KR20160142106A

KR20160142106A - Sweetening composition with regular ratio of components and preparation method thereof

Info

Publication number: KR20160142106A
Application number: KR1020150078037A
Authority: KR
Inventors: 김고은; 박성원; 류경헌; 박종진
Original assignee: 주식회사 삼양사
Priority date: 2015-06-02
Filing date: 2015-06-02
Publication date: 2016-12-12
Also published as: KR101784462B1

Abstract

More particularly, the present invention relates to a granular or powder-like sweetening composition having xylitol and sugar distributed in a uniform composition ratio, and a method for producing the same.

Description

TECHNICAL FIELD The present invention relates to a composition having a uniform composition and a method for preparing the composition.

More particularly, the present invention relates to a composition for granular or powdery feeling, in which xylitol and sugar are distributed in a uniform composition ratio, and a method for producing the same.

Sugar, a widely used sweetener in the food industry, has excellent sweetness and sweetness, and has been added to various foods and processed foods from the past to be a favorite sweetener for improving the taste and taste of food. However, recently, as the harmfulness of sugar continues to be revealed, various problems are being raised. Specifically, excessive intake of sugar is pointed out as a major cause of various lifestyle diseases such as cavities, obesity and diabetes, and the necessity of development of substitute sweeteners is increasing worldwide.

As a result, various sweeteners capable of replacing sugar have been studied, and moreover, studies have been actively made on methods for reducing saccharides so as not to overdose them even if they are consumed with sugar.

Xylitol is a natural sweetener extracted from plants. It has sweetness and sugar content similar to sugar, and is a sweetener that has recently attracted attention as a substitute for sugar in the food industry. Xylitol, which acts as a sweetener almost identical to sugar, has a refreshing effect that refreshes the mouth, promoting saliva secretion, inhibiting plaque formation and acid production in the oral cavity, inhibiting the growth of tooth decay and reducing the risk of tooth decay . In addition, insulin action to promote the secretion of insulin action into the cells do not affect the blood sugar, such as the characteristics of diabetes patients for medical purposes as a substitute for glucose is also used for energy supply purposes.

As described above, a technique for preparing sugar, xylitol and mixed sugar by replacing a part of xylitol sucrose which can be used for sugar substitute is being developed.

One example of a method for producing a mixed sugar is a method of adding xylose to sugar, and a method of simply " mixing " sugar with a crystalline form and xylose in a powder form can be noted at first. However, in a granular or powdery food composition in which two or more components are mixed, 'whether or not the ingredients are homogeneously mixed' and 'whether to re-isolate after mixing' is a very important problem. In the case of mixed saccharide products, overall unevenness or re-separation occurs, so that when a specific component is distributed in a specific region and a large amount of other components are distributed in another region, the intended compounding ratio can not be achieved as a whole, Lt; / RTI >

Thus, the problem of maintaining a uniform mixing ratio of each component and preventing the re-separation is an important problem in the production of a granular or powdery product, and a solution to such a problem must be accompanied thereby to enable distribution as a granular or powdery food .

1) Korean Patent Publication No. 2014-7016103 2) Korean Patent Publication No. 2007-0058993 3) Korean Patent Publication No. 2011-0047178

It is an object of the present invention to provide a composition containing xylitol and sugar in which a xylitol and a sugar composition ratio are uniformly distributed in any portion in a granular and / have.

The present invention provides a chewing composition having sugar and xylitol distributed in a uniform composition ratio and a method for producing the same.

First, there is provided a process for preparing a toning composition comprising a solid phase mixing step of sugar and xylitol and a part of liquid phase spray coating step.

More specifically, the method for preparing the composition for emulsification comprises

1) solid phase mixing step of solid phase mixing all the sugar, part of xylitol or part of sugar and xylitol, based on the sugar and xylitol content in the final gum composition; And

2) a part of the liquid phase spray coating step of spraying (spraying) the coating solution containing the part of xylitol used in the solid phase mixing step or the residual amount of xylitol or the remaining amount of sugar excluding the sugar portion to the solid phase mixing step

. &Lt; / RTI >

The composition for warming may include sugar and xylitol as essential constituents. Although the blending ratio between sugar and xylitol in the composition for warming is not particularly limited, when xylitol is contained in an excess amount, it may affect the sensory properties of the composition for the warming and cause diarrhea when xylitol is ingested in too much amount It is possible. Therefore, considering the sensory aspect and the physiological effect, the mixing ratio (mixing ratio or content ratio) of sugar and xylitol in the sweetening composition is about 1: 0.05 to 1: 0.5, 1: 0.05 to 1: 0.1 to 1: 0.5, 1: 0.1 to 1: 0.3, 1: 0.15 to 1: 0.5, 1: 0.15 to 1: 0.3, 1: 0.2 to 1: 0.5, Content (weight): xylitol content (weight)).

