KR20120119854A

KR20120119854A - Preparation method of a nutritional supplement and alcoholic drink prepared by solid-liquid seperation of traditional rice wine

Info

Publication number: KR20120119854A
Application number: KR1020110038079A
Authority: KR
Inventors: 이동희
Original assignee: 이동희
Priority date: 2011-04-22
Filing date: 2011-04-22
Publication date: 2012-10-31

Abstract

Although the makgeolli contains beneficial ingredients and anti-cancer ingredients for the human body, the alcohol contained in the makgeolli can adversely affect the human body due to intoxication or excessive drinking. It relates to an invention that is intended to allow people to consume all of them without losing the active ingredients contained in the rice wine.
The present application applies a solid-liquid separation method to alcohol forge and turbid substances and alcohol contained in makgeolli to provide alcoholic beverages with alcoholic beverages containing beneficial ingredients for alcoholic beverages, and alcohol components are not included. Unrefined Makgeolli is a means of providing the beneficial ingredients contained in the Makgeolli solid as a health supplement for those who cannot drink alcohol or who want to consume solids. Separation of liquor fork and mixed liquor with grains is separated by liquid and alcohol, and alcohol and water are not included through the drying and grinding of the liquor fork provided in the step. Traditional liquor and dry It relates to a method to get the supplements at the same time.

Description

Preparation method of a nutritional supplement and alcoholic drink prepared by solid-liquid seperation of traditional rice wine.}

The present invention is a liquid-liquid separation of turbid liquor mixed with alcohols and grains produced by microbial fermentation during the process of preparing various traditional liquors provided by adding medicinal herbs to grains to obtain conventional makgeolli, copper dongju or various functional effects. The liquor fork is separated from liquor by the method, and the liquor fork is dried and pulverized to obtain a powder of a dietary supplement containing no alcohols and water, and the liquor is prepared by filtration or distillation. The invention is to provide a healthy life by ingesting all the beneficial ingredients contained in the traditional liquor without losing any waste during the process of manufacturing traditional liquor.

When the technical idea of the present application is applied, it can extend the shelf life of traditional liquor or makgeolli, and can spread domestic traditional liquor, makgeolli or dongdongju, and at the same time obtain the health supplement and liquor by the traditional liquid and liquid separation method. It relates to an invention that can be.

Makgeolli is a traditional Korean liquor, also known as Takju, Nongju, Jaju, and Hoeju. It is usually made by adding yeast to rice or wheat, and fermenting alcohol during fermentation. Lactic acid bacteria fermentation is carried out, and the alcohol content of makgeolli is about 6 ~ 8% .In general, steam the glutinous rice, non-glutinous rice, barley, flour, and so on. At this time, it is Dong Dongju that floats rice grass without filtering sake lees.

Makgeolli is only 6-8 degrees in alcohol level and the level of beer, and recently, the report is rich in dietary fiber and contains a large amount of beneficial lactic acid bacteria, which has been used by many people and increasing interest.

If you look at the ingredients of makgeolli, water is about 80%, and among the remaining 20%, alcohol consists of 6 ~ 8%, protein 2%, carbohydrate 0.8%, fat 0.1%, and the remaining 10% is dietary fiber, vitamin B , C and lactic acid bacteria yeast have been reported.

In the case of lactic acid bacteria, one bottle of Makgeolli PET contains 70-80 billion lactic acid bacteria, which is equivalent to 100-120 bottles of yogurt, and lactic acid bacteria destroys harmful bacteria causing inflammation or cancer in the intestine and strengthens immunity. It is reported to do.

Also, it is said to be rich in vitamin B group, which is good for men, and 200 ml (3/4 bowl) of makgeolli contains vitamin B2, choline, and niacin.In the case of vitamin B group, it is especially helpful for middle-aged men. And it has the effect of skin regeneration and visual enhancement, and makgeolli is rich in dietary fiber, and it is reported that it is excellent in preventing constipation and preventing cardiovascular disease by actively providing colon motion.

According to the information released on April 14, 2011 by Dr. Hamo, a research team at the Korea Food Research Institute, Korea's Food Research Institute announced that the world's first discovery of anti-cancer substance panezol was found in makgeolli. It is an ingredient that can exert anticancer and anti-tumor effects even in a small amount of 5-7 mg / L, and the amount of panezol contained in commercially available wine and beer is about 15-20 ppb concentration. Makgeolli has a concentration of 150 ~ 500 ppb, and it is reported that 10 ~ 25 times more ingredients are found in the rice wine in Korea than wine or beer.

