CN111418618A - Multi-effect disinfection spray for vehicle and preparation method thereof - Google Patents
Multi-effect disinfection spray for vehicle and preparation method thereof Download PDFInfo
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- CN111418618A CN111418618A CN202010406924.7A CN202010406924A CN111418618A CN 111418618 A CN111418618 A CN 111418618A CN 202010406924 A CN202010406924 A CN 202010406924A CN 111418618 A CN111418618 A CN 111418618A
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- 238000004659 sterilization and disinfection Methods 0.000 title claims abstract description 80
- 239000007921 spray Substances 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000000284 extract Substances 0.000 claims abstract description 111
- 150000001875 compounds Chemical class 0.000 claims abstract description 99
- 230000001954 sterilising effect Effects 0.000 claims abstract description 48
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000008367 deionised water Substances 0.000 claims abstract description 31
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 31
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 24
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 24
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 24
- 239000011425 bamboo Substances 0.000 claims abstract description 24
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- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 23
- 239000011707 mineral Substances 0.000 claims abstract description 23
- 240000002924 Platycladus orientalis Species 0.000 claims abstract description 16
- 239000000645 desinfectant Substances 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 241001330002 Bambuseae Species 0.000 claims description 23
- 235000008109 Thuja occidentalis Nutrition 0.000 claims description 18
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 18
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- 229930003935 flavonoid Natural products 0.000 claims description 7
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- 244000052616 bacterial pathogen Species 0.000 abstract description 3
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- 238000012360 testing method Methods 0.000 description 20
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 15
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- 241000933832 Broussonetia Species 0.000 description 10
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- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000005507 spraying Methods 0.000 description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000003385 bacteriostatic effect Effects 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000705930 Broussonetia papyrifera Species 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- SXRSQZLOMIGNAQ-UHFFFAOYSA-N Glutaraldehyde Chemical compound O=CCCCC=O SXRSQZLOMIGNAQ-UHFFFAOYSA-N 0.000 description 2
- 241000218231 Moraceae Species 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 230000009471 action Effects 0.000 description 2
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- 239000000419 plant extract Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- MDYOLVRUBBJPFM-UHFFFAOYSA-N tropolone Chemical compound OC1=CC=CC=CC1=O MDYOLVRUBBJPFM-UHFFFAOYSA-N 0.000 description 2
- 244000063299 Bacillus subtilis Species 0.000 description 1
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- 241000193388 Bacillus thuringiensis Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 241000272168 Laridae Species 0.000 description 1
- 241001071917 Lithospermum Species 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 241000606856 Pasteurella multocida Species 0.000 description 1
- 241000588769 Proteus <enterobacteria> Species 0.000 description 1
- 241001478212 Riemerella anatipestifer Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 241000293871 Salmonella enterica subsp. enterica serovar Typhi Species 0.000 description 1
- 241000017433 Schefflera heptaphylla Species 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229940097012 bacillus thuringiensis Drugs 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
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- 239000012895 dilution Substances 0.000 description 1
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- 238000011156 evaluation Methods 0.000 description 1
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- 239000003205 fragrance Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- YOBAEOGBNPPUQV-UHFFFAOYSA-N iron;trihydrate Chemical compound O.O.O.[Fe].[Fe] YOBAEOGBNPPUQV-UHFFFAOYSA-N 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
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- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 229940051027 pasteurella multocida Drugs 0.000 description 1
- 239000002957 persistent organic pollutant Substances 0.000 description 1
- 238000013032 photocatalytic reaction Methods 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- FJOLTQXXWSRAIX-UHFFFAOYSA-K silver phosphate Chemical compound [Ag+].[Ag+].[Ag+].[O-]P([O-])([O-])=O FJOLTQXXWSRAIX-UHFFFAOYSA-K 0.000 description 1
- 229940019931 silver phosphate Drugs 0.000 description 1
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- 239000007858 starting material Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 230000009385 viral infection Effects 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/22—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/16—Disinfection, sterilisation or deodorisation of air using physical phenomena
- A61L9/18—Radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/66—Silver or gold
-
- B01J35/39—
Abstract
The invention relates to a multi-effect disinfectant spray for vehicles and a preparation method thereof, belongs to the technical field of disinfectants, and solves the problem of disinfectant which is low in irritation to human bodies and can efficiently remove harmful gases in vehicles, and the disinfectant is prepared from the following raw materials in parts by weight: 0.2-8 parts of negative ion aldehyde-removing compound consisting of natural polar mineral compound and photocatalyst compound, 33-73 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, platycladus orientalis extract and deionized water, 0.1-5 parts of odor-removing compound hydrolat and 0-80 parts of deionized water. The multi-effect disinfection spray for the vehicle is green, environment-friendly, safe, nontoxic, excellent in performance, low in irritation to a human body, capable of continuously and effectively removing harmful gas, peculiar smell and pathogenic bacteria in the vehicle and capable of achieving a health-care effect on the human body.