The content of the chewing composition, sugar, and xylitol described in the present specification refers to the content of the solid component from which the solvent component is removed, unless otherwise specified.

The above 1) some solid-phase mixing steps may be performed in a food preparation mixer or a drier such as a fluidized bed granulator dryer, a granulator, a coater or the like capable of liquid spraying. The mixing can be performed by a conventional solid-phase mixing method such as fluidization, stirring, and the like.

In the above 1) in some solid phase mixing steps, the term "solid phase mixing" means that each component to be mixed is mixed in a solid state such as a powder phase and / or a granular phase, not a liquid phase. The term " powdery "and" granular phase "can be used to mean strictly different particle sizes (for example, the average particle size in the powder phase ranges from 10 to 700 μm and the granular phase ranges from 30 to 1000 μm) In this specification, both terms are meant to refer to solid particles, unless otherwise specified, and can be used interchangeably.

The sugar and xylitol used in the above 1) some solid phase mixing steps are all solid phase particles (powdery or granular). For example, in the case of sugar, the average particle size is about 200 to about 800 μm, and in the case of xylitol, the average particle size is 300 to 800 μm, but the present invention is not limited thereto.

In the 2) liquid phase spray coating step, the remaining amount of xylitol or the residual amount of sugar contained in the coating solution used for coating the solid phase particles in the liquid phase spraying is 1 to 10% by weight, 1 to 9% by weight 1 to 8%, 1 to 7%, 1 to 6%, 1 to 5%, 2 to 10%, 2 to 9%, 2 to 8%, 2 to 7% 3 to 8 wt%, 3 to 7 wt%, 3 to 6 wt%, 3 to 5 wt%, 4 to 8 wt%, and 2 to 6 wt%, 2 to 5 wt%, 3 to 10 wt%, 3 to 9 wt% 4 to 9% by weight, 4 to 8% by weight, 4 to 7% by weight, 4 to 6% by weight, or 4 to 5% by weight.

In another example, the remaining amount of xylitol or the residual amount of sugar contained in the coating solution may be expressed based on the total content of xylitol or the total content of sugar contained in the final gum composition. For example, in the case of partially coating xylitol, the remaining amount of xylitol contained in the coating solution may be in the range of 4.6 to 46 wt%, 4.6 to 41.4 wt%, 4.6 to 36.8 wt% based on the total content of xylitol contained in the final chewing composition, 4.6 to 32.6 wt.%, 4.6 to 27.6 wt.%, 4.6 to 23 wt.%, 9.2 to 46 wt.%, 9.2 to 41.4 wt.%, 9.2 to 36.8 wt.%, 9.2 to 32.2 wt.%, 9.2 to 27.6 wt.%, 13.8 to 32.4 wt.%, 13.8 to 27.6 wt.%, 13.8 to 23 wt.%, 18.4 to 46 wt.%, 18.4 to 41.4 wt.% %, 18.4 to 36.8 wt.%, 18.4 to 32.2 wt.%, 18.4 to 27.6 wt.%, Or 18.4 to 23 wt.%. In addition, when the sugar is partially coated, the remaining amount of the sugar contained in the coating solution is 1.3 to 13% by weight, 1.3 to 11.7% by weight, 1.3 to 10.4% by weight based on the total amount of the sugar contained in the final toning composition, 2.6 to 9.7 wt%, 1.3 to 7.8 wt%, 1.3 to 6.5 wt%, 2.6 to 13 wt%, 2.6 to 11.7 wt%, 2.6 to 10.4 wt%, 2.6 to 9.7 wt%, 2.6 to 7.8 wt% 3.9 to 9.7 wt.%, 3.9 to 7.8 wt.%, 3.9 to 6.5 wt.%, 5.2 to 13 wt.%, 5.2 to 11.7 wt.%, , 5.2 to 10.4 wt%, 5.2 to 9.7 wt%, 5.2 to 7.8 wt%, or 5.2 to 6.5 wt%. As described above, the residual amount of xylitol or sugar in the coating solution contained on the basis of the content included in the final hair reducing composition is within the range defined by the total weight of the final hair cleansing composition described above.