However, since the turbid part of makgeolli contains more panesol, it is reported that the makgeolli is well shaken when drinking, and all the ingredients are mixed before drinking to see more anti-cancer effects. Also, the proper alcohol content of makgeolli is blood circulation and budding. It is said to facilitate metabolism, which removes fatigue substances and is effective for skin beauty.

In addition, Makgeolli contains 100 ~ 1000 times more dietary fiber than other commercially available food beverages, so it helps to increase bowel movements, which is not only good for constipation prevention, treatment, and diet, but also because calories are not high, but it prevents obesity due to satiety. There are also benefits.

Experts say that drinking makgeolli, which is more healthy than any alcohol, is like eating nutritional supplements except alcohol, while makgeolli contains 6-8% of alcohol. There is a problem that can not drink a large amount because it is included.

In addition, since the fermentation of the yeast bacteria makgeolli is added sour taste has a problem that it is difficult to distribute more than a certain distance in the brewery, it is difficult to store for a long time.

The present application, as it is clear from the background art, drink the makgeolli is very beneficial to the human body and anti-cancer ingredients are included, so even though the health and medical utility is high due to alcohol contained in the makgeolli due to alcohol or drunk drinking In order to provide adverse effects, the invention is intended to allow people to drink a limited amount of makgeolli or to consume it without losing the active ingredient contained in makgeolli in case of being unable to drink according to physical conditions.

The present invention is a method for solid-liquid separation of turbid liquor mixed with alcohols and grains produced by microbial fermentation during the manufacture of conventional makgeolli, copper dongju or various traditional sake provided by adding herbal medicine to grains to obtain various functional effects. The liquor fork is separated from the liquor by liquor, and the liquor fork has an object of the present invention to provide a dietary supplement containing no alcohols and water through a drying and grinding step.

This company provides alcoholic beverages that are transparent by liquor separation method and traditional liquor that co-exists with liquor fork, and provides a refreshing drinking environment by eliminating trim after drinking alcohol, and discarding the solids contained in traditional liquor. The purpose of the present invention is to find a way to maximize the environmental and health benefits by providing a high value-added health supplement.

The present application provides a liquid-liquid separation of alcohol and liquor fork and turbid matter contained in traditional liquor including makgeolli, and a transparent alcohol layer containing alcohol is provided to drink as an alcoholic beverage containing ingredients beneficial to the liquor, and does not include alcohol components. Traditional traditional solids are those who should not drink alcohol in the body at all, or those who want this part, by ingesting the beneficial ingredients contained in traditional liquor to increase the body's metabolism, increase resistance to disease, As a means for providing the invention, it is the invention of the technical concept to provide a dietary supplement and liquor at the same time by applying the traditional liquor liquid separation method.

Hereinafter, the technical idea of the present application will be described in detail as follows.

As a means to achieve the above object is a solid-liquid separation method of the mixed liquor mixed with alcohols and cereals made by mixing grains, yeast and water and fermentation at a constant temperature during the process of manufacturing makgeolli or Dongdongju, a traditional Korean liquor The liquor fork and liquor are separated by the liquor, and the liquor and liquor separated from the liquor are dried and pulverized to obtain a dietary supplement powder containing no alcohols and water, and the liquor is prepared by filtration or distillation. It has a technical idea to provide.

In addition, all of the makgeolli provided with added natural products, herbal medicines, or food additives in order to give functionality to the makgeolli to which the technical idea of the present application is applied may of course be equally applied to the technical idea of the present application.

The solid-liquid separation method of the turbidity mixed with alcohols and grains may be applied by selecting one or more solid-liquid separation methods from density separation method, dehydration method by centrifugation, reduced pressure filtration method, pressure filtration method, In order to further minimize the moisture and alcohol content in large quantities of makgeolli solids, a process in which dehydration is optionally carried out by a belt press can be added.

Among the solid-liquid separation methods, the density separation method uses a large capacity of rice wine containing sake lees and turbidity according to the separation method which slowly settles down due to the difference in specific gravity of the sake lees and turbid matter floating in the water of rice wine. It can be advantageously applied to separate it from the storage tank.