Description
Technical Field
The invention belongs to the technical field of disinfectants, and relates to a multi-effect disinfection spray for vehicles and a preparation method thereof.
Background
With the development of economy and the continuous improvement of living standard, automobiles become an important vehicle and are more and more popular. Because the inside of the automobile is a relatively closed space, the air circulation is not smooth, bacteria and viruses are easy to breed, and various diseases are induced; and because a large amount of plastics, leather, interior decorations and the like exist in the automobile, harmful gases such as formaldehyde, benzene, toluene, xylene and the like can be released for a long time, so that air pollutants in the automobile seriously exceed the standard, peculiar smell is emitted, and the health of people in the automobile is damaged. Therefore, improvement of the quality of air in the vehicle is very necessary. At present, most of the air quality in automobiles is improved by chemical disinfectants, so that the automobile air quality improvement has a good sterilization effect, but has irritation to human bodies and is easy to cause secondary pollution; the vehicle interior can be sterilized and disinfected by using natural and safe plant extracts and plant essential oil, but the disinfection effect needs to be improved, the removal capability of harmful gas in the vehicle is weak, and the disinfectant has single functionality.
As in the chinese invention [ application number: CN201610038810.5 discloses a vehicle air sterilizing and refreshing spray and a preparation process thereof, wherein the product is mainly prepared from hydrogen peroxide, glutaraldehyde, silver-containing oxidant, protective agent, stabilizing agent, pH regulator and the like according to a certain proportion. The sterilization effect is improved by compounding the hydrogen peroxide and the glutaraldehyde, but the removal capability of peculiar smell and harmful gas in the automobile is weaker, and the chemical disinfectant can cause harm to the human body after being used for a long time. As another example, the chinese invention [ application No.: CN201810762144.9 discloses a disinfectant for automobiles, which consists of the following components: 10-12 parts of bulbus magnoliae, 6-8 parts of lithospermum, 5-10 parts of folium isatidis, 3-5 parts of schefflera octophylla leaves, 5-8 parts of fructus forsythiae, 803-5 parts of tween, 3-5 parts of propylene glycol, 10-20 parts of ethanol and 100 parts of water; the invention utilizes the effective components of the compound extract of the vine plants to improve the disinfection and sterilization performance, freshen air and prevent virus infection such as influenza, but the invention has limited effect of removing harmful gases in the vehicle.
Therefore, the development of a disinfectant which has low irritation to human bodies and can efficiently remove harmful gases in vehicles becomes an urgent problem to be solved.
Disclosure of Invention
The invention aims to solve the problems and provide a multi-effect disinfection spray for vehicles;
the invention also aims to solve the problems and provide a preparation method of the multi-effect disinfection spray for the vehicle.