In addition, the xylitol part or the sugar part used in the above 1) some solid phase mixing step may be added to the total amount of xylitol contained in the final gum composition or the total content of xylitol contained in the final gum composition, The amount of xylitol remaining or the amount of sugar remaining can be deducted.

The coating solution used in the 2) liquid phase spray coating step may be prepared by mixing the remaining amount of xylitol or the remaining amount of sugar with a suitable solvent such as water (for example, purified water), an alcohol having 1 to 4 carbon atoms Lt; RTI ID = 0.0 > 1 < / RTI > In one example, the solvent may be selected from water, ethanol (e.g., fermentation alcohol), aqueous ethanol solution (e.g., 20 to 99% (v / v) ethanol aqueous solution) For example, the concentration of the coating solution may be in the range of 15 to 85 wt%, 15 to 75 wt%, 15 to 65 wt%, 25 to 85 wt% %, 25 to 75 wt%, 25 to 65 wt%, 35 to 85 wt%, 35 to 75 wt%, 35 to 65 wt%, 45 to 85 wt%, 45 to 75 wt%, 45 to 65 wt% 55 to 85 wt%, 55 to 75 wt%, or 45 to 65 wt%.

The 2) partial liquid spray coating step is a step of spraying (spraying) the coating solution containing the remaining amount of xylitol or the residual amount of sugar into the mixture of the step 1) (pre-mixing state, mixing state or post-mixing state) (Spraying) and coating the mixture). In one example, the 2) partial liquid spray coating step includes spraying (spraying) a coating solution containing the remaining amount of xylitol or the remaining amount of sugar into the mixture of the step 1) (pre-mixing state or mixing state or post-mixing state) (Or spraying the mixture to coat the mixture), and mixing the coated mixture. The step of mixing the spraying step with the coated mixture may be carried out sequentially or simultaneously.

In the process for preparing the emollient composition, 2) some liquid phase spray coating steps may be carried out 1) at the same time or after the 1) solid phase mixing step.

The above 1) some solid phase mixing step can be carried out under conditions that uniform solid phase mixing can take place. For example, 1) some solid phase mixing steps may be performed under conventional laboratory conditions (e.g., 15 to 30 C, 17 to 27 C, or 20 to 23 C and / or 40 to 55% or 45 to 50% ), And may be conducted for 0.5 to 60 minutes, but it is not limited thereto.

The 2) partial liquid spray coating may be carried out at 40 to 70 ° C, 45 to 65 ° C, or 50 to 60 ° C. If the temperature of the liquid phase spray coating (i.e., spraying of the coating liquid) is low, the moisture may be increased and bonding between the particles in the powder phase may occur, so that the size of the coated particles If the temperature of the spray coating step is too high, the coating liquid may be sprayed and moisture may evaporate at the same time, so that contact and coating with the mixture may not be performed well and loss to the dust collector may occur. In addition, when the temperature of the liquid phase spray coating step is set within the above range, there is an advantage that drying can be performed simultaneously with mixing.

2) some liquid phase spray coating steps (e.g., 1) between some solid phase mixing steps and 2) some liquid phase spray coating steps) to adjust the temperature of some liquid phase spray coating steps to this range, Deg.] C, 45 to 65 [deg.] C, or 50 to 60 [deg.] C.

The method for producing the composition for conditioning,

3) drying the coated mixture obtained in step 2)

. &Lt; / RTI >

The 3) drying step may be performed 2) at the same time as or after the subsequent liquid phase spray coating step.

The 3) drying step may be performed such that the water content is less than about 0.6%, less than about 0.4%, or less than about 0.2% by weight based on the total weight of the final toning composition.