The pressure reduction filtration method is a method of accelerating the filtration by reducing the inside of the container containing the filtrate by applying a pressure to the liquid level in the filter by the reduced pressure, this operation is to filter a large amount of rice wine in a short time, if the filtration rate is difficult to filter It is used to promote the pressure filtration method is a principle opposite to the pressure reduction filtration method, this method can also be used to promote the filtration rate.

In order to separate a large amount of makgeolli from liquor fork and turbid matter at high speed, it is preferable to use a dehydration method by centrifugal separation, and to provide makgeolli alcoholic beverages while increasing the alcohol content of makgeolli. Although it may be preferable to use a heat distillation method, the method of solid-liquid separation of makgeolli using the heat distillation method has the advantage of providing a very transparent makgeolli alcoholic beverage, but distillation is performed by temperature heating and vacuum distillation. As it should be, the price competitiveness can be reduced by increasing equipment, and lactic acid bacteria beneficial to the human body can be killed during the heating process.

When applying the solid-liquid separation method presented here is likely to include a large amount of water and alcohol, this may cause a problem that requires a lot of energy and time in the heating step to overcome this problem It is possible to apply a step of selectively dehydrating a large amount of water and alcohol into the solid content separated by the liquid separation method by a filter press.

As such, the transparent makgeolli, which is provided through the liquid and liquid separation method of sake lees and turbid substances contained in makgeolli, can prevent trimming that occurred when drinking makgeolli alcoholic beverages for alcoholic beverages. It provides the effect of providing a clean aftertaste to the taste of liquor lovers who like makgeolli, and solid and liquid separated solids do not contain alcohol and water through the following drying and grinding steps. The powder of the food can be obtained.

Drying and pulverizing the solids, which have undergone the solid-liquid separation process herein, can provide a dietary supplement so that alcohol and water are not contained while preventing the vanishing and destruction of beneficial ingredients contained in liquor fork and turbidity. As a means for obtaining a powder, the drying step may be dried by a heating method selected from a high temperature atmospheric pressure heating method, a high temperature reduced pressure heating method, a drying method using a normal temperature reduced pressure, a drying method using a normal temperature and atmospheric pressure, and a vacuum drying method. Can be.

Solid-liquid separated solids require heating means at the highest possible temperature to remove large amounts of water and alcohol.However, the lactic acid bacteria and other heat-sensitive beneficial substances present in the solids may be damaged during the heating process. Therefore, any of the drying methods described above may be applied, but in order to provide a health supplement for powdering while preventing damage to the beneficial ingredients contained therein, a drying method using a normal temperature or a normal pressure or a normal drying method, It is preferable to use the vacuum drying method by freezing.

In addition, the pulverization step may be provided as a powder or powder or tablets or capsules as a means for people to conveniently ingest as a dietary supplement of powders or pills while maintaining a uniform solid component dried by the drying step. .

The pulverization step is not particularly limited, and may be possible if the fine powder that can be mixed uniformly beneficial ingredients to the human body without providing a problem when people do not feel the objection when ingesting the powder, , Makgeolli solid dried in the drying step of the present invention, it is preferable to use a dry grinding method of the absence of water or alcohol.

In general, depending on the particle size of the particles (mainly powder products) [crushing] (10 cm-10 cm) → [heavy chain] (several cm → several m), grinding (several cm → 10 m), [ Fine grinding] (a few mm → several μm), it is advantageous to select and apply a grinder capable of grinding into fine powder in order to actively include the technical idea of the present application.

Grinding can be used by selecting one type of mill from turbo mill, super micro mill, roller mill, raymond mill, port mill, tube mill, conical mill, jet mill, jet mill, vibrating ball mill, Is preferably 1.0 µm to 3.5 mm, more preferably 10 µm to 1.0 mm, and most preferably 25 µm to 100 µm in size, so that the solid particles of makgeolli can be pulverized to 1.0 µm or less. In this case, there is a problem that not only the workability is insufficient because it has to go through the grinding process for a long time, but also it may cause a problem in the respiratory disease caused by the release of fine powder in the air. Can have the advantage of excellent workability, but the composition inside the solids may be non-uniform, can provide inconvenience for people to ingest The powder having a particle size in the proposed preferred because.

