KR20050047508A - Food Additives Antimicrobial Compositions and Manufacturing Methods Thereof - Google Patents
Food Additives Antimicrobial Compositions and Manufacturing Methods Thereof Download PDFInfo
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- KR20050047508A KR20050047508A KR1020050010878A KR20050010878A KR20050047508A KR 20050047508 A KR20050047508 A KR 20050047508A KR 1020050010878 A KR1020050010878 A KR 1020050010878A KR 20050010878 A KR20050010878 A KR 20050010878A KR 20050047508 A KR20050047508 A KR 20050047508A
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- silver
- powder
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- dissolved
- colloidal silver
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- 235000013373 food additive Nutrition 0.000 title claims abstract description 21
- 239000002778 food additive Substances 0.000 title claims abstract description 21
- 239000000203 mixture Substances 0.000 title claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 230000000845 anti-microbial effect Effects 0.000 title description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 66
- 239000000843 powder Substances 0.000 claims abstract description 47
- 229910052709 silver Inorganic materials 0.000 claims abstract description 34
- 239000004332 silver Substances 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 150000003839 salts Chemical class 0.000 claims abstract description 17
- 238000009835 boiling Methods 0.000 claims abstract description 14
- 239000004599 antimicrobial Substances 0.000 claims abstract description 13
- 229920002472 Starch Polymers 0.000 claims abstract description 11
- 239000012153 distilled water Substances 0.000 claims abstract description 11
- 239000002245 particle Substances 0.000 claims abstract description 11
- 235000019698 starch Nutrition 0.000 claims abstract description 11
- 239000008107 starch Substances 0.000 claims abstract description 11
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims abstract description 10
- 235000013305 food Nutrition 0.000 claims abstract description 9
- 235000000346 sugar Nutrition 0.000 claims abstract description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 7
- 239000011707 mineral Substances 0.000 claims abstract description 7
- -1 silver ions Chemical class 0.000 claims abstract description 7
- 238000001704 evaporation Methods 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 6
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229920001661 Chitosan Polymers 0.000 claims abstract description 5
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims abstract description 5
- 239000002253 acid Substances 0.000 claims abstract description 5
- 239000001506 calcium phosphate Substances 0.000 claims abstract description 5
- 235000011010 calcium phosphates Nutrition 0.000 claims abstract description 5
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 150000004676 glycans Chemical class 0.000 claims abstract description 5
- 229920001542 oligosaccharide Polymers 0.000 claims abstract description 5
- 150000002482 oligosaccharides Chemical class 0.000 claims abstract description 5
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 5
- 239000005017 polysaccharide Substances 0.000 claims abstract description 5
- 235000011009 potassium phosphates Nutrition 0.000 claims abstract description 5
- 239000001488 sodium phosphate Substances 0.000 claims abstract description 5
- 229910000162 sodium phosphate Inorganic materials 0.000 claims abstract description 5
- 239000006188 syrup Substances 0.000 claims abstract description 5
- 235000020357 syrup Nutrition 0.000 claims abstract description 5
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical class [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims abstract description 5
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims abstract description 5
- 238000004040 coloring Methods 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 229910000160 potassium phosphate Inorganic materials 0.000 claims abstract description 4