The method for preparing the composition for emollient according to the present invention is characterized in that sugar or xylitol is mixed with a certain amount of sugar or xylitol and a part thereof is solid-phase mixed with all the remaining components, A chewing composition containing xylitol as a solid phase (powdery and / or granular phase) and uniformly distributing the composition ratio of sugar and xylitol can be produced. For example, the composition for emulsification may be a solid-phase mixture comprising a mixture of sugar and xylitol in a uniformly distributed ratio and an average particle size of 300 to 1000 탆 (for example, xylitol-coated sugar particles or sugar-coated xylitol particles) .

Another example of the present invention is to provide a composition for a sensitivity, which is produced by the above-mentioned method. The composition for chewing comprises sugar and xylitol in an amount of about 1: 0.05 to 1: 0.5, 1: 0.05 to 1: 0.3, 1: 0.1 to 1: 0.5, 1: 0.1 to 1: 0.3, 1: 0.15 to 1: : 0.5, 1: 0.15 to 1: 0.3, 1: 0.2 to 1: 0.5, or 1: 0.2 to 1: 0.3 (or more, sugar weight: xylitol weight).

As described above, the chewing composition is prepared by mixing sugar and xylitol in such a manner that any one component of sugar or xylitol is partly solid-phase mixed with the entirety of the remaining components, and the remaining balance is dissolved and coated on the solid-phase mixture , Sugar and xylitol as a solid phase (powder phase and / or granular phase), and the composition ratio of sugar and xylitol is uniformly distributed. The expression "the composition ratio of sugar and xylitol is uniformly distributed" means that the composition ratio of sugar and xylitol in any one or more portions of the composition is in the range of the average composition ratio and uniformity of the composition or the composition ratio of sugar and xylitol Quot; means that they are in a uniform range. In one example, the chewing composition may have a deviation (±%) of the composition ratio of sugar and xylitol in any two or more parts of the composition (absolute value of the difference in sugar and xylitol composition ratio (% by weight) 2.5% or less, 2.2% or less, 2% or less, 1.7% or less, 1.5% or less or 1.3% or less. For example, the above-mentioned composition for warming may have a deviation (±%) in the composition ratio of sugar and xylitol in any two or more portions in the composition under normal conditions (normal indoor conditions under no harsh conditions such as vibration) , 2.5% or less, 2.2% or less, 2% or less, 1.7% or less, 1.5% or less, or 1.3% or less. In another example, the composition for emulsifying may be applied to a composition (for example, a vibration (for example, 500 to 700 vibrations per minute)) of the compositional deviation of the composition of sugar and xylitol %) Is 2.5% or less, 2.2% or less, or 2% or less.

The chewing composition may be used for the purpose of shielding sweet or bitter taste in a food composition or a pharmaceutical composition.

Another example of the present invention provides a food composition comprising the composition for chewing. As described above, the composition for warming includes sugar and xylitol in a solid phase (powdery and / or granular phase), so that the food composition containing the same may also be in a form containing solid particles and / or powder. For example, the food composition may be a powdered and / or granular sweetener food additive; A powdered and / or granular mix composition of various tasty beverages including coffee, green tea, black tea, or iced tea; A powdery and / or granular mix composition of a functional food comprising various herbal medicine materials such as red ginseng or ginseng; A powdery and / or granular premix composition for the production of bread, confectionery, rice cake, egg, ice cream, ice cream, etc., but is not limited thereto. The content of the chewing composition in the food composition may be appropriately adjusted depending on the kind of the food composition, for example, 0.0001 to 90% by weight, 0.001 to 80% by weight, 0.01 to 50% by weight, Can be appropriately adjusted in the range of 0.01 to 30% by weight.

Another example provides a pharmaceutical composition comprising the composition as described above. The composition for chewing gum contained in the above pharmaceutical composition may be included as an excipient for coating a bitter taste, imparting sweetness, a coating agent, and the like. For example, the pharmaceutical composition may be an oral formulation in the form of tablets, capsules, powders, syrups or the like. The content of the skin-care composition in the medicinal composition may be appropriately adjusted depending on the kind of the medicinal composition and is, for example, from 0.0001 to 90% by weight, from 0.001 to 80% by weight, from 0.01 to 50% by weight, Can be appropriately adjusted in the range of 0.01 to 30% by weight.

According to the present invention, by mixing sugar and xylitol by some solid phase mixing and a part of liquid phase spraying, it becomes possible to obtain a uniform mixed composition in which the respective components are distributed in a uniform composition throughout the composition, and even in a severe condition such as vibration, A composition can be provided which can maintain a composition distribution and solve the problem of separation due to transportation (distribution) or vibration during storage.

