동백꽃 생체를 채취하고 동백꽃 시료를 흐르는 물에 깨끗하게 수회에 걸쳐 세척하여 이물질을 제거하여서 추출에 적합한 동백꽃을 선별한다.First, in the raw material selection step (S110), the camellia flower living body is collected, and the camellia flower sample is washed cleanly several times in running water to remove foreign substances to select a camellia flower suitable for extraction.
참고로, 동백나무는 차나무과(Theaceae)에 속하는 약용식물로서 약 200여 종이 알려져 있다. 이 중 약 70여종이 동백아속, 즉 동백(Camellia japonica)과 애기동백(C sasanqua)의 근연종이다. 한국, 특히 부산 동백섬에 자생하는 동백나무는 1종(Camellia japonica L)으로 동백나무과(Theaceae), 동백속(Camelliae)의 교목이다.For reference, about 200 species of camellia are known as medicinal plants belonging to the family Theaceae. Among them, about 70 species are related to the subgenus Camellia, that is, Camellia japonica and C sasanqua. The camellia tree, which grows wild in Korea, especially on Dongbaek Island in Busan, is one species (Camellia japonica L) and is an arboreal tree in the family Theaceae and the genus Camellia.
또한, 동백나무 꽃에는 항균, 항산화, 및 항염증 활성을 갖는 트리테르펜(triterpene), 플라보노이드, 탄닌 및 지방산이 함유되어 있는 것으로 알려져 있고, 오래전부터 민간에서 출혈과 염증 등의 질환을 치료하는데 사용해왔을 뿐만 아니라, 동백나무 추출물이 혈중 요산 농도를 저하시키는 기능을 가져서, 동백나무를 식품소재 또는 건강보조식품으로 개발하여 상품화하기도 한다.In addition, camellia flowers are known to contain triterpenes, flavonoids, tannins and fatty acids with antibacterial, antioxidant, and anti-inflammatory activities, and have been used in folklore for a long time to treat diseases such as bleeding and inflammation. In addition, camellia extract has the function of lowering the concentration of uric acid in the blood, so it is developed and commercialized as a food material or health supplement.
다음, 동결 건조 단계(S120)에서는, 앞서 선별된 동백꽃 시료의 물기를 제거한 후 세절하고 동결건조기를 이용하여 급속 동결 건조하여 성분변질없이 일정기간동안 저장하도록 한다.Next, in the freeze-drying step (S120), after removing the moisture of the previously selected camellia flower sample, it is chopped and then freeze-dried using a freeze-dryer to store it for a certain period of time without changing the ingredients.
다음, 발효숙성 단계(S130)에서는, 앞서 동결 건조된 동백꽃 시료를 분쇄하여 중량부 100에 당류 50 내지 200 중량부를 첨가하여 발효숙성시킨다.Next, in the fermentation and aging step (S130), the previously freeze-dried camellia flower sample is crushed and fermented and aged by adding 50 to 200 parts by weight of sugar to 100 parts by weight.
여기서, 동백꽃 시료를 10℃ 내지 30℃에서 100일 내지 200일 동안 발효숙성할 수 있다.Here, the camellia flower sample may be fermented and aged at 10° C. to 30° C. for 100 to 200 days.
한편, 당류로는 설탕, 과당, 포도당, 유당, 엿류, 당시럽류, 덱스트린 및 올리고당으로 이루어진 군에서 선택될 수 있다.Meanwhile, as the saccharide, it may be selected from the group consisting of sugar, fructose, glucose, lactose, syrup, sugar syrup, dextrin, and oligosaccharide.
다음, 침지 단계(S140)에서는, 앞서 발효숙성된 동백꽃 시료를 지방족알코올에 냉침 또는 온침의 방법으로 침지하여(immerse), DPPH(1,1-diphenyl-2-picryl hydrazyl) 라디칼 소거활성를 수행할 수 있다.Next, in the immersion step (S140), the previously fermented and matured camellia flower sample is immersed in aliphatic alcohol by cold or warm immersion, and DPPH (1,1-diphenyl-2-picryl hydrazyl) radical scavenging activity can be performed. there is.
다음, 동백꽃 추출물 추출 단계(S150)에서는, 앞서 침지된 동백꽃 시료를 5℃ 이하에서 저온가압하고 농축하여 동백꽃 추출물을 초고속 용매 추출한다(high-speed essence undiluted solution extraction).Next, in the camellia flower extract extraction step (S150), the previously immersed camellia flower sample is pressurized at a low temperature below 5° C. and concentrated to extract the camellia flower extract with high-speed solvent extraction (high-speed essence undiluted solution extraction).