In order to achieve the purpose, the invention adopts the following technical scheme:
a multi-effect disinfection spray for vehicles is composed of the following raw materials in parts by weight: 0.2-8 parts of negative ion aldehyde-removing compound consisting of natural polar mineral compound and photocatalyst compound, 33-73 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, platycladus orientalis extract and deionized water, 0.1-5 parts of odor-removing compound hydrolat and 0-80 parts of deionized water.
In the multi-effect disinfection spray for the vehicle, the weight ratio of the natural polar mineral compound to the photocatalyst compound in the negative ion formaldehyde-removing compound is 1:0.6-1, and the sterilization stabilizer comprises 10-18 parts by weight of bamboo leaf extract, 8-50 parts by weight of mulberry plant leaf extract, 5-10 parts by weight of platycladus orientalis extract and 40-80 parts by weight of deionized water.
In the multi-effect disinfection spray for the vehicle, the natural polar mineral compound is composed of nano tourmaline and nano medical stone according to the weight ratio of 3-5:1, and the photocatalyst compound is compounded of nano titanium oxide, nano zinc oxide and nano silver.
In the multi-effect disinfection spray for the vehicle, the purity of total flavonoids in the bamboo leaf extract is more than 70%, the mulberry leaf extract and the papermulberry leaf extract are prepared according to the weight ratio of 0.8-1:1-2, and the extraction ratio of the biota orientalis extract is not more than 20: 1.
In the multi-effect disinfection spray for the vehicle, the purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is not less than 40%, the extraction ratio of the papermulberry leaf extract is not more than 15:1, and the arborvitae extract is a arborvitae extract.
In the multi-effect disinfection spray for the vehicle, the odor-removing compound hydrolat is composed of lavender hydrolat, nutmeg hydrolat and bran-fried fructus aurantii hydrolat according to the weight ratio of 6-10:2-3: 5-7.
The preparation method of the multi-effect disinfection spraying agent for the vehicle comprises the following steps,
s1 preparing aldehyde-removing compound and sterilizing stabilizer respectively according to the weight percentage,
s2 preparing the odor-removing compound hydrolat, preparing a uniform and stable solution according to the weight percentage,
s3, adding the aldehyde-removing compound prepared in the S1 into a sterilization stabilizer for mixing, adding the rest other components after fully mixing to obtain stable mixed liquid, and then sterilizing to obtain the multi-effect disinfection spray for the vehicle.
In the above preparation method of the multi-effect disinfection spray for vehicles, in the step S3, the aldehyde-removing compound prepared in the step S1 is added into the sterilization stabilizer to be mixed, and then fully mixed, and simultaneously the solution prepared in the step S2 is uniformly mixed with deionized water, and the diluted odor-removing compound hydrolat is added into the mixture of the aldehyde-removing compound and the sterilization stabilizer to obtain a stable mixed solution, and then the mixed solution is sterilized, so that the multi-effect disinfection spray for vehicles is obtained.
In the preparation method of the multi-effect disinfection spray for the vehicle, the step S3 is that deionized water is added into the aldehyde-removing compound prepared in the step S1 to form an aldehyde-removing compound aqueous solution, then the sterilization stabilizer is added into the aldehyde-removing compound aqueous solution, and the odor-removing compound hydrolat prepared in the step S2 is added after the sterilization stabilizer is uniformly stirred.
In the above method for preparing the multi-effect sterilization spray for vehicles, the sterilization stabilizer in the step S1 is prepared by preparing a bamboo leaf extract, a leaf extract of a Moraceae plant, a biota orientalis extract and deionized water in a weight percentage ratio, adding an appropriate amount of deionized water to the leaf extract of the Moraceae plant, stirring uniformly, and then adding the rest components of the sterilization stabilizer.
Compared with the prior art, the invention has the advantages that:
1. the multi-effect disinfection spray for the vehicle is green, environment-friendly, safe, nontoxic, excellent in performance, low in irritation to a human body, capable of continuously and effectively removing harmful gas, peculiar smell and pathogenic bacteria in the vehicle and capable of achieving a health-care effect on the human body.