In addition, when the present invention includes sugar and xylitol, there is an advantage that the excessive consumption of sugar is reduced, xylitol prevents cavities, prevents the increase of blood sugar level, and is effective in preventing adult diseases such as diabetes and obesity.

EXAMPLES The present invention will be described in more detail with reference to the following examples, comparative examples and comparative examples, but the scope of protection of the present invention is not intended to be limited to the following examples.

Example One. Xylitol By coating Xylitol &Lt; / RTI >

A total of 750 g of a mixture of sugar and xylitol having a mixing ratio of 78.3: 21.7 (sugar weight: xylitol weight) by weight of sugar and xylitol was prepared by coating a part of the above xylitol as a solution and coating.

Specifically, a commercially available sugar (Samyang Corp; powder phase; average particle size: about 597 탆) was prepared in an amount of 587.3 g corresponding to 78.3% by weight based on the total weight of the mixture of 750 g, and xylitol Average particle size: about 500-700 탆) was prepared in an amount of 162.7 g corresponding to 21.7% by weight based on 750 g of the total weight of the mixture. 126.8 g (powdery form) corresponding to 16.9% by weight of the total weight of the mixture was weighed out in 162.7 g of the prepared xylitol and mixed with 587.3 g (powdery form) of the prepared sugar in a mixer (fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr, slowly adjusted to a proper air intensity, room temperature) and mixed for about 3 minutes. Thereafter, 35.9 g (corresponding to 4.8% of the total weight of the mixture) of 162.7 g of the prepared xylitol, excluding 126.8 g (corresponding to 16.9 wt% of the total weight of the mixture) used in the mixing with the sugar, w / w) was prepared, and the mixture in the mixer was evenly sprayed while being mixed and uniformly coated. Before spraying the coating liquid (xylitol solution), the hot air temperature inside the mixer was raised to 60-70 ° C to adjust the temperature of the product temperature to 50-60 ° C. When the temperature stabilized within the above range, the coating liquid was sprayed, Mixing and drying were performed simultaneously. Dried to a water content of 0.2% by weight or less based on the total weight of the mixed and dried composition to prepare a solid mixed composition of sugar and xylitol having a uniform composition (average particle size of xylitol-coated sugar particles: 602.6 Mu m).

compare Example 1-1. Xylitol Spraying the entire mixture to prepare a mixed composition

A commercially available sugar (powdery phase; Samyang Co., average particle size: about 597 탆) was mixed with 587.3 g of an equivalent amount of 78.3% by weight of a total weight of 750 g of the mixture (Fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr), the temperature of the mixer was raised, and the temperature of the mixer was raised. The mixture was stirred at room temperature for 5 minutes to prepare a solution containing 162.7 g of xylitol (Loquat (import: Samyang Genex) (Corresponding to 21.7% by weight of the total weight of the mixture) was dissolved in water and mixed with spraying xylitol solution (60 Bx,% concentration), and the sugar was evenly coated with xylitol solution. As in Example 1, the temperature of the hot air inside the mixer was raised to 50-60 DEG C before the coating liquid was sprayed, so that the mixing and drying were simultaneously performed. Based on the total weight of the mixed and dried composition, until the moisture content was 0.2 wt% or less.

compare Example 1-2. Xylitol The amount of coating spray is reduced to produce a mixed composition

A commercially available sugar (powdery phase; Samyang Corp., average particle size: about 597 탆) was prepared in an amount of 587.3 g corresponding to 78.3% by weight based on 750 g of the total weight of the mixture, and xylitol (Roquet (imported: Samyang Genex) Average particle size: about 500-700 탆) was prepared in an amount of 162.7 g corresponding to 21.7% by weight based on 750 g of the total weight of the mixture. 159.0 g (powder phase) corresponding to 21.2% by weight of the total weight of the mixture of the prepared xylitol was mixed with 587.3 g (powdery phase) of the prepared sugar in a mixer (fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr The mixture was gradually added in a gradual manner under the condition, adjusted to a proper air intensity, room temperature) and mixed uniformly. Thereafter, 3.7 g (corresponding to 0.5% by weight of the total weight of the mixture) of 162.7 g of the prepared xylitol, excluding 159.0 g (corresponding to 21.2 wt% of the total weight of the mixture) used in the mixing with the sugar, (w / w) was prepared, and the mixture in the mixer was evenly sprayed while being mixed and uniformly coated. As in Example 1, the temperature of the hot air inside the mixer was raised to 50-60 DEG C before the coating liquid was sprayed, so that the mixing and drying were simultaneously performed. Based on the total weight of the mixed and dried composition, until the moisture content was 0.2 wt% or less.