- 235000013599 spices Nutrition 0.000 claims abstract description 4
- 238000005507 spraying Methods 0.000 claims abstract 7
- 150000007513 acids Chemical class 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims 1
- 235000013336 milk Nutrition 0.000 claims 1
- 239000008267 milk Substances 0.000 claims 1
- 210000004080 milk Anatomy 0.000 claims 1
- 238000001953 recrystallisation Methods 0.000 claims 1
- 239000007921 spray Substances 0.000 abstract description 5
- 238000005868 electrolysis reaction Methods 0.000 abstract description 3
- 230000008020 evaporation Effects 0.000 abstract description 2
- 241001226615 Asphodelus albus Species 0.000 abstract 1
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 229940127554 medical product Drugs 0.000 abstract 1
- 229940098458 powder spray Drugs 0.000 abstract 1
- 150000008163 sugars Chemical class 0.000 abstract 1
- 244000052616 bacterial pathogen Species 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 2
- 239000003053 toxin Substances 0.000 description 2
- 231100000765 toxin Toxicity 0.000 description 2
- 108700012359 toxins Proteins 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 208000004898 Herpes Labialis Diseases 0.000 description 1
- YJPIGAIKUZMOQA-UHFFFAOYSA-N Melatonin Natural products COC1=CC=C2N(C(C)=O)C=C(CCN)C2=C1 YJPIGAIKUZMOQA-UHFFFAOYSA-N 0.000 description 1
- 206010067152 Oral herpes Diseases 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 241000590428 Panacea Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 241001441724 Tetraodontidae Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- FMGSKLZLMKYGDP-USOAJAOKSA-N dehydroepiandrosterone Chemical compound C1[C@@H](O)CC[C@]2(C)[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CC=C21 FMGSKLZLMKYGDP-USOAJAOKSA-N 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 206010015037 epilepsy Diseases 0.000 description 1
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000009920 food preservation Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- DRLFMBDRBRZALE-UHFFFAOYSA-N melatonin Chemical compound COC1=CC=C2NC=C(CCNC(C)=O)C2=C1 DRLFMBDRBRZALE-UHFFFAOYSA-N 0.000 description 1
- 229960003987 melatonin Drugs 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 208000020016 psychiatric disease Diseases 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 235000010199 sorbic acid Nutrition 0.000 description 1
- 239000004334 sorbic acid Substances 0.000 description 1
- 229940075582 sorbic acid Drugs 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000001384 succinic acid Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000010200 validation analysis Methods 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Inorganic Chemistry (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
본 발명은 식품첨가용 항균제의 조성물 및 그의 제조방법에 관한 것으로서, (1). 99.99% 순도의 은(銀)봉이 장착된 전기분해장치에 증류수를 넣고서 만들어진 0.005-0.015미크론 입자의 콜로이달 은(銀) 상태의 10ppm 농도의 은(銀) 콜로이달 용액 400cc 을 (2). 실리코알루민산나트륨(sodium silico aluminate(TIXOLEX 28F)) 분말 300gr에 스프레이 분사하여 분산 교반하여 함침 시킨 후 건조한 분말. (3). 각종의 미네날이 함유된 곡물의 분말(또는 전분, 구근류 분말) 300gr에 (1)의 콜로이달 은(銀 )용액 400cc를 스프레이 분사 교반하여 함침 시킨 후 건조한 분말. (4). 인산칼슘(calcium phosphates)(또는 인산칼륨분말, 인산나트륨분말)분말 300gr에 (1)의 콜로이달 은(銀 ) 용액 400cc를 스프레이 분사 교반하여 함침시킨 후 건조한 분말. (4). 키토산분말 300gr에 (1)의 콜로이달 은(銀 )용액 400cc를 스프레이 분사 교반하여 함침 시킨 후 건조한 분말. (5). 각종의 미네날이 함유된 소금(salt) 40중량%에 (1)의 콜로이달 은(銀 )용액 60중량%를 첨가하여 섭씨 100℃의 온도로 끓이면서 용해한 후 냉각시킨 용액과 수분을 증발 시킨 후 은(銀 )이온이 이온 결합된 결정화 된 소금(salt). (6). 식품 첨가물(또는 의학품) 로 지정된 미네날 분말 300gr에 (1)의 콜로이달 은(銀 )용액 400cc를 스프레이 분사 교반하여 함침 시킨 후 건조한 분말. (7). 설탕(sugar)(또는 다당류(맥아당, 물엿, 올리고당, 스테비온)) 40중량%를 (1)의 콜로이달 은(銀) 용액 60중량%에 첨가하여 섭씨 100℃의 온도로 끓이면서 용해한 후 냉각 시킨 용액과, 수분을 증발시켜 은(銀 ) 이온이 이온결합 된 결정화된 설탕(또는 다당류(맥아당, 물엿, 올리고당, 스테비온)).(8). 식품첨가용 산(acid)류 염류 및 소포제, 향신료, 식용색소 등 분말 및 액상 각각 40중량%에 (1)의 콜로이달 은(銀 )용액 각각 60중량%를 첨가하여 섭씨 50-100℃의 온도로 끓이면서 용해 후 냉각시킨 용액과 수분을 증발시킨 후 결정화 한 것에 그 특징이 있는 식품첨가용 항균제의 조성물 및 그의 제조방법.The present invention relates to a composition of a food additive antimicrobial agent and a method for producing the same, (1). 