KR101596687B1 - Deodorizers comprising phytoncide - Google Patents

Deodorizers comprising phytoncide Download PDF

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KR101596687B1
KR101596687B1 KR1020150106890A KR20150106890A KR101596687B1 KR 101596687 B1 KR101596687 B1 KR 101596687B1 KR 1020150106890 A KR1020150106890 A KR 1020150106890A KR 20150106890 A KR20150106890 A KR 20150106890A KR 101596687 B1 KR101596687 B1 KR 101596687B1
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extract
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purified water
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김윤환
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주식회사 에코제로
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
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  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The present invention relates to a deodorizer containing phytoncide containing 20-24 parts by weight of a phytoncide extract, 5-9 parts by weight of an Orostachys japonicus extract, and 10-14 parts by weight of a grape extract for 100 parts by weight of purified water, thereby being harmless to a humanbody, and having strong sterilization and deodorization function by comprising a phytoncide oil and using only a natural material.

Description

피톤치드를 함유한 탈취제 {Deodorizers comprising phytoncide} Deodorizers comprising phytoncide < RTI ID = 0.0 >

본 발명은 피톤치드를 함유한 탈취제에 관한 것이다.The present invention relates to a deodorant containing phytoncide.

대한민국 등록특허 제0634943호(등록일자: 2006. 8. 31., 발명의 명칭: 항균 탈취성 상온 촉매 코팅제 및 그의 제조방법)는 금속수산화물 0.1∼20 중량%, 실리카겔, 제올라이트, 활성백토 등에서 선택된 1종 이상의 무기 흡착제 0.1∼5 중량%, 입자경 5∼15 nm의 은콜로이드로 구성된 나노실버 0.0001∼0.1 중량%에 피톤치드오일 0.01∼5 중량%, 바인더 0.1∼10 중량% 및 음이온 계면활성제, 양이온 계면활성제, 비이온 계면활성제 등에서 선택된 1종 이상의 계면활성제 0.01∼5.0 중량%를 첨가하고, 물, 저급 알코올, 고급 알코올 또는 이들의 혼합용액에서 선택된 용매 70∼99 중량%에 분산 용해시키킨 항균 탈취성 상온 촉매 코팅제가 개시되어 있다.Korean Patent No. 0634943 (filed on August 31, 2006, entitled "Antimicrobial and Deodorizing Room Temperature Catalyst Coating Agent and Method for Producing the Same"), 0.1 to 5% by weight of an inorganic adsorbent and 0.1 to 5% by weight of a silver colloid having a particle diameter of 5 to 15 nm, 0.01 to 5% by weight of phytoncide oil, 0.1 to 10% by weight of a binder and an anionic surfactant, 0.01 to 5.0% by weight of at least one surfactant selected from water, a lower alcohol, a higher alcohol, or a mixed solution thereof is dispersed in 70 to 99% by weight of a solvent selected from the group consisting of water, A catalyst coating agent is disclosed.

이러한 종래 기술은, 실내에서 발생하는 포름알데히드 등 VOC와 생활 악취가스를 상온에서 제거할 수 있도록 상온에서 작용하는 촉매물질과 천연식물중 유효성분을 이용하여 촉매에 의한 산화분해 그리고 천연식물질에 의한 중화 반응을 통해 유해가스 등을 제거할 수 있다고 주장하는 반면, 화학물질이 포함되어 있어 자연친화적이지 못한 단점이 있었다.Such prior art techniques are based on catalytic materials acting at room temperature to remove VOCs and living odor gases such as formaldehyde generated in the room at room temperature, oxidative decomposition by catalysts using active ingredients in natural plants, While it claims to be able to remove harmful gases through neutralization reaction, it has a disadvantage that it is not environmentally friendly because it contains chemical substances.