Example 2. Sugar solution Coated sugar and Xylitol Preparation of mixed composition

A total of 750 g of a mixture of sugar and xylitol having a mixing ratio of 78.3: 21.7 (sugar weight: xylitol weight) by weight of sugar and xylitol was prepared by coating a part of the sugar with a solution.

Specifically, a commercially available sugar (powdery phase; Samyang Corp., average particle size: about 597 탆) was prepared in an amount of 587.3 g corresponding to 78.3% by weight based on the total weight of the mixture of 750 g, and xylitol Average particle size: about 500-700 [mu] m) was prepared in an amount of 162.7 g corresponding to 21.7% by weight based on 750 g of the total weight of the mixture. 551.3 g (corresponding to 73.5 wt% of the total weight of the mixture; powdery phase) of 587.3 g of the prepared sugar was mixed with 162.7 g (powdery phase) of the prepared xylitol in a mixer (fluid bed drier: Enger (China), Air Fan 40-120 m ³ / hr And the mixture was homogeneously mixed for about 3 minutes at room temperature. Thereafter, 36.0 g (corresponding to 4.8% by weight of the total weight of the mixture) of the 587.3 g of the prepared sugar except for 551.3 g which was used for mixing with xylitol was dissolved in water to prepare a sugar solution having a concentration of 60% (w / w) After the preparation, the mixture in the mixer was evenly sprayed while being mixed and uniformly coated. As in Example 1, the temperature of the hot air inside the mixer was raised to 50-60 DEG C before the coating liquid was sprayed, so that the mixing and drying were simultaneously performed. Dried to a water content of 0.2% by weight or less based on the total weight of the mixed and dried composition to prepare a solid mixed composition of sugar and xylitol having a uniform composition (average particle size of sugar coated xylitol particles: 624.2 Mu m).

compare Example 2

As in Comparative Example 1, there is a relatively large proportion of the sugar (78.3%) to be mixed, and there is a real problem in preparing and spraying as much of this amount as the solution. In other words, if the amount of the solution to be sprayed is too large, the amount of water becomes large and it melts due to moisture absorption or takes a long time to dry, so that it is practically inefficient and is not easily produced. Therefore, in this comparative example, a mixture of sugar and xylitol was prepared by varying the amount of the coating solution to be sprayed.

2-1. Increase the coating spray amount of sugar to produce mixed composition

A commercially available sugar (powdery phase; Samyang Corp., average particle size: about 597 탆) was prepared in an amount of 587.3 g corresponding to 78.3% by weight based on the total weight of the mixture of 750 g, and xylitol (Roeit (import: Samyang Genex); Average particle size: about 500-700 [mu] m) was prepared in an amount of 162.7 g corresponding to 21.7% by weight based on 750 g of the total weight of the mixture. 510.0 g (corresponding to 68.0 wt% of the total weight of the mixture; powdery phase) of 587.3 g of the prepared sugar was mixed with 162.7 g (powdery form) of the prepared xylitol in a mixer (fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr The mixture was gradually added in a gradual manner under the condition, adjusted to a proper air intensity, room temperature) and mixed uniformly. Thereafter, 77.3 g (corresponding to 10.3% by weight of the total weight of the mixture) of 5107 g of the prepared sugar (excluding 510.0 g) used in the mixing with xylitol was dissolved in water to prepare a sugar solution having a concentration of 60% (w / w) After the preparation, the mixture in the mixer was evenly sprayed while being mixed and uniformly coated. As in Example 1, the temperature of the hot air inside the mixer was raised to 50-60 DEG C before the coating liquid was sprayed, so that the mixing and drying were simultaneously performed. Dried to a water content of 0.2% by weight or less based on the total weight of the mixed and dried composition to prepare a mixed composition of sugar and xylitol.