400cc silver colloidal solution with 10ppm concentration of colloidal silver of 0.005-0.015 micron particles made by adding distilled water to an electrolysis device equipped with 99.99% pure silver rod (2). Sodium silico aluminate (TIXOLEX 28F) powder spray sprayed on 300gr, dispersed, impregnated and impregnated to dry powder. (3). Dry powder after impregnating by spraying, stirring and impregnating 400cc of colloidal silver solution (1) into 300gr of powder (or starch, bulbous powder) containing various minerals. (4). Dry powder after impregnating 400 grams of a colloidal silver solution of (1) by spraying and stirring into calcium phosphates (or potassium phosphate powder, sodium phosphate powder) in 300 gr. (4). The powder was dried by impregnating 300cc of chitosan powder with 400cc of colloidal silver solution of (1) by spraying and stirring. (5). After adding 60% by weight of the colloidal silver solution of (1) to 40% by weight of salt containing various minerals, dissolving it by boiling at a temperature of 100 ° C, evaporating the cooled solution and water, (Iii) Crystallized salt in which ions are ionically bonded. (6). Dry powder after impregnating by spray spray stirring and impregnating 400cc of colloidal silver solution of (1) to 300gr of miner powder designated as a food additive (or medical product). (7). 40% by weight of sugar (or polysaccharides (maltose, starch syrup, oligosaccharide, stebion)) was added to 60% by weight of a colloidal silver solution of (1), dissolved by boiling at a temperature of 100 ° C, and cooled. Crystallized sugars (or polysaccharides (maltose, starch syrup, oligosaccharides, stevione)) in which solutions and water are evaporated to ion-bond silver ions. (8). 50 to 100 ° C by adding 60% by weight of each colloidal silver solution of (1) to 40% by weight of powders and liquids such as acid salts, antifoaming agents, spices, food colorings, etc. A composition of a food-added antimicrobial agent characterized by the crystallization after evaporation of a solution and water cooled after dissolution and boiling by boiling with a method for producing the same.
Description
본 발명은 식품첨가용 항균제의 조성물 및 그의 제조방법에 관한 것으로서, 통상의 식품첨가용 살균제는 염소제와 과산화수소, 보존료로 안식향산, 소르빈산 및 그의 염류, 파라옥시안식향산, 식품첨가물의 사용 허용기준에 따라 인체에 미치는 독성이 있으며, 식품첨가물의 PH 및 조리온도, 보관상태, 식품의 보존기간에 따라 살균 및 보존의 기능이 저하 및 소멸 등의 문제점이 있고, 일반적으로 사용하기에는 제한적인 문제점을 가지고 있는바, 본 발명의 식품첨가용 항균제는 99.99%순도의 순수한 은(銀 )을 전기분해장치에 증류수를 넣고서 만들어진 0.005-0.015미크론 입자의 콜로이달 은(colloidal silver)상태의 10ppm 농도의 콜로이달 은(colloidal silver) 용액으로서, FDA의 공식적인 입장은 콜로이달 은(銀 )에 대하여 1991년 가을 다음과 같은 입장을 밝혔다. 콜로이달 은(銀 )은 1938년 이전의 약으로 간주된다. 원래의 방식으로 제조되고, 1938년과 동일한 용도로 사용되고 광고되기만 한다면 특별히 안전성이나, 유효성 자료를 제출하지 않아도 유통될 수 있다. 라고 하였고, 민간요법으로서 FDA에서 특별히 승인 받을 필요가 없다. 식약청에서도 FDA에 준하여 특별한 승인을 받을 필요가 없다고 승인하였다.The present invention relates to a composition of a food additive antimicrobial agent and a manufacturing method thereof, a conventional food additive disinfectant is a chlorine agent and hydrogen peroxide, a preservative as benzoic acid, sorbic acid and its salts, paraoxybenzoic acid, food additives according to the acceptance criteria It is toxic to human body, and there are problems such as deterioration and extinction of sterilization and preservation according to pH and cooking temperature of food additives, storage condition, and food preservation period. , Colloidal silver of 10ppm concentration of colloidal silver (colloidal silver) of 0.005-0.015 micron particles made by adding distilled water to the electrolysis device of pure silver of 99.99% purity of the present invention As a silver solution, the FDA's official position on colloidal silver in the fall of 1991 was: Colloidal silver is considered a drug before 1938. If manufactured in the original manner, and used and advertised for the same purposes as 1938, it can be distributed without special safety or validation data. It is a folk remedy and does not need to be specifically approved by the FDA. The FDA also approved that there is no need for special approval under the FDA.