In the case of the turbo mill and the super micron mill, as a pulverization method by the impact shear force with a high-speed rotary impact grinder, which is a centrifugal classification type, a high-speed rotating shock plate, an impact caused by several impact plates while moving in an axial direction along the airflow, and a wall It is pulverized by the strong shear magnetic bridge between the wall and the wall, and by the pulverization between the airflow and the particles. The representative types are horizontal type (supermicron mill, turbo mill) and vertical type (contraflux, ultra fin).

Looking at the grinder in detail, in the case of the roller mill and Raymond mill, the method of grinding by compression, shear partial friction in the roll rotation type, it is built in an air classifier, and rotates 3-4 rollers or forced balls by pressing on the disc At the same time, it can be described as a pulverizer that is crushed by applying the compression, friction and shearing action between the roller and the disc and the inner wall of the edge at the same time.

In the case of port mills, tube mills, and conical mills, the ball media mill is a method of grinding by impact friction caused by low-speed rotational vibration, which is dry and wet, and puts the ball into the grinding media in a rotating cylinder and vibrates it. Can be.

In the case of jet crusher and jet mill, it is a jet crusher. It is a pulverizer by impact and friction that uses jet streams. have.

In addition, in the case of a vibrating ball mill, as a grinding method by shear friction in a low-speed rotary vibration type, the grinding machine can be described as a grinder in which a medium is put in a cylinder or trap sand mill and subjected to vibration.

Therefore, the technical idea of the present invention is a dietary supplement obtained through the traditional liquor manufacturing process made using grains, and solid-liquid separation of liquor forge and turbid mixture of alcohols and grains produced by microbial fermentation during traditional liquor manufacturing process. It is an invention of the technical idea to separate a liquid alcohol and liquor fork by the process, and to dry and grind the liquor fork and turbid matter obtained in the above separation step to obtain a health supplement.

Hereinafter, embodiments of the present invention will be described in detail with reference to the following examples in the 'Specific Content for Implementing the Invention' section.

As described above, although the conventional rice wine can provide very beneficial nutrients to the human body, it contains 6 to 8% of alcohol contained in the rice wine, improving and eliminating all the problems of the prior art, which had to be limitedly drinkable. Has the effect.

When applying the solid-liquid separation method of the present application, alcohol-containing makgeolli offers alcoholic beverages containing beneficial ingredients to drinkers and has no effect of trimming, and the solid content of makgeolli that does not contain alcohol is a beneficial ingredient. It is provided as a dietary supplement for humans to increase the body's resistance to diseases by activating metabolism, providing the best physical condition, and no waste is generated after manufacturing and processing makgeolli. It has an effect that can contribute.

1: is a photographic example in which the solid-liquid separation process of makgeolli in this embodiment is applied using a rotary evaporator.

Prior to describing the embodiments of the invention for embodying the technical idea of the present application by way of example, the terms or words used in the specification or claims of the present application shall not be construed as being limited to a common or dictionary meaning, The scope of protection of the present application should be construed as meanings and concepts corresponding to the technical spirit of the present invention, and the embodiments described herein are merely preferred embodiments of the present invention and do not represent all of the technical ideas of the present application. It is to be understood that there may be various equivalents and variations in place of them at the time of this application.

Hereinafter, an example of the present invention to which the technical concept of the present application is applied, and the result of performing the solid-liquid separation process of the makgeolli stock solution in various ways was compared.

Example 1

Wash 8 kg of non-glutinous rice, immerse in water for about 10 hours, then sift to drain the water. In order for water vapor to be supplied to the rice to be a gourd rice, water is present in the lower layer of the heating vessel, and a cloth and rice are supplied to the rice pedestal and then heated. After cooling the gourd rice, the leaven of the powder was supplied at a weight% of about 1/10 to the amount of the gourd rice, and then mixed uniformly, and the makgeolli was prepared by maintaining the room temperature at about 30 ° C. for 3 days. It was intended to be used as a sample for.

Example 2

About 5 liters of the rice wine prepared in Example 1 was aliquoted into a bucket, which was allowed to stand for 5 hours to separate solid and liquid by a density separation method. The transparent upper layer was taken as a Makgeolli alcoholic beverage sample, and the other lower solids were dried by a dry oven at 100 ° C. to prepare a solid at high temperature and atmospheric pressure conditions. The solid was pulverized with a ball mill for 4 hours to obtain a powdered rice wine solid.