또한, 대한민국 등록특허 제1439385호(등록일자: 2014. 9. 2., 발명의 명칭: 탈취 및 살균력이 우수한 피톤치드 성분이 함유된 천연 조성물)는 탈취제, 방향제, 항균제 및 입욕제를 위한 천연 조성물로서, 편백나무 추출물 100 중량부, 라벤더 추출물 90 내지 100 중량부, 로즈마리 추출물 40 내지 100 중량부 및 약재추출물 25 내지 100 중량부로 이루어지며, 상기 편백나무 추출물은 정제수 100 중량부에 편백나무 분말 15 내지 25 중량부를 혼합하고, 증류추출법을 이용하여 120 내지 130℃의 온도에서 30 내지 50분 동안 가열하여 제조되고, 상기 라벤더 추출물은 정제수 100 중량부에 라벤더 10 내지 20 중량부를 혼합하고, 증류추출법을 이용하여 120 내지 130℃의 온도에서 30 내지 50분 동안 가열하여 제조되며, 상기 로즈마리 추출물은 정제수 100 중량부에 로즈마리 10 내지 20 중량부를 혼합하고, 증류추출법을 이용하여 120 내지 130℃의 온도에서 30 내지 50분 동안 가열하여 제조되고, 상기 약재는 박하로 이루어지는 것을 특징으로 하는 탈취 및 살균력이 우수한 피톤치드 성분이 함유된 천연 조성물이 개시되어 있다.Korean Patent No. 1439385 (Registered on April 9, 2014, title of the invention: Natural composition containing phytoncide component having excellent deodorizing and sterilizing power) is a natural composition for deodorant, aromatic, antibacterial agent and bathing agent, 100 to 100 parts by weight of an extract of Chamaecyparis obtusa, 90 to 100 parts by weight of a lavender extract, 40 to 100 parts by weight of a rosemary extract and 25 to 100 parts by weight of a medicinal extract, And the mixture is heated at a temperature of 120 to 130 DEG C for 30 to 50 minutes using a distillation extraction method. The lavender extract is prepared by mixing 10 to 20 parts by weight of lavender with 100 parts by weight of purified water, adding 120 To 130 < 0 > C for 30 to 50 minutes, wherein the rosemary extract is prepared by mixing 100 parts by weight of purified water with 10-20 parts by weight of rosemary And the mixture is heated at a temperature of 120 to 130 DEG C for 30 to 50 minutes by distillation extraction. The natural composition containing the phytonchip component having excellent deodorizing and sterilizing power, Lt; / RTI >

이러한 종래 기술은, 탈취 및 살균력이 우수한 피톤치드 성분이 함유된 천연 조성물은 중금속, 포름알데히드 및 메틸알코올과 같은 유해성분이 함유되어 있지 않고, 우수한 탈취력과 항균력을 나타내며 낮은 피부자극성을 나타내어, 탈취제, 방향제, 항균제 및 입욕제 등에 사용될 수 있는 탁월한 효과를 나타내는 것으로 주장하는 반면, 위와 같은 효과가 단순 피톤치드로 인한 것임에 불과한 문제점이 있었다.Such a conventional art has shown that a natural composition containing a phytoncide component having excellent deodorizing and sterilizing power does not contain harmful components such as heavy metals, formaldehyde and methyl alcohol, exhibits excellent deodorizing power and antibacterial power, exhibits low skin irritation, Antimicrobial agent, bathing agent and the like, while the above-mentioned effect is caused by the simple phytoncide.

또한, 대한민국 등록특허 제0803110호(등록일자: 2008. 2. 4., 발명의 명칭: 시멘트독 제거 및 휘발성 유기화합물 흡착용 조성물)는 바인더, 계면활성제 및 용매를 포함하고, ⅰ) 대나무 수액으로부터 추출한 테르펜, 규산 및 이들의 조합으로 이루어진 군에서 선택된 1종의 식물성 정유, 및 ⅱ) 셀룰로오스, 포도당, 알긴산, 녹말 및 이들의 조합으로 이루어진 군에서 선택된 1종의 천연 고분자를 전자선 그라프트 중합하여 제조된 텐타클(tentacle) 구조의 천연 그라프트 중합체를 포함하는 시멘트독 제거용 또는 휘발성 유기화합물 흡착용 조성물이 개시되어 있다.Korean Patent No. 0803110 (registered on Feb. 4, 2008, title of the invention: a composition for removing cement poison and adsorbing volatile organic compounds) comprises a binder, a surfactant and a solvent, and comprises: i) (Ii) one kind of natural polymer selected from the group consisting of cellulose, glucose, alginic acid, starch, and a combination thereof is subjected to electron beam graft polymerization to produce a plant essential oil selected from the group consisting of terpene, Discloses a composition for removing cement poison or adsorbing a volatile organic compound containing a natural graft polymer having a tentacle structure.