이와 같이 만들어진 콜로이달 은(colloidal silver)용액을 식품첨가물 제조품목 허가를 받은 실리코알루민산나트륨(sodium silico aluminate)분말, 곡물의 분말(또는 전분, 구근류분말), 인산칼륨(potassium phosphates), 인산나트륨(sodium phosphates), 인산칼슘(calcium phosphates), 키토산분말, 소금(salt), 식품첨가물(또는 금속이온, 의약품)로 지정된 미네날분말, 설탕(sugar)(또는 다당류(맥아당, 물엿, 올리고당), 식품첨가용 산(acid)류 및 염류, 소포제, 향신료, 식용색소 등에 각각 함침 및 이온 결합하여 액상 및 결정화 분말 등으로 만든 것을 식품의 제조시에 식품전체 중량비에 1중량% 첨가하여 항균력을 부여하는 데에 그 특징이 있는 식품첨가용 항균제의 조성물 및 그의 제조 방법.The colloidal silver solution prepared in this way was used as a food additive manufacturing product licensed sodium silico aluminate powder, grain powder (or starch, bulbous powder), potassium phosphates, sodium phosphate mineral phosphates, calcium phosphates, chitosan powder, salt, mineral powders designated as food additives (or metal ions, pharmaceuticals), sugar (or polysaccharides (maltose, starch syrup, oligosaccharides), food) Impregnated and ion-bonded with acids, salts, defoamers, spices, food colorings, etc., respectively, to make liquid and crystallized powders. The composition of the food additive antimicrobial agent characterized by the above, and its manufacturing method.
..
본 발명을 실시예를 들어 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail with reference to Examples.
실시예 1Example 1
본 발명은 (1). 통상의 가정용전기 교류 전원(AC) 220볼트(V)를 사용하여 직류(DC) 변환장치를 통하여 직류 28-30볼트(V)에 200밀리암페어(mA)의 전류가 통하는 음극과 양극에 순도 99.99%의 은(銀 )봉이 조립된 통상의 전기분해 장치에 증류수를 1리트를 넣고서 5시간 전원을 연결하여 은(銀) 입도가 0.005-0.015미크론의 콜로이달 은(colloidal silver) 10PPM의 용액을 만들었다.The present invention (1). Purity 99.99 Purity for the cathode and anode through which 200 milliamps (mA) of current flows through a DC converter to a DC current of 28-30 volts (V) using a typical household electrical alternating current (AC) 220 volts (V). 1 liter of distilled water was added to a conventional electrolysis device in which% silver rods were assembled, and the power was connected for 5 hours to prepare a solution of colloidal silver 10PPM having a silver particle size of 0.005-0.015 microns. .
실시예 2.Example 2.
(1). 실시예1의 (1) 콜로이달 은(colloidal silver)용액 400cc를 실리코알루민산나트륨(sodium silico aluminate)분말 300gr에 스프레이 분사하여 분산 교반하여 함침 시킨 후 건조한 분말.(One). (1) 400 cc of colloidal silver solution of Example 1 was spray-sprayed and dispersed by impregnating with 300 g of sodium silico aluminate powder, and then dried to dry powder.