또는, 저온가압추출을 대체하여, 침지된 동백꽃 시료를 열수추출하여 동백꽃 추출물을 추출하는 단계(S155)를 포함할 수 있다. 여기서, 동백꽃 시료를 에탄올에 5시간 동안 가열용 맨틀(heating mentle)에서 열수추출하고 필터 페이퍼를 여과하여 감압농축할 수도 있다.Alternatively, in place of the low-temperature pressure extraction, hot water extraction of the immersed camellia flower sample may include the step of extracting the camellia flower extract (S155). Here, the camellia flower sample may be extracted with hot water in a heating mantle for 5 hours in ethanol and concentrated under reduced pressure by filtering filter paper.
한편, 열수추출 이외에, 초음파 추출법 또는 환류 냉각 추출법이 적용될 수도 있다.On the other hand, in addition to hot water extraction, ultrasonic extraction method or reflux cooling extraction method may be applied.
다음, 상분리 단계(S160)에서는 동백꽃 추출물을 가라앉는 성분과 뜨는 성분으로 또는 순수 동백꽃 추출물과 잔여 고형물을 상분리한다.Next, in the phase separation step (S160), the camellia flower extract is phase-separated into a sinking component and a floating component or a pure camellia flower extract and the remaining solids.
다음, 동백나무 꽃 추출물 수득 단계(S170)에서는, 앞서 상분리된 동백꽃 추출물을 필터 페이터를 통해 여과하여 순수 액상인 동백나무 꽃 추출물을 수득한다.Next, in the step of obtaining a camellia flower extract (S170), the phase-separated camellia flower extract is filtered through a filter paper to obtain a pure liquid camellia flower extract.
다음, 동백나무 꽃 추출물 포장 단계(S180)에서는, 화장수, 유액, 크림, 젤 또는 에센스로 이루어진 화장료 조성물 100 중량부에 수득된 동백나무 꽃 추출물 0.001 내지 90 중량부를 혼합하고 포장용기에 주입한다.Next, in the camellia flower extract packaging step (S180), 0.001 to 90 parts by weight of the obtained camellia flower extract is mixed with 100 parts by weight of the cosmetic composition consisting of lotion, milky lotion, cream, gel or essence and injected into a packaging container.
여기서, 화장수는, 각질층에 수분을 공급하기 위한 정제수, 유용성 성분을 용해하고 살균하여 청량을 제공하기 위한 알코올, 수분 증발을 억제하는 보습제, 가용화제, 완충제, 향을 부가하기 위한 향료, 착색제, 자외선을 흡수하여 퇴색 또는 변색을 방지하기 위한 퇴색 방지제, 수렴제, 미생물을 억제하여 부패를 방지하기 위한 살균제, 활력제, 소염제, 또는 미색 화이트닝 또는 톤업을 위한 미백제 중 2종 이상을 포함할 수 있다.Here, the lotion includes purified water for supplying moisture to the stratum corneum, alcohol for dissolving and sterilizing oil-soluble components to provide a refreshing feeling, a humectant for suppressing water evaporation, solubilizer, buffering agent, fragrance for adding fragrance, colorant, ultraviolet rays It may contain two or more of an anti-fading agent for preventing fading or discoloration, an astringent, a bactericide, an energizer, an anti-inflammatory agent, or a whitening agent for whitening or tone-up by inhibiting microorganisms to prevent decay.
예컨대, 에센스는 유제, 가용화제, 보습제, 물 또는 약제를 포함하고, 유제는 올리브유, 동백유, 참기름, 해바라기유, 스위트아몬드유, 또는 호호바유의 천연 식물유와, 카프린산, 미리스틴산, 올레인산 또는 이소스테아린산의 지방산의 디글리세린 에스테르 또는 트리글리세린 에스테르 중 어느 하나 이상을 포함하고, 가용화제는 글리세린지방산에스테르, 폴리글리세린지방산에스테르, 솔비탄지방산에스테르 및 모노스테아린산프로필렌 글리콜 등의 프로필렌글리콜지방산에스테르류, 글리세린, 디글리세린, 에틸렌글리콜, 프로필렌글리콜 또는 1,3－부틸렌글리콜의 다가알코올 중 어느 하나 이상을 포함하고, 물은 증류수 또는 탈이온수를 포함하고, 약제로는 살균제, 비타민류, 천연 액기스, 색소 또는 향료를 포함할 수 있다.For example, the essence includes an emulsion, a solubilizer, a moisturizing agent, water, or a pharmaceutical, and the emulsion includes a natural vegetable oil of olive oil, camellia oil, sesame oil, sunflower oil, sweet almond oil, or jojoba oil, capric acid, myristic acid, oleic acid or Propylene glycol fatty acid esters such as glycerin fatty acid ester, polyglycerol fatty acid ester, sorbitan fatty acid ester and propylene glycol monostearate, glycerin, including at least one of diglycerin ester or triglycerin ester of fatty acid of isostearic acid , Diglycerin, ethylene glycol, propylene glycol, or any one or more polyhydric alcohols of 1,3-butylene glycol, water includes distilled water or deionized water, and pharmaceuticals include disinfectants, vitamins, natural extracts, pigments Or it may contain a fragrance.
