KR100556337B1 - 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 - Google Patents
단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 Download PDFInfo
- Publication number
- KR100556337B1 KR100556337B1 KR1020020006593A KR20020006593A KR100556337B1 KR 100556337 B1 KR100556337 B1 KR 100556337B1 KR 1020020006593 A KR1020020006593 A KR 1020020006593A KR 20020006593 A KR20020006593 A KR 20020006593A KR 100556337 B1 KR100556337 B1 KR 100556337B1
- Authority
- KR
- South Korea
- Prior art keywords
- fatty acid
- acid alkyl
- alkyl ester
- alcohol
- reaction
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
- C11C3/10—Ester interchange
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Fats And Perfumes (AREA)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020020006593A KR100556337B1 (ko) | 2002-02-05 | 2002-02-05 | 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 |
AU2002248054A AU2002248054A1 (en) | 2002-02-05 | 2002-04-09 | Process for preparing an alkylester of fatty acid with high purity via one-step continuous process |
PCT/KR2002/000629 WO2003066567A1 (en) | 2002-02-05 | 2002-04-09 | Process for preparing an alkylester of fatty acid with high purity via one-step continuous process |
CNB028284569A CN1318380C (zh) | 2002-02-05 | 2002-04-09 | 通过一步连续法制备脂肪酸烷基酯的方法 |
JP2003565942A JP4297267B2 (ja) | 2002-02-05 | 2002-04-09 | 単一段階連続工程による高純度脂肪酸アルキルエステルの製造方法 |
US10/913,300 US20050080280A1 (en) | 2002-02-05 | 2004-08-05 | Process for producing alkylester of fatty acid in a single-phase continuous process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020020006593A KR100556337B1 (ko) | 2002-02-05 | 2002-02-05 | 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20030066246A KR20030066246A (ko) | 2003-08-09 |
KR100556337B1 true KR100556337B1 (ko) | 2006-03-03 |
Family
ID=27725695
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020020006593A KR100556337B1 (ko) | 2002-02-05 | 2002-02-05 | 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20050080280A1 (zh) |
JP (1) | JP4297267B2 (zh) |
KR (1) | KR100556337B1 (zh) |
CN (1) | CN1318380C (zh) |
AU (1) | AU2002248054A1 (zh) |
WO (1) | WO2003066567A1 (zh) |
Cited By (4)
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---|---|---|---|---|
KR101028660B1 (ko) | 2010-12-28 | 2011-04-12 | 주식회사 한두아이펨 | 방제용 약제 살포 장치 |
KR101034324B1 (ko) * | 2008-04-30 | 2011-05-16 | 주식회사 한두아이펨 | 방제용 약제 살포 장치 |
KR101034323B1 (ko) * | 2010-08-10 | 2011-05-16 | 주식회사 한두아이펨 | 방제용 약제 및 약제 살포 장치 |
KR101368047B1 (ko) | 2013-07-22 | 2014-02-27 | 윤정용 | 고순도 메틸에스테르 제조 방법 |
Families Citing this family (36)
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US20070282118A1 (en) * | 2003-12-30 | 2007-12-06 | Gupta Ashok K | Process For Preparing Fatty Acid Alkylesters Using As Biodiesel |
US7619104B2 (en) | 2005-04-04 | 2009-11-17 | Renewable Products Development Laboratories, Inc. | Process for producing biodiesel or fatty acid esters from multiple triglyceride feedstocks |
JP4219349B2 (ja) * | 2005-09-16 | 2009-02-04 | 富士フイルム株式会社 | 脂肪酸アルキルエステルの製造方法及び燃料 |
US20070087085A1 (en) * | 2005-10-17 | 2007-04-19 | Bunge Oils, Inc. | Protein-containing food product and coating for a food product and method of making same |
US20080113067A1 (en) * | 2005-10-17 | 2008-05-15 | Monoj Sarma | Protein-Containing Food Product and Coating for a Food Product and Method of Making Same |
US20070148311A1 (en) * | 2005-12-22 | 2007-06-28 | Bunge Oils, Inc. | Phytosterol esterification product and method of make same |
US20080004458A1 (en) * | 2006-06-20 | 2008-01-03 | Wiedemann Rudolf A | Transesterification catalyst mixing system |