Example 3

About 5 liters of the rice wine prepared in Example 1 was aliquoted into a bucket, which was allowed to stand for 5 hours to separate solid and liquid by the density separation method. The transparent upper layer was taken as a Makgeolli alcoholic beverage sample, and the solids of the other lower layer were dried as follows. In a 1 liter round flask, 500 ml of the solid separated by the density separation method was collected and mounted on a rotary evaporator. The temperature of the water bath was set to 85 ° C., and the pressure was distilled under reduced pressure to reduce the high temperature. Solids were prepared. The solid was pulverized with a ball mill for 4 hours to obtain a powdered rice wine solid.

Example 4

The filter paper was placed in a Buchner funnel and inserted into a reduced pressure flask, and about 5 liters of the rice wine prepared in Example 1 was filtered under reduced pressure. The filtered liquid was used as an alcoholic beverage sample, and the filtered solid was dried by a dry oven at 100 ° C. to prepare a solid by high temperature and atmospheric pressure. The solid was pulverized with a ball mill for 4 hours to obtain a powdered rice wine solid.

Example 5

The filter paper was placed in a Buchner funnel and inserted into a reduced pressure flask, and about 5 liters of the rice wine prepared in Example 1 was filtered under reduced pressure. The filtered liquid was used as an alcoholic beverage sample, and the filtered solid was placed in a desiccator, the lid was closed, and dried using a vacuum pump to prepare a solid by decompression at room temperature. The solid was pulverized with a ball mill for 4 hours to obtain a powdered rice wine solid.

Example 6

In a 1 liter round flask, about 500 ml of the rice wine prepared in Example 1 was collected, mounted in a rotary evaporator in which the temperature of the water bath was adjusted to 40 ° C., and the vacuum pump was operated to operate the rice wine. Solid-liquid separation was performed, and the cooling water was allowed to cool the ethylene glycol solution maintained at 0 ° C. instead of tap water by a circulation pump. The liquid produced by the depressurization at room temperature was an alcoholic beverage sample, and the solid dried by distillation under reduced pressure at room temperature was pulverized with a ball mill for 4 hours to obtain a powdered rice wine.

Comparative Example 1

The stock solution prepared in Example 1 was prepared.

Comparative Example 2

The makgeolli stock was regarded as the state prior to providing the subject with 1 g of the powder solid-liquid separated by each method.

The Makgeolli stock solution was solid-liquid separated by each method, and the dried solid and liquid phase were compared with each other. For liquid makgeolli alcoholic beverages, we tried to check the turbidity (LaMotte 2020e), whether trimming occurred after drinking alcohol, and the atmosphere of drinking. The participants in this experiment were 11 adult men and women (7 men, 4 women) by the sensory method, and the average age of the experiment was 41.8 years old, and the results are shown in Table 1. .

division Experiment item Turbidity (NTU) burp Feeling Example 2 8.6 Not at all Refreshing Example 3 8.6 Not at all Refreshing Example 4 3.7 Not at all Refreshing Example 5 3.7 Not at all Refreshing Example 6 0.15 Not at all Very refreshing Comparative Example 1 124 2.6times usually

As shown in Table 1, in Comparative Example 1 of the makgeolli stock solution, which was not subjected to any solid-liquid separation process, it was confirmed that the alcoholic beverage was very opaque as the turbidity was 124. While the condition after drinking Makgeolli was normal with about 2.6 times of trimming after drinking, the liquid-liquid separation process was applied as shown in Examples 2 to 6, so that the alcoholic beverage was transparent inside Makgeolli alcoholic beverage. And because the turbid material is not included, after the drinking did not occur at all, it was confirmed that the mood feels very refreshing.

In particular, in the case of a transparent alcoholic beverage made using a rotary evaporator of the room temperature decompression method was not only very transparent but also very refreshing feeling after drinking.

When the makgeolli stock solution was solid, liquid separated, dried and pulverized by the respective methods, the atmosphere of bowel movement and the condition of life were compared. For this, 1 g of tablets were formed. The participants were 25 male and female adults (4 males, 21 females), and the average age of the participants was 28.6 years. Subjects were asked to take one tablet of solids made by the experimental method for 7 days after breakfast, lunch and dinner, and the results were confirmed. The results for solids are shown in Table 2.

division Defecation Condition Example 2 Pleasure Refreshing Example 3 Pleasure Refreshing Example 4 Pleasure Refreshing Example 5 Very pleasant Very refreshing Example 6 Very pleasant Very refreshing Comparative Example 2 Constipation serious Very unpleasant

As shown in Table 2 above, in the case of Comparative Example 2, most young women had serious constipation in the state before the makgeolli stock solution was subjected to the solid-liquid separation process by each method to give 1 g of the powder to the subject. And, due to this condition of living is very unpleasant, when the solid-liquid separation process of Example 2 to Example 6, the bowel movement is excellent, it was confirmed that the condition of life is refreshed.