한편, 본 발명은, 앞서 언급한 동백나무 꽃 추출물 추출 방법에 의해 추출된 동백나무 꽃 추출물을 제공할 수 있다.On the other hand, the present invention can provide a camellia flower extract extracted by the aforementioned camellia flower extract extraction method.
이에, 전술한 바와 같은 구성의 동백나무 꽃 추출물 추출 방법 및 이에 의한 동백나무 꽃 추출물에 의해서, 저온 고속 추출법을 적용하여, 천연성분 주름개선과 노화방지와 미백과 향균효과를 발휘하는 동백나무 꽃 추출물을 제공하여서, 도 3에 예시된 바와 같이, 색소 침착을 방지하는 톤업 및 미백용, 수분층진하는 보습용, 노화방지용 또는 항균용 화장료 조성물, 특히 에센스 조성물을 제공할 수 있다.Accordingly, by applying the low-temperature and high-speed extraction method by the camellia flower extract extraction method having the composition as described above and the camellia flower extract by this method, the natural ingredient wrinkle improvement, anti-aging, and whitening and antibacterial effects are achieved. By providing, as exemplified in FIG. 3, it is possible to provide a cosmetic composition for tone-up and whitening that prevents pigmentation, for moisturizing, anti-aging or antibacterial, in particular an essence composition.
본 명세서에 기재된 실시예와 도면에 도시된 구성은 본 발명의 가장 바람직한 일 실시예에 불과할 뿐이고, 본 발명의 기술적 사상을 모두 대변하는 것은 아니므로, 본 출원 시점에 있어서 이들을 대체할 수 있는 다양한 균등물과 변형예들이 있을 수 있음을 이해하여야 한다.The embodiments described in this specification and the configurations shown in the drawings are only the most preferred embodiment of the present invention, and do not represent all of the technical spirit of the present invention, so various equivalents that can be substituted for them at the time of the present application It should be understood that there may be water and variations.
S110 : 원료선정 단계
S120 : 동결 건조 단계
S130 : 발효 숙성 단계
S140 : 침지 단계
S150 : 동백꽃 추출물 추출 단계
S155 : 열수추출 단계
S160 : 상분리 단계
S170 : 동백나무 꽃 추출물 수득 단계
S180 :: 동백나무 꽃 추출물 포장 단계S110: raw material selection step
S120: freeze drying step
S130: Fermentation ripening stage
S140: immersion step
S150: Camellia flower extract extraction step
S155: hot water extraction step
S160: phase separation step
S170: Camellia flower extract obtaining step
S180 :: Camellia Flower Extract Packaging Step
Claims (7)
상기 선별된 동백꽃 시료의 물기를 제거한 후 세절하고 동결 건조하는 단계;
상기 동결 건조된 동백꽃 시료를 분쇄하여 중량부 100에 당류 50 내지 200 중량부를 첨가하여 발효숙성시키는 단계;
상기 발효숙성된 동백꽃 시료를 지방족알코올에 침지하는 단계;
상기 침지된 동백꽃 시료를 저온가압하고 농축하여 동백꽃 추출물을 추출하는 단계;
상기 동백꽃 추출물을 상분리하는 단계;
상기 상분리된 동백꽃 추출물을 여과하여 동백나무 꽃 추출물을 수득하는 단계; 및
화장수, 유액, 크림, 젤 또는 에센스로 이루어진 화장료 조성물 100 중량부에 상기 수득된 동백나무 꽃 추출물 0.001 내지 90 중량부를 혼합하고 포장용기에 주입하여 동백나무 꽃 추출물을 포장하는 단계;를 포함하는, 동백나무 꽃 추출물 추출 방법.