실시예 3.Example 3.
(1). 실시예1의 (1). 콜로이달 은(colloidal silver )용액 400cc를 곡물의 분말(또는 전분, 구근류전분 분말) 300gr에 스프레이 분사하여 분산 교반하여 함침 시킨 후 건조한 분말.(One). Example 1 (1). 400cc colloidal silver solution is spray-sprayed to 300gr of grain powder (or starch, bulbous starch powder), dispersed, impregnated, and then dried.
실시예 4.Example 4.
(1). 실시예1의 (1). 콜로이달 은(colloidal silver )용액 400cc를 인산칼슘(calcium phosphates)(또는 인산칼륨, 인산나트륨)분말 300gr에 스프레이 분사하여 분산 교반하여 함침 시킨 후 건조한 분말.(One). Example 1 (1). 400cc colloidal silver solution spray sprayed on calcium phosphate (or potassium phosphate, sodium phosphate) powder 300gr, dispersed, stirred, impregnated to dry powder.
실시예 5.Example 5.
(1). 실시예1의 (1). 콜로이달 은(colloidal silver)용액 400cc를 키토산분말 300gr에 스프레이 분사하여 분산 교반 후 건조한 분말.(One). Example 1 (1). Spray powder 400cc colloidal silver solution to 300gr of chitosan powder to disperse and stir dry powder.
실시예 6.Example 6.
(1). 실시예1의 (1).콜로이달 은(colloidal silver)용액 60중량%에 소금(salt) 40중량%를 첨가하여 섭씨 100℃의 온도로 끓이면서 용해한 후 냉각시킨 용액과, 섭씨 100℃의 온도로 끓이면서 수분을 증발 시킨 후 은(silver)이온이 소금(salt)이온과 이온 결합되어 재결정화 된 소금(salt).(One). Example 1 (1). To 60% by weight of colloidal silver solution (40% by weight of salt) added to the salt (salt) to boil at 100 ℃ Celsius, dissolved in a solution and cooled to a temperature of 100 ℃ The salt is recrystallized by silver ion ions combined with salt ions after evaporating moisture while boiling.
실시예 7.Example 7.
(1). 실시예1의 (1). 콜로이달 은(colloidal silver)용액 400cc를 식품첨가물로 지정된 미네날(또는 금속염)분말 300gr에 스프레이 분사하여 분산 교반 후 건조한 분말.(One). Example 1 (1). Powder sprayed by colloidal silver solution 400cc spray sprayed to 300gr of mineral (or metal salt) powder designated as food additives, and then dispersed and agitated.
실시예 8.Example 8.
(1). 실시예1의 (1). 콜로이달 은(colloidal silver)용액 60중량%에 설탕(sugar)(또는 다당류(맥아당, 물엿, 올리고당, 스테비온))40중량%를 첨가하여 섭씨 100℃의 온도로 끓이면서 용해한 후 냉각시킨 용액과, 섭씨 100℃의 온도로 끓이면서 수분을 증발시켜 은(silver)이온이 이온결합된 결정화 된 설탕.(One). Example 1 (1). 60% by weight of colloidal silver solution (40% by weight of sugar (or polysaccharides (maltose, starch syrup, oligosaccharide, stebion)) was added to boil at a temperature of 100 ℃ to dissolve and then cooled, Crystallized sugar in which silver ions are ion-bonded by boiling water at a temperature of 100 ° C and evaporating moisture.
실시예 9.Example 9.