In particular, in the case of Examples 2 to 4 it was confirmed that the heating temperature during the drying process is high, the lactic acid bacteria contained in the solid content is killed, so that the effect of bowel movement is not very excellent.

This is due to the dietary fiber and a large amount of minerals inside the solids, showing a certain degree of pleasure effect by smoothing the metabolism, and at the same time could increase the condition of life.

In particular, when people ingest the dried solid in the temperature range in which the lactic acid bacteria are not killed, as in Example 5, people live by additional reactions by dietary fiber and minerals as well as by the pleasure of lactic acid bacteria, to stay in a very refreshing environment We could confirm that we could.

Example 7

In Example 6, the inorganic substance contained in the solid powder and liquid transparent makgeolli alcoholic beverage was separated. In the case of powdered solids for the analysis of inorganic components, precisely weigh 1 g of the sample into the microwave digestion vessel to the fourth decimal point, supply sulfuric acid and nitric acid, close the lid, and use the microwave digestion system (Anton Paar. Multiwave). 3000) to give a clear solution. The pretreated solution was transferred to a 100 ml volumetric flask and vigorously shaken to prepare a pretreatment solution for inorganic component analysis. The clear liquid alcoholic beverage was analyzed directly without pretreatment. The analysis items were calcium (Ca), sodium (Na), potassium (K), magnesium (Mg), iron (Fe), and phosphorus (P). Among them, calcium, sodium, potassium, magnesium and iron were Thermo Scientific iCAP. 6500 duo Inductively Coupled Plasma-Atomic Emission Spectrometer (ICP-AES) was used, and phosphorus was performed by total phosphorus analysis method in the water pollution process test method, and the results are shown in Table 3.

Comparative Example 3 was carried out in the same manner as in Example 7, except that a uniform sample was obtained by vigorously shaking the makgeolli stock solution prepared in Example 1.

division Analysis item Ca
(ppm) Na
(ppm) K
(ppm) Mg
(ppm) Fe
(ppm) P
(ppm) Example 7 Liquid N.D. N.D. N.D. N.D. N.D. N.D. Solids 22.4 8.45 4.66 6.24 3.86 624 Comparative Example 3 1.34 2.65 0.885 0.246 0.124 18.6 N.D. means Non detectable and the detection limit is 0.025 ppm.

As shown in Table 3, in Comparative Example 3, it was confirmed that the mineral component of the low concentration was included, but in Example 7, the liquid phase did not detect any results, and in the case of solids, several times to several tens of makgeolli stock solution. The result contained the mineral component of the pear was confirmed.

It is determined by the present application that inorganic components having a high boiling point (bp, boiling point) do not volatilize during solid-liquid separation and remain in solids, so that a large amount of minerals are present. In the case of transparent makgeolli alcoholic beverages classified as, water or ethanol with low boiling point was distilled out, and the result was observed to be made of makgeolli alcoholic beverage containing only inorganic water and alcohol.

Example 8

Vitamin B1 and B2, ethanol, and Parnesol, which are anticancer agents, were included in the powdered solid and the liquid transparent Makgeolli alcoholic beverage, which were separated in Example 6, and the powdered solid was extracted by solid phase extraction. For liquid transparent makgeolli alcoholic beverages, liquid-liquid extraction was used.

The solution extracted by the extraction method was concentrated to 10 ml by distillation under reduced pressure using a rotary evaporator, and GC / MS (Agilent 6890N Gas Chromatograph / Leco PEGASUS III Time of Flight Mass Spectrometer) confirmed the beneficial elements to the human body. The results are shown in Table 4, and Comparative Example 4 was carried out in the same manner as in Example 8, except that the makgeolli stock solution prepared in Example 1 was vigorously shaken to collect a uniform sample and then liquid-liquid extraction was performed. .

division Analysis item Vitamin
B1 (ppb) Vitamin
B2 (ppb) Ethanol
(%) Parnesol
(ppb) Example 8 Liquid N.D. N.D. 7.6 N.D. Solids 62 6.8 N.D. 1,100 Comparative Example 4 11 1.4 7.1 260 N.D. means Non detectable, and the detection limit is 1.0 ppb of Vitamin B1, B2, Parnesol, and 1.0 ppm of ethanol.