이러한 종래 기술은, 시멘트독을 비롯하여 각종 휘발성 유기화합물을 제거함으로써 새집 증후군 또는 새차증후군의 해소에 적용될 수 있다고 주장하고 있으나, 천연 그라프트 중합체의 제조방법이나 구성에 대하여 상세한 설명이 없이 실시가 용이하지 못한 단점이 있었다.Such prior art claims that it can be applied to the elimination of sick house syndrome or New Car Syndrome by removing various volatile organic compounds including cement poison, but it is easy to carry out without detailed description of the method and composition for producing natural graft polymer There were disadvantages.

상기와 같은 문제점을 해결하고자 창출된 본 발명의 목적은, 피톤치드 오일을 포함하고 천연 물질만을 활용하여 인체에 무해하고 살균 및 강력한 탈취 기능을 갖는 피톤치드를 함유한 탈취제를 제공하는 데 있다.An object of the present invention is to provide a deodorant containing phytoncide oil and using phytoncide oil and containing phytoncide which is harmless to the human body and has a strong deodorizing function by utilizing only natural substances.

이러한 본 발명의 목적은, 정제수 100 중량부에 대하여, 피톤치드 추출물 20 ~ 24 중량부, 와송 추출물 5 ~ 9 중량부 및 포도 추출물 10 ~ 14 중량부를 함유하는 피톤치드를 함유한 탈취제에 의해 달성될 수 있다.The object of the present invention can be achieved by a deodorant containing phytoncide containing 20 to 24 parts by weight of a phytoncide extract, 5 to 9 parts by weight of an extract of Wassong extract and 10 to 14 parts by weight of a grape extract, based on 100 parts by weight of purified water .

바람직하게는, 본 발명의 상기 피톤치드 추출물은, a) 편백나무 칩 100 중량부에 대하여, 편백잎 20 ~ 30 중량부 및 천일염 5 ~ 7 중량부를 혼합한 후 80 ~ 95℃에서 30 ~ 45분 가열하sm는 단계와, b) 솔잎 4 ~ 8 중량부 및 송진 1 ~ 2.4 중량부를 더 첨가한 후 40 ~ 55℃에서 10 ~ 20분 가열하면서 살구씨 오일 0.2 ~ 0.4 중량부를 혼합한 다음 서냉하는 단계와; c) 정제수 200 중량부 및 일랑일랑 오일 0.2 ~ 0.5 중량부를 더 첨가한 후 밀폐된 상태로 120 ~ 150℃에서 10 ~ 12시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 한다.Preferably, the phytoncide extract of the present invention is obtained by a) mixing 20 to 30 parts by weight of white cotton leaves and 5 to 7 parts by weight of sunflower seeds per 100 parts by weight of the white cotton chips, heating at 80 to 95 ° C for 30 to 45 minutes Adding b) 4 to 8 parts by weight of pine needles and 1 to 2.4 parts by weight of pine needles, heating the mixture at 40 to 55 ° C for 10 to 20 minutes, mixing 0.2 to 0.4 parts by weight of apricot seed oil, Wow; c) 200 parts by weight of purified water and 0.2 to 0.5 parts by weight of ylang ylang oil, and heating the mixture at 120 to 150 ° C for 10 to 12 hours in a sealed state, followed by filtration.

바람직하게는, 본 발명의 상기 와송 추출물은, a) 건조된 와송잎 100 중량부에 대하여, 건조된 와송꽃 4 ~ 10 중량부, 민들레 10 ~ 30 중량부 및 죽염 4 ~ 9 중량부를 혼합한 후 120 ~ 145℃에서 5 ~ 8분 가열하는 단계와; b) 정제수 400 ~ 450 중량부, 솔잎 10 ~ 12 중량부 및 오동자 분말 4 ~ 8 중량부를 더 첨가하여 120 ~ 145℃에서 24 ~ 28시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 한다.Preferably, the wakoshi extract of the present invention is obtained by a) mixing 4 to 10 parts by weight of dried hanbong flower, 10 to 30 parts by weight of dried hanbong flower and 4 to 9 parts by weight of bamboo salt with respect to 100 parts by weight of dried wanbai Heating at 120 to 145 ° C for 5 to 8 minutes; b) 400 to 450 parts by weight of purified water, 10 to 12 parts by weight of pine needles and 4 to 8 parts by weight of a powder of mica powder, followed by heating at 120 to 145 ° C for 24 to 28 hours, followed by filtration.