a raw material selection step of collecting the camellia flower living body and washing and selecting the camellia flower sample;
removing moisture from the selected camellia flower sample, then shredding and freeze-drying;
fermenting and aging the freeze-dried camellia flower sample by adding 50 to 200 parts by weight of sugar to 100 parts by weight;
immersing the fermented and matured camellia flower sample in aliphatic alcohol;
extracting the camellia flower extract by low-temperature pressurizing and concentrating the immersed camellia flower sample;
phase-separating the camellia flower extract;
filtering the phase-separated camellia flower extract to obtain a camellia flower extract; and
A step of mixing 0.001 to 90 parts by weight of the obtained camellia flower extract to 100 parts by weight of a cosmetic composition consisting of a lotion, emulsion, cream, gel or essence, and injecting it into a packaging container to package the camellia flower extract; containing, camellia Tree Flower Extract Extraction Method.
상기 동백꽃 시료를 10℃ 내지 30℃에서 100일 내지 200일 동안 발효숙성하는 것을 특징으로 하는, 동백나무 꽃 추출물 추출 방법.
According to claim 1,
A method for extracting camellia flower extract, characterized in that the camellia flower sample is fermented and aged at 10° C. to 30° C. for 100 to 200 days.
상기 당류는 설탕, 과당, 포도당, 유당, 엿류, 당시럽류, 덱스트린 및 올리고당으로 이루어진 군에서 선택되는 것을 특징으로 하는, 동백나무 꽃 추출물 추출 방법.
According to claim 1,
The sugar, fructose, glucose, lactose, syrup, sugar syrup, dextrin and oligosaccharide, characterized in that selected from the group consisting of, Camellia flower extract extraction method.
상기 화장수는, 정제수, 알코올, 보습제, 가용화제, 완충제, 향료, 착색제, 퇴색 방지제, 수렴제, 살균제, 활력제, 소염제 또는 미백제 중 2종 이상을 포함하는 것을 특징으로 하는, 동백나무 꽃 추출물 추출 방법.
According to claim 1,
The lotion is purified water, alcohol, moisturizing agent, solubilizer, buffering agent, flavoring agent, colorant, anti-fading agent, astringent, bactericidal agent, activating agent, anti-inflammatory agent or whitening agent, characterized in that it contains two or more kinds of, camellia flower extract extraction method .
상기 에센스는 유제, 가용화제, 보습제, 물 또는 약제를 포함하고,
상기 유제는 올리브유, 동백유, 참기름, 해바라기유, 스위트아몬드유, 또는 호호바유의 천연 식물유와, 카프린산, 미리스틴산, 올레인산 또는 이소스테아린산의 지방산의 디글리세린 에스테르 또는 트리글리세린 에스테르 중 어느 하나 이상을 포함하고,
상기 가용화제는 글리세린지방산에스테르, 폴리글리세린지방산에스테르, 솔비탄지방산에스테르 및 모노스테아린산프로필렌 글리콜 등의 프로필렌글리콜지방산에스테르류, 글리세린, 디글리세린, 에틸렌글리콜, 프로필렌글리콜 또는 1,3－부틸렌글리콜의 다가알코올 중 어느 하나 이상을 포함하고,
상기 물은 증류수 또는 탈이온수를 포함하고,
상기 약제로는 살균제, 비타민류, 천연 액기스, 색소 또는 향료를 포함하는 것을 특징으로 하는, 동백나무 꽃 추출물 추출 방법.
According to claim 1,
The essence includes an emulsion, a solubilizer, a humectant, water or a pharmaceutical,
The emulsion is olive oil, camellia oil, sesame oil, sunflower oil, sweet almond oil, or natural vegetable oil of jojoba oil, capric acid, myristic acid, oleic acid or isostearic acid of a fatty acid of diglycerin ester or triglycerin ester of any one or more including,
The solubilizing agent is glycerin fatty acid ester, polyglycerol fatty acid ester, sorbitan fatty acid ester, and propylene glycol fatty acid esters such as propylene glycol monostearate, glycerin, diglycerin, ethylene glycol, propylene glycol or 1,3-butylene glycol polyvalent containing any one or more of alcohol,
The water includes distilled water or deionized water,
The method of extracting camellia flower extract, characterized in that it includes a bactericide, vitamins, natural extracts, colorants or fragrances as the pharmaceutical.
상기 침지된 동백꽃 시료를 열수추출하여 동백꽃 추출물을 추출하는 단계를 포함하는 것을 특징으로 하는, 동백나무 꽃 추출물 추출 방법.
According to claim 1,
Camellia flower extract extraction method, characterized in that it comprises the step of extracting the camellia flower extract by hot water extraction of the immersed camellia flower sample.
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