2. The multi-effect disinfection spraying agent for the vehicle ensures the effects of efficiently sterilizing, deodorizing and removing harmful gases for a long time by the slow release of the natural polar mineral compound in the negative ion formaldehyde-removing compound and the anti-oxidation and anti-inactivation arrangement of the photocatalyst compound.
3. The preparation method of the multi-effect disinfection spraying agent for the vehicle ensures the stability and the effect of the multi-effect disinfection spraying agent for the vehicle and prolongs the service life through the arrangement of a series of steps.
Additional advantages, objects, and features of the invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Detailed Description
The technical scheme of the invention is further specifically described by the following embodiments. The starting materials used are commercially available except as indicated, and the tabulated data are the average of the three test values.
Example 1
A multi-effect disinfection spray for vehicles is composed of the following raw materials in parts by weight: 0.2 part of negative ion aldehyde-removing compound consisting of a natural polar mineral compound and a photocatalyst compound, 33 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, arborvitae extract and deionized water and 0.1 part of odor-removing compound pure water.
The anion formaldehyde-removing compound in the embodiment firstly utilizes the characteristic that the natural polar mineral compound generates anions to adsorb organic volatile matters such as formaldehyde and the like in the vehicle, and can also perform bacteriostasis, degerming and odor removal on the space in the vehicle. The natural polar mineral compound can be compound powder composed of tourmaline and one or more of six-ring stone, medical stone and gull rock. The photocatalyst compound in the anion aldehyde-removing compound can be composite powder consisting of any two or more of nano titanium oxide, nano zinc oxide, nano tin oxide, nano silver and silver phosphate. The photocatalyst can generate a photocatalytic reaction similar to photosynthesis under the irradiation of light to generate free hydroxyl and active oxygen with extremely strong oxidizing power, has a very strong photo-oxidation-reduction function, can oxidize and decompose various organic compounds and partial inorganic matters, and decomposes organic pollutants into pollution-free water and carbon dioxide. However, the photocatalyst composite has limited effect when sunlight is insufficient or the concentration of chemical pollutants is high, so the natural polar mineral composite and the photocatalyst composite are comprehensively utilized to ensure the effect of removing harmful gases such as formaldehyde to the maximum, and the natural polar mineral composite and the photocatalyst composite can play a role durably and continuously under the condition that the environment is relatively stable, so the service life of the embodiment is fundamentally ensured.
However, some sulfate and nitrate ions affect the life and effect of the photocatalyst, deactivation occurs, and meanwhile, the natural polar mineral complex is easy to scale and affect the effect of releasing negative ions. Therefore, the present example also employs a sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, arborvitae extract and deionized water.
The bamboo leaf extract is used as a plant flavonoid, has typical bamboo leaf fragrance, good thermal stability, broad-spectrum antibacterial property and strong inhibition effect on bacteria, mould and yeast. Wherein the extract has stronger inhibiting effect on bacteria, such as salmonella typhi, escherichia coli, staphylococcus aureus, bacillus subtilis, proteus and bacillus thuringiensis, and is enhanced along with the prolonging of the action time and the increase of the concentration of the used extract.
The extract of the mulberry leaves in the embodiment preferably can provide a mulberry leaf extract and a broussonetia papyrifera leaf extract of high-purity mulberry leaf polysaccharide, and the broussonetia papyrifera leaf extract contains various antibacterial components and has an inhibiting effect on pathogenic bacteria such as staphylococcus aureus, pasteurella multocida, escherichia coli, salmonella, riemerella anatipestifer and the like. The arborvitae extract contains active substances such as tropolone and the like, and also has excellent bacteriostatic ability.
The bactericidal stabilizer in this embodiment utilizes the stability of the extract itself, in addition to the antibacterial and bacteriostatic ability of the extract itself. Meanwhile, the inventor unexpectedly discovers that the extract in the sterilization stabilizer has the ion exchange capacity as a weakly alkaline macromolecular organic compound, so that the lasting using effect of the embodiment is ensured.