바람직하게는, 본 발명의 상기 포도 추출물은, a) 정제수 100 중량부에 대하여, 건조된 포도 껍질 30 ~ 35 중량부 및 포도씨 분말 10 ~ 13 중량부를 혼합한 후 180 ~ 230℃에서 12 ~ 15 시간 가열한 다음 서냉하는 단계와; b) 정제수 50 ~ 70 중량부 및 포도씨 분말 10 ~ 15 중량부를 더 첨가한 후 80 ~ 95℃에서 2 ~ 4시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 한다.Preferably, the grape extract of the present invention comprises: a) 30 to 35 parts by weight of dried grape skin and 10 to 13 parts by weight of dried grape seed powder per 100 parts by weight of purified water, followed by stirring at 180 to 230 ° C for 12 to 15 hours Heating and then slowly cooling; b) adding 50 to 70 parts by weight of purified water and 10 to 15 parts by weight of grape seed powder, heating at 80 to 95 ° C for 2 to 4 hours, and then filtering.

바람직하게는, 본 발명의 마전자 추출물 3 ~ 8 중량부 또는 해마 추출물 0.01 ~ 0.13 중량부를 더 함유하되, 상기 마전자 추출물은, a) 마전자 100 중량부와 천일염 3 ~ 5 중량부를 혼합한 후 120 ~ 150℃에서 5분 간격으로 10회 가열하는 단계와; b) 정제수 300 중량부, 구기자 5 ~ 9 중량부 및 건조된 민들레 뿌리 10 ~ 13 중량부를 혼합하여 180 ~ 230℃에서 5 ~ 7 시간 가열한 다음 여과하여 제조되고, 상기 해마 추출물은, 정제수 100 중량부에 대하여, 건조된 해마 1 ~ 3 중량부를 혼합한 후 50 ~ 55℃에서 120 ~ 150분간 가열한 후 여과하여 제조되는 것을 특징으로 한다.Preferably, the horsetail extract further comprises 3 to 8 parts by weight of the horsetail extract of the present invention or 0.01 to 0.13 parts by weight of the horsetail extract, wherein the horsetail extract is obtained by mixing a) 100 parts by weight of hemp and 3 to 5 parts by weight of sunflower Heating at 120 to 150 ° C for 10 times at intervals of 5 minutes; b) 300 parts by weight of purified water, 5 to 9 parts by weight of ginger and 10 to 13 parts by weight of dried dandelion root are mixed and heated at 180 to 230 ° C for 5 to 7 hours and then filtered. The hippocampus extract is prepared by adding 100 parts by weight of purified water 1 to 3 parts by weight of dried hippocampus is mixed and heated at 50 to 55 ° C for 120 to 150 minutes, followed by filtration.

이상과 같은 본 발명은 피톤치드 오일을 포함하고 천연 물질만을 활용하여 인체에 무해하고 살균 및 강력한 탈취 기능을 구현할 수 있는 효과가 있다.As described above, the present invention has an effect that phytoncide oil is contained and only natural materials are used, so that it is harmless to the human body and disinfection and strong deodorizing function can be realized.

이하, 본 발명의 실시예를 참조하여 설명하기로 한다.Hereinafter, embodiments of the present invention will be described.

본 발명에 의한 피톤치드 함유 탈취제는 정제수 100 중량부에 대하여, 피톤치드 추출물 20 ~ 24 중량부, 와송 추출물 5 ~ 9 중량부 및 포도 추출물 10 ~ 14 중량부를 함유한다.The deodorant containing phytoncide according to the present invention contains 20 to 24 parts by weight of the phytoncide extract, 5 to 9 parts by weight of the extract and 10 to 14 parts by weight of the grape extract, based on 100 parts by weight of purified water.