2-2. Reducing the coating spray amount of sugar to produce mixed composition

A commercially available sugar (powdery phase; Samyang Corp., average particle size: about 597 탆) was prepared in an amount of 587.3 g corresponding to 78.3% by weight based on the total weight of the mixture of 750 g, and xylitol (Roeit (import: Samyang Genex); Average particle size: about 500-700 [mu] m) was prepared in an amount of 162.7 g corresponding to 21.7% by weight based on 750 g of the total weight of the mixture. (Fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr (powder)) together with 162.7 g (powdery form) of the prepared xylitol was added to 583.5 g of the prepared sugar (corresponding to 77.8% The mixture was gradually added in a gradual manner under the condition, adjusted to a proper air intensity, room temperature) and mixed uniformly. Thereafter, 3.8 g (corresponding to 0.5% by weight of the total weight of the mixture) of 587.3 g of the prepared sugar except for 583.5 g which was used for mixing with xylitol was dissolved in water to prepare a sugar solution having a concentration of 60% (w / w) After the preparation, the mixture in the mixer was evenly sprayed while being mixed and uniformly coated. As in Example 1, the temperature of the hot air inside the mixer was raised to 50-60 DEG C before the coating liquid was sprayed, so that the mixing and drying were simultaneously performed. Dried to a water content of 0.2% by weight or less based on the total weight of the mixed and dried composition to prepare a mixed composition of sugar and xylitol.

compare Example 3. Xylitol And solid solids blend of sugar

A commercially available sugar (powdery phase; Samyang Corp., average particle size: about 597 탆) was prepared in an amount of 587.3 g (powdery form) corresponding to 78.3% based on the total weight of the mixture of 750 g, and xylitol (An average particle size of about 500-700 탆) in an amount of 162.7 g (powder form) corresponding to 21.7% of the total weight of the mixture was prepared and mixed with a full-volume mixer (fluid bed dryer: Enger (China), Air Fan 40-120 m ³ / hr, slowly adjusted to a proper air intensity, room temperature) and mixed evenly.

Test Example 1. With sugar Xylitol Mixed composition Per party Comparison of content variation

Whether the sugar and xylitol in the mixed composition prepared according to each of Examples 1 and 2 and Comparative Examples 1-1, 1-2, 2-1, 2-2 and 3 were uniformly mixed And 6 parts of each sample were randomly selected and partially sampled in an amount of 1 g and analyzed by high performance liquid chromatography to confirm the sugar composition of each sample (manufacturer: Agillent, analysis column: Biolad Carbohydrate Aminex

Solvent: water, flow rate: 0.6 ml / min, column temperature: 80 占 폚, injection volume: 10 占 퐇). At this time, it was tested under laboratory conditions (20-23 ° C and humidity 45-50%) without any special harsh conditions (such as vibration). The results are shown in Table 1. It was determined that mixing of the granular sugar was uniformly performed well to the level of the sugar composition deviation between the components in the above mixed composition to the level of 1.5% or less.

Mix Uniformity Analysis Item Average content of sugar composition% Sugar Xylitol Deviation (±%) Example One 78.4 21.6 0.4 Comparative Example 1-1 82.1 17.9 2.8 Comparative Examples 1-2 78.0 22.0 2.3 Example 2 78.8 21.2 1.2 Comparative Example 2-1 76.4 23.6 4.0 Comparative Example 2-2 77.9 22.1 3.5 Comparative Example 3 80.1 19.5 5.5

compare Test Example 2. Comparison of sugar content under severe (vibration) conditions

In order to confirm whether the components of the mixed composition prepared according to each of Examples 1 and 2 and Comparative Examples 1-1, 1-2, 2-1, 2-2 and 3 were evenly distributed throughout the composition, We analyzed the variation of sugar content after applying the vibration (harsh) condition so that the unmixed components could be separated.

More specifically, a wide tray was placed on a vibrator, and 100 g of each sample was placed on the top of the tray. Then, 600 vibrations per minute were applied for 1 minute to disperse all the powders. Then, 1 g of each of the powders scattered at the position corresponding to the height of the tray was collected at 9 sites and analyzed by high performance liquid chromatography to confirm the sugar composition of each sample. The results are shown in Table 2. Since the sugar composition deviation between the components in the mixed composition induced the separation between the components of each sample under severe conditions, it was determined that the granular sugar mixture was uniformly mixed to a level of 2.5% or less in consideration of the severe condition.