DE102006028560A1 (de) * | 2006-06-22 | 2007-12-27 | Cognis Ip Management Gmbh | Verfahren zur Umesterung von Triglyceriden |
EP1878716A1 (en) * | 2006-07-14 | 2008-01-16 | Rohm and Haas Company | Method for transesterification of triglycerides |
KR100725335B1 (ko) * | 2006-07-20 | 2007-06-07 | (주)퓨렉스에너지 | 고순도 메틸에스테르의 정제방법 |
US8445709B2 (en) * | 2006-08-04 | 2013-05-21 | Mcneff Research Consultants, Inc. | Systems and methods for refining alkyl ester compositions |
US7897798B2 (en) * | 2006-08-04 | 2011-03-01 | Mcneff Research Consultants, Inc. | Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same |
KR100843501B1 (ko) * | 2007-01-29 | 2008-07-03 | 주식회사 가야에너지 | 버블링 술폰화 반응을 이용한 고수율 알파-술포 지방산알킬에스테르염의 제조 방법 및 이에 의해 생산된알파-술포 지방산 알킬 에스테르염 |
US8017796B2 (en) * | 2007-02-13 | 2011-09-13 | Mcneff Research Consultants, Inc. | Systems for selective removal of contaminants from a composition and methods of regenerating the same |
US8585976B2 (en) * | 2007-02-13 | 2013-11-19 | Mcneff Research Consultants, Inc. | Devices for selective removal of contaminants from a composition |
KR100864298B1 (ko) * | 2007-02-21 | 2008-10-20 | 엄성일 | 고순도 메틸에스테르 제조방법 |
US7918905B2 (en) * | 2007-05-17 | 2011-04-05 | Baker Hughes Incorporated | Method for improving biodiesel fuel |
US20090023808A1 (en) * | 2007-06-29 | 2009-01-22 | Martek Biosciences Corporation | Production and Purification of Esters of Polyunsaturated Fatty Acids |
US7754905B2 (en) | 2007-08-08 | 2010-07-13 | Arisdyne Systems, Inc. | Apparatus and method for producing biodiesel from fatty acid feedstock |
US7935157B2 (en) | 2007-08-08 | 2011-05-03 | Arisdyne Systems, Inc. | Method for reducing free fatty acid content of biodiesel feedstock |
US7943791B2 (en) * | 2007-09-28 | 2011-05-17 | Mcneff Research Consultants, Inc. | Methods and compositions for refining lipid feed stocks |
US20090119979A1 (en) * | 2007-11-08 | 2009-05-14 | Imperial Petroleum, Inc. | Catalysts for production of biodiesel fuel and glycerol |
US8865080B2 (en) * | 2008-06-09 | 2014-10-21 | Renewable Energy Group, Inc. | Devices, processes and methods for the production of lower alkyl esters |
JP4876111B2 (ja) * | 2008-09-18 | 2012-02-15 | 富士フイルム株式会社 | 脂肪酸石鹸含有量の調整法 |
US8361174B2 (en) * | 2008-10-07 | 2013-01-29 | Sartec Corporation | Catalysts, systems, and methods for producing fuels and fuel additives from polyols |
US9102877B2 (en) * | 2008-11-12 | 2015-08-11 | Sartec Corporation | Systems and methods for producing fuels from biomass |
US8637689B2 (en) | 2010-08-31 | 2014-01-28 | Biosynthetic Technologies, Llc | Catalytic processes for preparing estolide base oils |
US8624073B1 (en) * | 2013-02-05 | 2014-01-07 | Cpc Corporation, Taiwan | Homogeneous catalysts for biodiesel production |
CN106281723A (zh) * | 2016-08-31 | 2017-01-04 | 菏泽尧舜牡丹生物科技有限公司 | 一种高酸价牡丹籽油乙酯化工艺 |
US10239812B2 (en) | 2017-04-27 | 2019-03-26 | Sartec Corporation | Systems and methods for synthesis of phenolics and ketones |
US10544381B2 (en) | 2018-02-07 | 2020-01-28 | Sartec Corporation | Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid |
US10696923B2 (en) | 2018-02-07 | 2020-06-30 | Sartec Corporation | Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids |
BR112021018808A8 (pt) * | 2019-03-21 | 2022-07-05 | Visionary Fiber Tech Inc | Processo e sistema para produzir biodiesel |
CN110790668B (zh) * | 2019-10-22 | 2020-12-08 | 浙江工业大学 | 一种基于生物柴油制备脂肪酸丁酯的连续化生产方法 |
WO2022013278A1 (de) | 2020-07-17 | 2022-01-20 | Werner & Mertz Gmbh | Verfahren zur herstellung eines biobasierten produkts, entsprechendes produkt und verwendungen |