또한, 본 발명의 피톤치드 함유 탈취제는 마전자(馬錢子) 3 ~ 8 중량부를 더 함유한다.In addition, the deodorant containing phytoncide of the present invention further contains 3 to 8 parts by weight of horse emery.

또한, 본 발명의 피톤치드 함유 탈취제는 해마(sea horse, 海馬) 추출물 0.01 ~ 0.13 중량부를 더 함유한다.The phytoncide-containing deodorant of the present invention further contains 0.01 to 0.13 parts by weight of sea horse (hippocampus) extract.

1. 피톤치드 추출물 제조하기1. Preparation of Phytoncide Extract

① 편백나무 칩 100 중량부에 대하여, 편백잎 20 ~ 30 중량부 및 천일염 5 ~ 7 중량부를 혼합한 후 80 ~ 95℃에서 30 ~ 45분 가열한다.(1) 20 to 30 parts by weight of cottonwood leaves and 5 to 7 parts by weight of sun-salt are mixed with 100 parts by weight of the white rice flour chips, followed by heating at 80 to 95 ° C for 30 to 45 minutes.

② 그런 다음, 솔잎 4 ~ 8 중량부 및 송진 1 ~ 2.4 중량부를 더 첨가한 후 40 ~ 55℃에서 10 ~ 20분 가열하면서 살구씨 오일 0.2 ~ 0.4 중량부를 혼합한 다음 서냉한다.Then, 4 to 8 parts by weight of pine needle and 1 to 2.4 parts by weight of pine root are further added, and 0.2 to 0.4 part by weight of apricot seed oil is mixed while heating at 40 to 55 DEG C for 10 to 20 minutes, followed by slow cooling.

③ 이어서, 정제수 200 중량부 및 일랑일랑 오일 0.2 ~ 0.5 중량부를 더 첨가한 후 밀폐된 상태로 120 ~ 150℃에서 10 ~ 12시간 가열한 후 여과한다.(3) 200 parts by weight of purified water and 0.2 to 0.5 parts by weight of ylang ylang oil are further added, and the mixture is heated at 120 to 150 ° C for 10 to 12 hours in a sealed state, followed by filtration.

2. 와송 추출물 제조하기2. Preparation of Wassong Extract

① 건조된 와송잎 100 중량부에 대하여, 건조된 와송꽃 4 ~ 10 중량부, 민들레 10 ~ 30 중량부 및 죽염 4 ~ 9 중량부를 혼합한 후 120 ~ 145℃에서 5 ~ 8분 가열한다.(1) 4 to 10 parts by weight of dried green tea flowers, 10 to 30 parts by weight of dandelion, and 4 to 9 parts by weight of bamboo salt are mixed with 100 parts by weight of dried green tea leaves, followed by heating at 120 to 145 ° C for 5 to 8 minutes.

② 그런 다음, 정제수 400 ~ 450 중량부, 솔잎 10 ~ 12 중량부 및 오동자 (梧桐子) 분말 4 ~ 8 중량부를 더 첨가하여 120 ~ 145℃에서 24 ~ 28시간 가열한 후 여과한다.(2) Next, 400 to 450 parts by weight of purified water, 10 to 12 parts by weight of pine needles and 4 to 8 parts by weight of powder of paulownia starch are further added and heated at 120 to 145 DEG C for 24 to 28 hours and then filtered.

3. 포도 추출물 제조하기3. Making grape extracts

① 정제수 100 중량부에 대하여, 건조된 포도 껍질 30 ~ 35 중량부 및 포도씨 분말 10 ~ 13 중량부를 혼합한 후 180 ~ 230℃에서 12 ~ 15 시간 가열한 다음 서냉한다.(1) 30 to 35 parts by weight of dried grape skin and 10 to 13 parts by weight of grape seed powder are mixed with 100 parts by weight of purified water, heated at 180 to 230 ° C for 12 to 15 hours, and then slowly cooled.

② 그런 다음, 정제수 50 ~ 70 중량부 및 포도씨 분말 10 ~ 15 중량부를 더 첨가한 후 80 ~ 95℃에서 2 ~ 4시간 가열한 후 여과한다.(2) 50 to 70 parts by weight of purified water and 10 to 15 parts by weight of grape seed powder are further added, and the mixture is heated at 80 to 95 DEG C for 2 to 4 hours and then filtered.