Mix Uniformity Analysis Item Average content after vibration% Sugar Xylitol Deviation (±%) Example One 77.8 22.3 1.0 Comparative Example 1-1 83.0 17.0 4.8 Comparative Examples 1-2 78.5 21.5 2.8 Example 2 77.9 22.1 1.9 Comparative Example 2-1 79.0 21.0 3.4 Comparative Example 2-2 83.0 17.0 5.1 Comparative Example 3 78.9 21.1 6.7

As shown in Tables 1 and 2, the mixed compositions prepared in Examples 1 and 2 were prepared by mixing the mixed composition prepared in Comparative Examples 1-1, 1-2, 2-1, 2-2, and 3 It can be seen that the sugar and xylitol are distributed in a uniform composition throughout the composition and the uniform composition distribution is not maintained even under severe conditions. In addition, if the amount of the coating liquid sprayed in the liquid phase and coating the powder is large, loss may occur during the spraying process, resulting in deviation (refer to Comparative Examples 1-1 and 2-1). When the amount of the coating liquid is small, (See Comparative Examples 1 and 2 and 2-2). Therefore, it is necessary to determine the appropriate amount of the coating liquid depending on each component. Based on the results of Tables 1 and 2, the amount of the coating liquid is suitably in the range of about 1 to 10% by weight based on the total weight of the mixture .

Claims

1) solid phase mixing step of solid phase mixing all the sugar, part of xylitol or part of sugar and xylitol, based on the sugar and xylitol content in the final gum composition; And
2) a portion of the xylitol used in the solid-phase mixing step, or a part of the liquid phase spray coating step of spraying the coating solution containing the remaining amount of xylitol or the remaining amount of sugar excluding the sugar portion into the mixture in the solid-
&Lt; RTI ID = 0.0 >

The method according to claim 1,
The remaining amount of xylitol or the residual amount of sugar contained in the coating solution used in the 2) partial liquid spray coating step is 1 to 10% by weight based on the total weight of the final toning composition,
The xylitol part or the sugar part used in the above 1) some solid phase mixing step may be the xylitol residual amount contained in the coating solution of the 2) partial liquid spray coating step or the total amount of xylitol contained in the final gum composition or the total content of xylitol The amount of sugar,
Gt;

The method according to claim 1,
The remaining amount of xylitol or the residual amount of sugar contained in the coating solution used in the 2) partial liquid spray coating step is 3 to 7% by weight based on the total weight of the final toning composition,
The xylitol part or the sugar part used in the above 1) some solid phase mixing step may be the xylitol residual amount contained in the coating solution of the 2) partial liquid spray coating step or the total amount of xylitol contained in the final gum composition or the total content of xylitol The amount of sugar,
Gt;

The method according to claim 1,
Wherein the ratio of the content of sugar to xylitol in the final gum composition is from 1: 0.15 to 1: 0.5 by weight (sugar content: xylitol content)
Gt;

The method according to claim 1,
Wherein the 2) partial liquid spray coating step is performed at the same time as or after the 1) partial solid phase mixing step.
Gt;

The method according to claim 1,
3) drying to a moisture content of less than or equal to about 0.2% by weight, based on the total weight of the final toning composition.
Gt;

The method according to claim 1,
Wherein the conditioning composition is in powder or granular form,
Gt;

A chewable composition comprising sugar and xylitol,
A method for producing a chewing gum composition according to any one of claims 1 to 7,
Powdery or granular,
(±%) of the composition ratio of sugar and xylitol in the composition is 2.2% or less,
Sensitive composition.

9. The method of claim 8,
Wherein the compositional deviation (±%) of the sugar and xylitol in the composition is 2.0% or less,
Sensitive composition.

9. A food composition comprising the composition of claim 8.

[Claim 11] The food composition according to claim 10, wherein the food composition is selected from the group consisting of a powdery or granular taste food additive, a powdery or granular mix composition of a tasty drink, a powdery or granular mix composition of a functional food or a powdery or granular premix composition , &Lt; / RTI >

9. A pharmaceutical composition comprising the composition of claim 8.

13. The food composition of claim 12, wherein the pharmaceutical composition is an oral formulation in the form of tablets, capsules, powders, or syrups.