The odor-removing compound pure dew is natural odor-removing and can prevent the multi-effect disinfection spraying agent for the vehicle from being oxidized to influence the biological activity.
Furthermore, the weight ratio of the natural polar mineral compound to the photocatalyst compound in the negative ion aldehyde removal compound is 1:0.6, and the sterilization stabilizer comprises 10 parts by weight of bamboo leaf extract, 8 parts by weight of mulberry leaf extract, 5 parts by weight of platycladus orientalis extract and 40 parts by weight of deionized water.
Further, the natural polar mineral compound is composed of nano-scale tourmaline and nano-scale medical stone according to the weight ratio of 3:1, and the photocatalyst compound is compounded by nano titanium oxide, nano zinc oxide and nano silver. In the embodiment, the nano titanium oxide, the nano zinc oxide and the nano silver are compounded according to the weight ratio of 1:1: 1.
The tourmaline has better anion release capacity, and the medical stone has adsorbability, dissolubility, adjustability, biological activity, mineralization and the like, can adsorb free metal ions in water and is beneficial to prolonging the service life of the multi-effect disinfection spray for vehicles. Thereby delaying the inactivation of the photocatalyst compound and further enhancing the anti-scaling effect of the natural polar mineral compound. The nanometer tourmaline and the nanometer medical stone can also play the superfine effect of polar ores.
Preferably, the purity of the total flavonoids in the bamboo leaf extract is 70%, the mulberry leaf extract and the papermulberry leaf extract are prepared according to the weight ratio of 0.8:1, and the extraction ratio of the biota orientalis extract is 20: 1.
Preferably, the purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is 40%, the extraction specification of the papermulberry leaf extract is 15:1, and the arborvitae extract is a arborvitae extract.
Furthermore, the odor-removing compound hydrolat is prepared from lavender, nutmeg and bran-fried fructus aurantii hydrolat according to a ratio of 6:2: 5. The lavender, the nutmeg and the bran-fried fructus aurantii hydrolat have excellent oxidation resistance and sterilization and odor removal effects.
The bamboo leaf extract and the mulberry leaf extract used in this example were provided by shanxi scanty biotechnology limited, and the paper mulberry leaf extract and the arborvitae extract were provided by sienna grass science and technology limited.
Example 2
A multi-effect disinfection spray for vehicles is composed of the following raw materials in parts by weight: 8 parts of negative ion aldehyde-removing compound consisting of a natural polar mineral compound and a photocatalyst compound, 73 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, arborvitae extract and deionized water, 5 parts of odor-removing compound hydrolat and 80 parts of deionized water.
The weight ratio of the natural polar mineral compound to the photocatalyst compound in the negative ion aldehyde-removing compound is 1:1, and the sterilization stabilizer comprises 18 parts of bamboo leaf extract, 50 parts of mulberry plant leaf extract, 10 parts of arborvitae extract and 80 parts of deionized water in parts by weight.
The natural polar mineral compound is composed of nanoscale tourmaline and nanoscale medical stone according to a weight ratio of 5:1, and the photocatalyst compound is compounded of nanometer titanium oxide, nanometer zinc oxide and nanometer silver. In the embodiment, the nano titanium oxide, the nano zinc oxide and the nano silver are compounded according to the weight ratio of 1:1: 1.
The purity of the total flavonoids in the bamboo leaf extract is 80%, the mulberry leaf extract and the papermulberry leaf extract are prepared according to a ratio of 1:2, and the extraction specification of the biota orientalis extract is 25: 1.
The purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is 45%, the extraction specification of the papermulberry leaf extract is 20:1, and the arborvitae extract is a arborvitae extract.
The odor-removing compound hydrolat is composed of lavender, nutmeg and bran-fried fructus aurantii hydrolat according to a ratio of 10:3: 7.