4. 마전자 추출물 제조하기4. Preparation of hemp extract

① 마전자 100 중량부와 천일염 3 ~ 5 중량부를 혼합한 후 120 ~ 150℃에서 5분 간격으로 10회 가열한다.(1) 100 parts by weight of hemp and 3 to 5 parts by weight of sun salt are mixed and heated at 120 to 150 ° C for 10 minutes at intervals of 5 minutes.

③ 정제수 300 중량부, 구기자 5 ~ 9 중량부 및 건조된 민들레 뿌리 10 ~ 13 중량부를 혼합하여 180 ~ 230℃에서 5 ~ 7 시간 가열한 다음 여과한다.(3) 300 parts by weight of purified water, 5 to 9 parts by weight of ginger and 10 to 13 parts by weight of dried dandelion roots are mixed and heated at 180 to 230 DEG C for 5 to 7 hours and then filtered.

5. 해마 추출물 제조하기5. Making hippocampus extract

정제수 100 중량부에 대하여, 건조된 해마 1 ~ 3 중량부를 혼합한 후 50 ~ 55℃에서 120 ~ 150분간 가열한 후 여과한다.1 to 3 parts by weight of dried hippocampus is mixed with 100 parts by weight of purified water, heated at 50 to 55 ° C for 120 to 150 minutes, and then filtered.

이하, 모든 시험에 적용된 실시예는 정제수 100 중량부에 대하여, 피톤치드 추출물 20 ~ 24 중량부, 와송 추출물 5 ~ 9 중량부 및 포도 추출물 10 ~ 14 중량부를 함유한 구성이다.Hereinafter, the examples applied to all the tests are composed of 20 to 24 parts by weight of the phytoncide extract, 5 to 9 parts by weight of the extract and 10 to 14 parts by weight of the grape extract, based on 100 parts by weight of purified water.

a) 살균(항균)시험a) sterilization (antibacterial) test

본 실시예의 살균(항균) 효과를 검증하기 위하여 대장균, 황색포도상구균 및 살모넬라균에 의한 살균(항균)시험을 수행하였으며 이에 대한 결과는 표 1과 같다.In order to verify the sterilization (antibacterial) effect of this example, the sterilization (antibacterial) test with Escherichia coli, Staphylococcus aureus and Salmonella was carried out.

Figure 112015073532819-pat00001
Figure 112015073532819-pat00001

여기서, CFU는 Colony Forming Unit이고, 접종균 세균농도(CFU/mL)는 대장균 1.7 x 106, 황색포도상구균 1.4 x 106 및 살모넬라균 1.5 x 106이다.Here, CFU is a colony forming unit, and the inoculum concentration (CFU / mL) is 1.7 x 10 6 for E. coli, 1.4 x 10 6 for S. aureus and 1.5 x 10 6 for Salmonella.

사용균주 : Escherichia coli ATCC 25922Strain used: Escherichia coli ATCC 25922

Staphylococcus aureus ATCC 6538 Staphylococcus aureus ATCC 6538

Salmonella typhimurium IFO 14193 Salmonella typhimurium IFO 14193

표 1을 참조하면, 본 실시예는 24시간 경과후 99.9%의 세균 감소율을 나타내어 강력한 살균력이 있는 것으로 판명되었다.Referring to Table 1, this example showed a bacterial reduction rate of 99.9% after 24 hours and proved to have strong germicidal power.

b) 탈취시험b) Deodorization test

본 실시예의 탈취 효과를 검증하기 위하여 암모니아 및 황화수소에 대한 탈취시험을 수행하였으며 이에 대한 결과는 표 2 및 표 3과 같다.Deodorization tests on ammonia and hydrogen sulfide were conducted to verify the deodorizing effect of this example, and the results are shown in Tables 2 and 3.

Figure 112015073532819-pat00002
Figure 112015073532819-pat00002

Figure 112015073532819-pat00003
Figure 112015073532819-pat00003

표 2 및 도 3을 참조하면, 본 실시예는 60분 경과후 암모니아 및 황화수소는 각기 100% 및 76%의 탈취율을 확인할 수 있었으며, 120분 경과후에는 황화수소는 88% 정도 탈취되는 것으로 확인되어 강력한 탈취 효과가 있는 것으로 판명되었다.Referring to Table 2 and FIG. 3, after 60 minutes, the deodorization rates of ammonia and hydrogen sulfide were 100% and 76%, respectively, and after 120 minutes, the hydrogen sulfide was deodorized by 88% Deodorizing effect proved to be.