DE102020119024A1 (de) | 2020-07-17 | 2022-01-20 | Werner & Mertz Gmbh | Verfahren zur Herstellung eines biobasierten Produkts, entsprechendes Produkt und Verwendungen |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4371470A (en) * | 1980-02-28 | 1983-02-01 | Lion Corporation | Method for manufacturing high quality fatty acid esters |
EP0391485A1 (en) * | 1989-04-05 | 1990-10-10 | Unilever N.V. | Process for producing fatty-acid lower-alkyl monoesters |
US5354878A (en) * | 1992-03-26 | 1994-10-11 | Joosten Connemann | Process for the continuous production of lower alkyl esters of higher fatty acids |
US6127560A (en) * | 1998-12-29 | 2000-10-03 | West Central Cooperative | Method for preparing a lower alkyl ester product from vegetable oil |
KR20020028120A (ko) * | 2000-10-07 | 2002-04-16 | 최재경 | 금속산화물 촉매를 이용한 지방산 에스테르의 제조방법 |
Family Cites Families (7)
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US3852315A (en) * | 1967-07-14 | 1974-12-03 | Lever Brothers Ltd | Process of interesterification of glyceride oils |
JPS6025478B2 (ja) * | 1977-03-17 | 1985-06-18 | 花王株式会社 | 脂肪酸低級アルコ−ルエステルの製造法 |
DE3421217A1 (de) * | 1984-06-07 | 1985-09-05 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von fettsaeureestern kurzkettiger alkohole |
US5514820A (en) * | 1989-09-29 | 1996-05-07 | Henkel Kommanditgesellschaft Auf Aktien | Continuous process for the production of lower alkyl esters |
AT399336B (de) * | 1993-07-14 | 1995-04-25 | Martin Mag Dr Mittelbach | Verfahren zur herstellung von fettsäurealkylestern |
JP3533061B2 (ja) * | 1996-12-27 | 2004-05-31 | 有限会社染谷商店 | 廃食用油等から高級脂肪酸のメチルエステルとグリセリンとを連続的に製造する方法および装置 |
US20030032826A1 (en) * | 2001-07-20 | 2003-02-13 | The Board Of Regents Of The University Of Nebraska | Transesterification process for production of biodiesel |
-
2002
- 2002-02-05 KR KR1020020006593A patent/KR100556337B1/ko not_active IP Right Cessation
- 2002-04-09 JP JP2003565942A patent/JP4297267B2/ja not_active Expired - Fee Related
- 2002-04-09 WO PCT/KR2002/000629 patent/WO2003066567A1/en active Application Filing
- 2002-04-09 CN CNB028284569A patent/CN1318380C/zh not_active Expired - Fee Related
- 2002-04-09 AU AU2002248054A patent/AU2002248054A1/en not_active Abandoned
-
2004
- 2004-08-05 US US10/913,300 patent/US20050080280A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4371470A (en) * | 1980-02-28 | 1983-02-01 | Lion Corporation | Method for manufacturing high quality fatty acid esters |
EP0391485A1 (en) * | 1989-04-05 | 1990-10-10 | Unilever N.V. | Process for producing fatty-acid lower-alkyl monoesters |
US5354878A (en) * | 1992-03-26 | 1994-10-11 | Joosten Connemann | Process for the continuous production of lower alkyl esters of higher fatty acids |
US6127560A (en) * | 1998-12-29 | 2000-10-03 | West Central Cooperative | Method for preparing a lower alkyl ester product from vegetable oil |
KR20020028120A (ko) * | 2000-10-07 | 2002-04-16 | 최재경 | 금속산화물 촉매를 이용한 지방산 에스테르의 제조방법 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101034324B1 (ko) * | 2008-04-30 | 2011-05-16 | 주식회사 한두아이펨 | 방제용 약제 살포 장치 |
KR101034323B1 (ko) * | 2010-08-10 | 2011-05-16 | 주식회사 한두아이펨 | 방제용 약제 및 약제 살포 장치 |
KR101028660B1 (ko) | 2010-12-28 | 2011-04-12 | 주식회사 한두아이펨 | 방제용 약제 살포 장치 |
KR101368047B1 (ko) | 2013-07-22 | 2014-02-27 | 윤정용 | 고순도 메틸에스테르 제조 방법 |
Also Published As
Publication number | Publication date |
---|---|
US20050080280A1 (en) | 2005-04-14 |
JP4297267B2 (ja) | 2009-07-15 |
JP2005517002A (ja) | 2005-06-09 |
AU2002248054A1 (en) | 2003-09-02 |
CN1318380C (zh) | 2007-05-30 |
WO2003066567A1 (en) | 2003-08-14 |
CN1622933A (zh) | 2005-06-01 |
KR20030066246A (ko) | 2003-08-09 |
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