Example 3
A multi-effect disinfection spray for vehicles is composed of the following raw materials in parts by weight: 3 parts of negative ion formaldehyde-removing compound consisting of natural polar mineral compound and photocatalyst compound, 50 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, arborvitae extract and deionized water, 2 parts of odor-removing compound pure water and 30 parts of deionized water.
The weight ratio of the natural polar mineral compound to the photocatalyst compound in the negative ion aldehyde-removing compound is 1:0.8, and the sterilization stabilizer comprises 15 parts of bamboo leaf extract, 35 parts of mulberry leaf extract, 7 parts of platycladus orientalis extract and 60 parts of deionized water in parts by weight.
The natural polar mineral compound is composed of nano-tourmaline and nano medical stone according to a weight ratio of 4:1, and the photocatalyst compound is compounded by nano titanium oxide, nano zinc oxide and nano silver. In the embodiment, the nano titanium oxide, the nano zinc oxide and the nano silver are compounded according to the weight ratio of 1:1: 1.
The purity of the total flavonoids in the bamboo leaf extract is 70%, the mulberry leaf extract and the papermulberry leaf extract are prepared according to a ratio of 1:1, and the extraction specification of the biota orientalis extract is 20: 1.
The purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is 40%, the extraction specification of the papermulberry leaf extract is 15:1, and the arborvitae extract is a arborvitae extract.
The odor-removing compound hydrolat is composed of lavender, nutmeg and bran-fried fructus aurantii hydrolat according to a ratio of 8:3: 6.
Example 4
A preparation method of a multi-effect disinfection spray for vehicles comprises the following steps,
s1 preparing aldehyde-removing compound and sterilizing stabilizer respectively according to the weight percentage,
s2 preparing the odor-removing compound hydrolat, preparing a uniform and stable solution according to the weight percentage,
s3, adding the aldehyde-removing compound prepared in the S1 into a sterilization stabilizer for mixing, adding the rest other components after fully mixing to obtain stable mixed liquid, and then sterilizing to obtain the multi-effect disinfection spray for the vehicle.
In this embodiment, the formaldehyde-removing compound is first mixed with the sterilization stabilizer, the formaldehyde-removing compound is uniformly dispersed in the sterilization stabilizer system to realize a uniform and stable system, and then the odor-removing compound hydrolat and deionized water are added into the system for dilution.
Further, preparing the bamboo leaf extract, the mulberry leaf extract, the platycladus orientalis extract and deionized water according to the weight percentage, adding a proper amount of deionized water into the mulberry leaf extract, stirring uniformly, and then adding the rest components of the sterilization stabilizer.
The mulberry leaf extract contains more mulberry leaf polysaccharide, and forms a stable colloidal solution after being added with deionized water, thereby being more beneficial to the dispersion of the other components.
Example 5
The embodiment is basically the same as the embodiment 4, except that the step S3 is to add the aldehyde-removing compound prepared in the step S1 into the sterilization stabilizer for mixing, fully mix, simultaneously mix the solution prepared in the step S2 with deionized water uniformly, add the diluted odor-removing compound hydrolat into the mixture of the aldehyde-removing compound and the sterilization stabilizer to obtain a stable mixed solution, and then perform sterilization treatment, thereby obtaining the multi-effect disinfection spray for vehicles.
Example 6
This example is substantially the same as example 4, except that in step S3, deionized water is added to the aldehyde-removing complex prepared in step S1 to form an aqueous solution of the aldehyde-removing complex, then a bactericidal stabilizer is added to the aqueous solution of the aldehyde-removing complex, and after stirring, the odor-removing compound hydrolat prepared in step S2 is added.
Comparative example 1
Comparative example 1 is substantially the same as example 3 except that no germicidal stabilizer is added.
Comparative example 2
Comparative example 2 is substantially the same as example 3 except that no odor-removing compounded hydrolat is added.