이상과 같은 본 발명은 일 실시예에 한정되어 설명되었으나, 이에 한정되지 않고 본 발명의 기술적 사상을 토대로 변형되는 실시예들은 모두 본 발명의 권리범위에 속함이 분명하다.While the present invention has been described with reference to exemplary embodiments, it is to be understood that the invention is not limited to the disclosed exemplary embodiments.

Claims (5)

정제수 100 중량부에 대하여, 피톤치드 추출물 20 ~ 24 중량부, 와송 추출물 5 ~ 9 중량부 및 포도 추출물 10 ~ 14 중량부를 함유하고,
상기 피톤치드 추출물은, a) 편백나무 칩 100 중량부에 대하여, 편백잎 20 ~ 30 중량부 및 천일염 5 ~ 7 중량부를 혼합한 후 80 ~ 95℃에서 30 ~ 45분 가열하sm는 단계와, b) 솔잎 4 ~ 8 중량부 및 송진 1 ~ 2.4 중량부를 더 첨가한 후 40 ~ 55℃에서 10 ~ 20분 가열하면서 살구씨 오일 0.2 ~ 0.4 중량부를 혼합한 다음 서냉하는 단계와; c) 정제수 200 중량부 및 일랑일랑 오일 0.2 ~ 0.5 중량부를 더 첨가한 후 밀폐된 상태로 120 ~ 150℃에서 10 ~ 12시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 하는 피톤치드를 함유한 탈취제.
20 to 24 parts by weight of a phytoncide extract, 5 to 9 parts by weight of an extract of Wassong extract, and 10 to 14 parts by weight of a grape extract, based on 100 parts by weight of purified water,
The phytoncide extract is prepared by a) mixing 20 to 30 parts by weight of a flat leaf and 5 to 7 parts by weight of a sunflower with respect to 100 parts by weight of a white rice flour, heating at 80 to 95 ° C for 30 to 45 minutes, ) 4 to 8 parts by weight of pine needles and 1 to 2.4 parts by weight of pine root, and heating at 40 to 55 ° C for 10 to 20 minutes to mix 0.2 to 0.4 parts by weight of apricot seed oil followed by slow cooling; c) adding 200 parts by weight of purified water and 0.2 to 0.5 parts by weight of ylang ylang oil, and then heating the mixture at 120 to 150 ° C. for 10 to 12 hours in an airtight state, followed by filtering the deodorant containing phytoncide .
삭제delete 제 1 항에 있어서,
상기 와송 추출물은, a) 건조된 와송잎 100 중량부에 대하여, 건조된 와송꽃 4 ~ 10 중량부, 민들레 10 ~ 30 중량부 및 죽염 4 ~ 9 중량부를 혼합한 후 120 ~ 145℃에서 5 ~ 8분 가열하는 단계와; b) 정제수 400 ~ 450 중량부, 솔잎 10 ~ 12 중량부 및 오동자 분말 4 ~ 8 중량부를 더 첨가하여 120 ~ 145℃에서 24 ~ 28시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 하는 피톤치드를 함유한 탈취제.
The method according to claim 1,
The above dried persimmon extracts are obtained by a) mixing 100 parts by weight of dried green tea leaves with 4 to 10 parts by weight of dried green tea flowers, 10 to 30 parts by weight of dandelion, and 4 to 9 parts by weight of bamboo salt, Heating for 8 minutes; b) adding 400 to 450 parts by weight of purified water, 10 to 12 parts by weight of pine needles and 4 to 8 parts by weight of a powder of tin powder, heating at 120 to 145 ° C for 24 to 28 hours, and then filtering. ≪ / RTI >
제 1 항에 있어서,
상기 포도 추출물은, a) 정제수 100 중량부에 대하여, 건조된 포도 껍질 30 ~ 35 중량부 및 포도씨 분말 10 ~ 13 중량부를 혼합한 후 180 ~ 230℃에서 12 ~ 15 시간 가열한 다음 서냉하는 단계와; b) 정제수 50 ~ 70 중량부 및 포도씨 분말 10 ~ 15 중량부를 더 첨가한 후 80 ~ 95℃에서 2 ~ 4시간 가열한 후 여과하는 단계로 제조되는 것을 특징으로 하는 피톤치드를 함유한 탈취제.
The method according to claim 1,