As can be seen in the analytical results of Table 4, in Comparative Example 4, the concentration of ethanol is 7.1% Makgeolli, vitamin B1 and vitamin B2 and the anticancer drug can be confirmed to maintain a constant concentration, Rotary evaporator In the case of a liquid transparent Makgeolli alcoholic beverage distilled under reduced pressure, only 7.6% of ethanol was contained and the remaining vitamins were not contained.

This was judged because only the low boiling point ethanol was distilled by the reduced pressure distillation as in Example 7, on the contrary, the solid content did not contain any ethanol, and it was confirmed that a large amount of vitamins and anticancer agents beneficial to the human body were contained. .

Therefore, when the technical spirit of the present application is applied, the liquid alcohol layer is provided as an alcoholic beverage through a suitable liquid-liquid separation process of a traditional liquor containing a mixture of alcohol powder and liquor zucchini, which is produced when manufacturing makgeolli, Solid liquor forge layer without liquid can be provided as a dietary supplement through the drying and grinding step.

In addition, the dietary supplement powder provided by drying and pulverizing the liquor forge obtained in the separation step in the form of powder is Ca, Na, K, Mg, Fe, P and the like as shown in the analysis data of Table 3 and Table 4 above. It is provided as a powder containing various mineral ingredients and active ingredients such as Vitamin B1, Vitamin B2, and Parnesol, and it is provided by mixing it with other excipients together with excipients, or if it is desired to further enhance the pharmacological effect. It may be mixed / contained with other proven pharmacological ingredients and provided as a dietary supplement in the form of tablets or capsules.

1 is a photographic example of applying the technical idea of the present application is applied to the solid-liquid separation process of makgeolli using a rotary evaporator (to omit a separate code description).

Claims

In the manufacturing method for obtaining traditional liquor and health supplements in the traditional liquor manufacturing process using grain,
A first step of separating liquor liquor and liquor from liquor liquor mixed with alcohols and grains produced by microbial fermentation during the traditional liquor manufacturing process by a solid-liquid separation process;
The liquid alcohol obtained through the first separation step is provided as a traditional liquor, and the liquor fork and turbid matter obtained through the separation step are used as powders of health supplements containing no alcohols and water through the drying and grinding steps. Obtained step;
Traditional liquor and manufacturing method for obtaining a health supplement characterized in that it comprises a.

The method of claim 1,
Solid-liquid separation process for separating the liquor fork and turbid matter mixed with the alcohols and grains is a solid-liquid separation method selected from the density separation method, dehydration method by centrifugation, reduced pressure filtration method, pressure filtration method Method of obtaining traditional liquor and health supplements, characterized in that.

The method of claim 2,
Method for obtaining traditional liquor and health supplements, characterized in that the dehydration by the belt press is applied during the application process of the solid-liquid separation process.

The method of claim 1,
The liquor fork drying step is characterized in that the drying step is selected from a high temperature atmospheric pressure heating method, a high temperature reduced pressure heating method, a drying method at room temperature pressure reduction, a drying method at room temperature and atmospheric pressure, a drying method under reduced pressure by freezing and freezing. How to get traditional liquor and health supplements.

The method of claim 1,
The liquor fork mill grinding step is 1.0 ~ 3.5 mm particle size by the mill selected from turbo mill, super micro mill, roller mill, Raymond mill, port mill, tube mill, conical mill, jet mill, jet mill, vibrating ball mill Method of obtaining traditional liquor and health supplements, characterized in that it is crushed.

In the dietary supplement obtained through the traditional manufacturing process using grain,
The liquor of alcohol liquor mixed with alcohols and grains produced by microbial fermentation during the process of traditional liquor separation is separated from the liquid alcohol and liquor liquor by the solid-liquid separation process, and liquor liquor obtained in the above separation step. Health supplements characterized in that the powder is provided by drying and pulverizing.

The method according to claim 6,
A dietary supplement characterized in that the powder obtained by drying and grinding the liquor fork is mixed / contained with other excipients or other pharmacological ingredients and provided as a tablet or capsule.