Comparative example 3
Comparative example 3 is substantially the same as example 3 except that nanoscale tourmaline and nanoscale medical stone are not used.
Comparative example 4
Comparative example 4 is substantially the same as example 3, except that the purity of total flavonoids in the bamboo leaf extract is 60%, the biota orientalis extract is a biota orientalis leaf extract, and the extraction specification is 15: 1; the purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is 30%, and the extraction specification of the papermulberry leaf extract is 10: 1.
Test example 1
The components of examples 1-3 and comparative examples 1-4 were each prepared using the method of example 4. The obtained sample is subjected to a product stability test, the test standard is 2.2.3.2.1 accelerated test method in 2002 edition of disinfection technical specification, and the test condition is 3 months in a constant temperature box at 37 ℃.
TABLE 1 results of product stability test of examples 1-3 and comparative examples 1-4
As can be seen from Table 1, the reduction rates of the effective components of the examples 1-3 and the comparative examples 3-4 are less than 10%, and the test standards are met. Examples 1-3 are much lower than comparative examples 1-2, and examples 1-3 demonstrate that the formulations of the components of examples 1-3 are more stable and longer lasting. Among them, the reduction rate of the effective component of comparative example 1 is the highest, and it is presumed that the stability of the system of comparative example 1 is greatly reduced because no bactericidal stabilizer is added. In the comparative example 2, the stability of the product is difficult to ensure because no odor-removing compound hydrolat is added. Comparative example 3 the absence of nanoscale tourmaline and nanoscale medical stone although meeting the corresponding standards, the stability was slightly inferior to that of the examples. As can be seen from comparative example 4, the extraction criteria of the plant extract in the germicidal stabilizer also affected the stability of the system.
Test example 2
The components of examples 1-3 and comparative examples 1-4 were each prepared using the method of example 5. Testing the obtained sample by negative ions and removing harmful gases, wherein the testing equipment is negative ion testing equipment and an air quality detector of Shenzhen Wan instrument science and technology Limited; the formaldehyde test and TVOC test are carried out for 24h and 14d, and the test results of the test equipment are shown in Table 2.
Table 2 test results of examples 1 to 3 and comparative examples 1 to 4 for anion and harmful gas removal
As can be seen from Table 2, the anion release values 24h of examples 1 to 3 and comparative examples 3 to 4 were about 2000/cm3The effect of the disinfectant can be ensured. Meanwhile, the formaldehyde removal rate of examples 1 to 3 was higher than 24 hours at 14d, presumably because the concentration of the extract in the bactericidal stabilizer increased with the increase of the action time. In the examples 1-3, the formaldehyde removal rate can reach 97% in 24 h. The TVOC reduction rates of examples 1-3 and comparative examples 3-4 were also relatively stable at 14 d. Meanwhile, the method of example 5 is also reflected to prepare a stable and long-acting disinfection spray system.
Test example 3
The components of examples 1-3 and comparative examples 1-4 were each prepared using the method of example 6. And carrying out continuous antibacterial test on the obtained sample, wherein the detection standard is 5.2.7 continuous antibacterial test in the WST650-2019 antibacterial and bacteriostatic effect evaluation method, and the test time is 15 d. The test results are shown in Table 3.
TABLE 3 examples 1-3 and comparative examples 1-4 continuous antibacterial tests
As can be seen from Table 3, examples 1-3 and comparative examples 3-4 all met the standard that the sterilization rate was greater than 90%, and could achieve the effect of continuous antibacterial. Comparative example 1 has no bactericidal stabilizer, but has better antibacterial effect due to the negative ion formaldehyde-removing compound. Meanwhile, the method of the embodiment 6 can be used for preparing a stable and long-acting disinfection spray system.
The specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (10)
1. A multi-effect disinfection spray for vehicles is characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 0.2-8 parts of negative ion aldehyde-removing compound consisting of natural polar mineral compound and photocatalyst compound, 33-73 parts of sterilization stabilizer consisting of bamboo leaf extract, mulberry leaf extract, platycladus orientalis extract and deionized water, 0.1-5 parts of odor-removing compound hydrolat and 0-80 parts of deionized water.
2. The multi-effect disinfectant spray for vehicles according to claim 1, wherein: the weight ratio of the natural polar mineral compound to the photocatalyst compound in the negative ion aldehyde-removing compound is 1:0.6-1, and the sterilization stabilizer comprises 10-18 parts of bamboo leaf extract, 8-50 parts of mulberry leaf extract, 5-10 parts of platycladus orientalis extract and 40-80 parts of deionized water in parts by weight.
3. The multi-effect disinfectant spray for vehicles according to claim 1, wherein: the natural polar mineral compound is composed of nano-tourmaline and nano medical stone according to the weight ratio of 3-5:1, and the photocatalyst compound is compounded by nano titanium oxide, nano zinc oxide and nano silver.
4. The multi-effect disinfectant spray for vehicles according to claim 1, wherein: the purity of the total flavonoids in the bamboo leaf extract is more than 70%, the mulberry leaf extract and the papermulberry leaf extract are prepared according to the weight ratio of 0.8-1:1-2, and the extraction ratio of the biota orientalis extract is not more than 20: 1.
5. The multi-effect disinfectant spray for vehicles according to claim 4, wherein: the purity of the mulberry leaf total polysaccharide of the mulberry leaf extract is not less than 40%, the extraction ratio of the papermulberry leaf extract is not more than 15:1, and the arborvitae extract is a arborvitae extract.
6. The multi-effect disinfectant spray for vehicles according to claim 1, wherein: the odor-removing compound hydrolat is composed of lavender hydrolat, nutmeg hydrolat and bran-fried fructus aurantii hydrolat according to the weight ratio of 6-10:2-3: 5-7.
7. The method for preparing the multi-effect disinfection spray for the vehicle according to the claims 1-6, wherein the method comprises the following steps: the steps are as follows,
s1 preparing aldehyde-removing compound and sterilizing stabilizer respectively according to the weight percentage,
s2 preparing the odor-removing compound hydrolat, preparing a uniform and stable solution according to the weight percentage,
s3, adding the aldehyde-removing compound prepared in the S1 into a sterilization stabilizer for mixing, adding the rest other components after fully mixing to obtain stable mixed liquid, and then sterilizing to obtain the multi-effect disinfection spray for the vehicle.
8. The preparation method of the multi-effect disinfection spray for the vehicle as claimed in claim 7, wherein the preparation method comprises the following steps: and S3, adding the aldehyde-removing compound prepared in S1 into a sterilization stabilizer for mixing, fully mixing, simultaneously uniformly mixing the solution prepared in S2 with deionized water, adding the diluted odor-removing compound hydrolat into the mixture of the aldehyde-removing compound and the sterilization stabilizer to obtain a stable mixed solution, and then sterilizing to obtain the multi-effect disinfection spray for the vehicle.
9. The preparation method of the multi-effect disinfection spray for the vehicle as claimed in claim 7, wherein the preparation method comprises the following steps: and step S3, adding deionized water into the aldehyde-removing compound prepared in step S1 to form an aldehyde-removing compound aqueous solution, adding a sterilization stabilizer into the aldehyde-removing compound aqueous solution, uniformly stirring, and adding the odor-removing compound hydrolat prepared in step S2.
10. The preparation method of the multi-effect disinfection spray for the vehicle as claimed in claim 7, wherein the preparation method comprises the following steps: the preparation method of the sterilization stabilizer in the step S1 comprises the steps of preparing the bamboo leaf extract, the mulberry leaf extract, the arborvitae extract and deionized water according to the weight percentage, adding a proper amount of deionized water into the mulberry leaf extract, stirring uniformly, and then adding the rest components of the sterilization stabilizer.
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