The grape extract may be prepared by: a) mixing 30 to 35 parts by weight of dried grape skin and 10 to 13 parts by weight of grape seed powder with 100 parts by weight of purified water, heating the mixture at 180 to 230 ° C for 12 to 15 hours, ; b) adding 50 to 70 parts by weight of purified water and 10 to 15 parts by weight of grape seed powder, heating at 80 to 95 ° C for 2 to 4 hours, and then filtering the deodorant.
제 1 항에 있어서,
마전자 추출물 3 ~ 8 중량부 또는 해마 추출물 0.01 ~ 0.13 중량부를 더 함유하되,
상기 마전자 추출물은, a) 마전자 100 중량부와 천일염 3 ~ 5 중량부를 혼합한 후 120 ~ 150℃에서 5분 간격으로 10회 가열하는 단계와; b) 정제수 300 중량부, 구기자 5 ~ 9 중량부 및 건조된 민들레 뿌리 10 ~ 13 중량부를 혼합하여 180 ~ 230℃에서 5 ~ 7 시간 가열한 다음 여과하여 제조되고,
상기 해마 추출물은, 정제수 100 중량부에 대하여, 건조된 해마 1 ~ 3 중량부를 혼합한 후 50 ~ 55℃에서 120 ~ 150분간 가열한 후 여과하여 제조되는 것을 특징으로 하는 피톤치드를 함유한 탈취제.
The method according to claim 1,
3 to 8 parts by weight of an extract of horseshoe extract or 0.01 to 0.13 parts by weight of horsetail extract,
The horsetail extract may be prepared by: a) mixing 100 parts by weight of hemp and 3 to 5 parts by weight of a salt of the salt, and heating the mixture at 120 to 150 ° C for 10 minutes at intervals of 5 minutes; b) 300 parts by weight of purified water, 5 to 9 parts by weight of ginger and 10 to 13 parts by weight of dried dandelion roots are mixed, heated at 180 to 230 ° C for 5 to 7 hours,
The hippopotamus extract is prepared by mixing 1 to 3 parts by weight of dried hippocampus with 100 parts by weight of purified water, heating the mixture at 50 to 55 ° C for 120 to 150 minutes, and filtering the mixture.
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KR101960295B1 (en) * 2018-11-27 2019-03-20 황민지 Composition for deodorization or prevention of dust adsorption
CN112337303A (en) * 2020-11-20 2021-02-09 四川力洁狮环保科技有限公司 Biodegradable formaldehyde scavenger
CN113367167A (en) * 2021-06-16 2021-09-10 杭州华好生物科技有限公司 Deodorizing disinfectant
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JP2000342671A (en) * 1999-06-02 2000-12-12 Kunio Suzuki Botanical deodorizing agent
JP2008110944A (en) * 2006-10-31 2008-05-15 Taiyo Corp Deodorant composition
KR101439385B1 (en) * 2014-03-04 2014-09-12 김태성 Natural composition containing phytoncide having excellent deodorizing and sterilizing

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101960295B1 (en) * 2018-11-27 2019-03-20 황민지 Composition for deodorization or prevention of dust adsorption
KR20210129536A (en) * 2020-04-20 2021-10-28 나정식 Manufacturing method for colloidal silver ion composition comprising phytoncide oil and colloidal silver ion composition manufactured using the same
KR102414509B1 (en) 2020-04-20 2022-06-30 나정식 Manufacturing method for colloidal silver ion composition comprising phytoncide oil and colloidal silver ion composition manufactured using the same
CN112337303A (en) * 2020-11-20 2021-02-09 四川力洁狮环保科技有限公司 Biodegradable formaldehyde scavenger
CN113367167A (en) * 2021-06-16 2021-09-10 杭州华好生物科技有限公司 Deodorizing disinfectant

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