(1). 실시예1의 (1).콜로이달 은(colloidal silver)용액 60중량%에 식품첨가용 산(acid)류 (또는 염류, 소포제, 향신료, 식용색소)등의 분말 및 액상에 각각 40중량%를 첨가하여 섭씨 50-100℃의 온도로 끓이면서 용해 후 냉각 시킨 용액과, 섭씨 50-100℃의 온도로 끓이면서 수분을 증발시킨 후 재결정화 한 것에 그 특징이 있는 것.(One). Example 1 (1). 60% by weight of colloidal silver solution, 40% by weight in powders and liquids, such as acids (or salts, antifoams, spices, food colorings) for food addition. It is characterized by being recrystallized after evaporation of water while boiling and dissolving the solution after boiling while boiling at a temperature of 50-100 ° C. and boiling at a temperature of 50-100 ° C.
위와 같이 실시예를 들어서 살펴본바와 같이 본 발명의 중요 성분중의 콜로이달 은(colloidal silver)이 항균력의 기능을 갖는 그 화학적 특징 및 기능을 살펴보면 다음과 같다.Looking at the chemical characteristics and functions of the colloidal silver (colloidal silver) among the important components of the present invention as shown in the examples as described above has the function of antibacterial activity as follows.
은(silver)의 색상은 회백색의 금속이나 분말의 경우는 회색을 띤다. 비중은 10-12이며, 모스경도는 2.5-3, 용융점은 960.5℃로서 순은의 경우 대기중에 방치 하든가 또는 가열하여도 녹이 생기지 않는다. 은 실험결과 지상의 모든 단세포 병균을 죽일 수 있음이 증명되었고, 은이 단세포 병균의 소화나 호흡 등의 신진대사 작용을 하는 특수한 효소의 작용을 무력화시켜 결과적으로 병균을 살균 한다는 게 가장 유력한 학설이며, 은과 접촉해 6분 이상 생존 할 수 있는 세균은 없다고 알려졌다. 은(銀 )은 병균의 신진대사를 막아 살균하는 것과 더불어 금속의 은(metalic silver)이 방출하는 은이온(Ag+)의 전기적부하는 병균의 생식기능을 제거한다. 그래서 질병치료에도 중요한 역할을 한다. 은(銀 )은 매우 적은 량이라도 물에 녹아 들어가면 물속의 미생물을 죽이는 신기한 작용을 한다. 1리트(L)의 물을 소독하는 데는 수백만 분의 1그람(gr)만 있어도 충분하다. 은(銀 )은 복어알이나, 독버섯, 독극물처럼 인체에 해로운 독소가 함유된 음식물에서는 변색이 되어 독소 유무를 판별할 수 있고, 유황성분과 반응하면 독특한 색을 내기도 한다. 은(銀 )은 간질 및 경기 등 정신질환과 냉 대하와 같은 부인병 예방 및 치료에 쓰이며, 항생물질은 대략 5-6가지의 병원체들을 죽이는 반면 은(銀 )은 650여종을 죽인다.The color of silver is grayish white for grayish metals or powders. Specific gravity is 10-12, Mohs hardness is 2.5-3, melting point is 960.5 ℃, and pure silver does not rust even if left in the air or heated. The experiment proved that it can kill all single cell germs on the ground, and the most powerful theory is that silver neutralizes the action of special enzymes that metabolize the single cell germs, such as digestion or respiration. It is known that no bacteria can survive in contact for more than 6 minutes. Silver prevents germ metabolism and sterilizes, as well as the electrical load of silver ions (Ag +) released by metallic silver removes germs. Therefore, it plays an important role in the treatment of diseases. Silver (銀) is a very small amount of dissolved in water to act as a mysterious killing of microorganisms in the water. Millions of grams of gr are sufficient to disinfect one liter (L) of water. Silver (銀) discolors in foods containing toxins that are harmful to the human body, such as blowfish eggs, poisonous mushrooms, and poisons, and can determine the presence or absence of toxins. Silver is used to prevent and treat mental illnesses such as epilepsy and race and gynecological diseases such as cold sores. Antibiotics kill about 5-6 pathogens, while silver kills about 650 species.
현재 미국에서는 콜로이달 은(colloidal silver)를 멜라토닌, DHEA와 더불어 만병통치약으로 건강식품 상점에서 보급되고 있으며, FDA승인 자연항생제로 사용하고 있다. 본 발명의 조성물중 실리코알루민산나트륨(sodium silico aluminate)는 식품위생법 제 22조 제2항 및 동법시행규칙 제25조의 규정에 의하여 식품첨가물의 품목제조허가를 받은 것으로서, 백색의 미세한분말로 무미, 무취이다. 또한 식품첨가물인 갑각류에서 추출한 키토산분말, 인산칼슘, 인산칼륨, 인산나트륨, 설탕, 소금, 미네날분말, 산(acid)류인 호박산, 구연산나트륨 등을 콜로이달 은(colloidal silver)이온의 충진제로 사용하여 식품의 항균기능을 부여한 것에 그 특징이 있는 식품첨가용 항균제의 조성물 및 그의 제조방법.In the United States, colloidal silver, along with melatonin and DHEA, is widely used in health food stores as a panacea, and is used as an FDA-approved natural antibiotic. Sodium silico aluminate in the composition of the present invention has been approved for the production of food additives in accordance with the provisions of Article 22 (2) of the Food Sanitation Act and Article 25 of the Enforcement Regulations of the Act, white fine powder tasteless, It is odorless. In addition, chitosan powder, calcium phosphate, potassium phosphate, sodium phosphate, sugar, salt, mineral powder, acidic succinic acid and sodium citrate are used as fillers for colloidal silver ions. The composition of the food additive antimicrobial agent which has the characteristic which gave the antibacterial function of food, and its manufacturing method.
상술한 바와 같이 본 발명의 항균제를 1중량% 첨가하여 산업 환경 연구센터에서 항균력 실험 결과(KATRI NO BSO4-00002121) 대장균 99.9%, 황색 포도상구균 99.9%의 항균력 실험 결과를 확인 하였다.As described above, by adding 1% by weight of the antimicrobial agent of the present invention, the antimicrobial activity test result (KATRI NO BSO4-00002121) of E. coli 99.9% and Staphylococcus aureus 99.9% were confirmed in the Industrial Environment Research Center.
Claims (8)
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| KR1020050010878A KR20050047508A (en) | 2005-02-02 | 2005-02-02 | Food Additives Antimicrobial Compositions and Manufacturing Methods Thereof |
| PCT/KR2006/000314 WO2006083092A1 (en) | 2005-02-02 | 2006-01-27 | Antibacterial agent composition and manufacturing method thereof |
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|---|---|---|---|---|
| KR100848184B1 (en) * | 2006-03-16 | 2008-07-23 | 전창호 | Process for preparing low sodium chloride compound |
| KR101108762B1 (en) * | 2005-05-03 | 2012-02-15 | 은나노기술주식회사 | Composition of detergent for cleaning a cookroom and their manufacturing process |
| KR101917180B1 (en) * | 2018-05-03 | 2019-01-25 | 김동술 | Method of manufacturing silica based food additive |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH04321628A (en) * | 1991-04-18 | 1992-11-11 | Kanebo Ltd | Antimicrobial agent consisting of colloid particle of silver |
| JP2000247822A (en) * | 1999-02-23 | 2000-09-12 | Toyo Beauty Kk | Liquid antimicrobial composition |
| KR100352643B1 (en) * | 1999-12-03 | 2002-09-12 | 정영기 | natural antiseptic substance made from mixture of natural mugwort and silver |
| JP2002173405A (en) * | 2000-12-04 | 2002-06-21 | Hidehiro Tagusari | Sterilizing method with colloidal silver and sterilization material using the same |
| KR20040106843A (en) * | 2003-06-11 | 2004-12-18 | 안정오 | Method of treating cereal with gold or silver by immersing cereal in gold or silver solution having effect of preventing pests |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR101108762B1 (en) * | 2005-05-03 | 2012-02-15 | 은나노기술주식회사 | Composition of detergent for cleaning a cookroom and their manufacturing process |
| KR100848184B1 (en) * | 2006-03-16 | 2008-07-23 | 전창호 | Process for preparing low sodium chloride compound |
| KR101917180B1 (en) * | 2018-05-03 | 2019-01-25 | 김동술 | Method of manufacturing silica based food additive |
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