KR100556337B1 - 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 - Google Patents

단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 Download PDF

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KR100556337B1
KR100556337B1 KR1020020006593A KR20020006593A KR100556337B1 KR 100556337 B1 KR100556337 B1 KR 100556337B1 KR 1020020006593 A KR1020020006593 A KR 1020020006593A KR 20020006593 A KR20020006593 A KR 20020006593A KR 100556337 B1 KR100556337 B1 KR 100556337B1
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South Korea
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fatty acid
acid alkyl
alkyl ester
alcohol
reaction
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KR1020020006593A
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Korean (ko)
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KR20030066246A (ko
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유정우
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주식회사 가야에너지
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Priority to KR1020020006593A priority Critical patent/KR100556337B1/ko
Priority to AU2002248054A priority patent/AU2002248054A1/en
Priority to PCT/KR2002/000629 priority patent/WO2003066567A1/en
Priority to CNB028284569A priority patent/CN1318380C/zh
Priority to JP2003565942A priority patent/JP4297267B2/ja
Publication of KR20030066246A publication Critical patent/KR20030066246A/ko
Priority to US10/913,300 priority patent/US20050080280A1/en
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fats And Perfumes (AREA)
KR1020020006593A 2002-02-05 2002-02-05 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법 KR100556337B1 (ko)

Priority Applications (6)

Application Number Priority Date Filing Date Title
KR1020020006593A KR100556337B1 (ko) 2002-02-05 2002-02-05 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법
AU2002248054A AU2002248054A1 (en) 2002-02-05 2002-04-09 Process for preparing an alkylester of fatty acid with high purity via one-step continuous process
PCT/KR2002/000629 WO2003066567A1 (en) 2002-02-05 2002-04-09 Process for preparing an alkylester of fatty acid with high purity via one-step continuous process
CNB028284569A CN1318380C (zh) 2002-02-05 2002-04-09 通过一步连续法制备脂肪酸烷基酯的方法
JP2003565942A JP4297267B2 (ja) 2002-02-05 2002-04-09 単一段階連続工程による高純度脂肪酸アルキルエステルの製造方法
US10/913,300 US20050080280A1 (en) 2002-02-05 2004-08-05 Process for producing alkylester of fatty acid in a single-phase continuous process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020020006593A KR100556337B1 (ko) 2002-02-05 2002-02-05 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법

Publications (2)

Publication Number Publication Date
KR20030066246A KR20030066246A (ko) 2003-08-09
KR100556337B1 true KR100556337B1 (ko) 2006-03-03

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KR1020020006593A KR100556337B1 (ko) 2002-02-05 2002-02-05 단일단계 연속공정을 통한 고순도 지방산 알킬에스테르의제조방법

Country Status (6)

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US (1) US20050080280A1 (zh)
JP (1) JP4297267B2 (zh)
KR (1) KR100556337B1 (zh)
CN (1) CN1318380C (zh)
AU (1) AU2002248054A1 (zh)
WO (1) WO2003066567A1 (zh)

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KR101028660B1 (ko) 2010-12-28 2011-04-12 주식회사 한두아이펨 방제용 약제 살포 장치
KR101034324B1 (ko) * 2008-04-30 2011-05-16 주식회사 한두아이펨 방제용 약제 살포 장치
KR101034323B1 (ko) * 2010-08-10 2011-05-16 주식회사 한두아이펨 방제용 약제 및 약제 살포 장치
KR101368047B1 (ko) 2013-07-22 2014-02-27 윤정용 고순도 메틸에스테르 제조 방법

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US20070282118A1 (en) * 2003-12-30 2007-12-06 Gupta Ashok K Process For Preparing Fatty Acid Alkylesters Using As Biodiesel
US7619104B2 (en) 2005-04-04 2009-11-17 Renewable Products Development Laboratories, Inc. Process for producing biodiesel or fatty acid esters from multiple triglyceride feedstocks
JP4219349B2 (ja) * 2005-09-16 2009-02-04 富士フイルム株式会社 脂肪酸アルキルエステルの製造方法及び燃料
US20070087085A1 (en) * 2005-10-17 2007-04-19 Bunge Oils, Inc. Protein-containing food product and coating for a food product and method of making same
US20080113067A1 (en) * 2005-10-17 2008-05-15 Monoj Sarma Protein-Containing Food Product and Coating for a Food Product and Method of Making Same
US20070148311A1 (en) * 2005-12-22 2007-06-28 Bunge Oils, Inc. Phytosterol esterification product and method of make same
US20080004458A1 (en) * 2006-06-20 2008-01-03 Wiedemann Rudolf A Transesterification catalyst mixing system
DE102006028560A1 (de) * 2006-06-22 2007-12-27 Cognis Ip Management Gmbh Verfahren zur Umesterung von Triglyceriden
EP1878716A1 (en) * 2006-07-14 2008-01-16 Rohm and Haas Company Method for transesterification of triglycerides
KR100725335B1 (ko) * 2006-07-20 2007-06-07 (주)퓨렉스에너지 고순도 메틸에스테르의 정제방법
US8445709B2 (en) * 2006-08-04 2013-05-21 Mcneff Research Consultants, Inc. Systems and methods for refining alkyl ester compositions
US7897798B2 (en) * 2006-08-04 2011-03-01 Mcneff Research Consultants, Inc. Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same
KR100843501B1 (ko) * 2007-01-29 2008-07-03 주식회사 가야에너지 버블링 술폰화 반응을 이용한 고수율 알파-술포 지방산알킬에스테르염의 제조 방법 및 이에 의해 생산된알파-술포 지방산 알킬 에스테르염
US8017796B2 (en) * 2007-02-13 2011-09-13 Mcneff Research Consultants, Inc. Systems for selective removal of contaminants from a composition and methods of regenerating the same
US8585976B2 (en) * 2007-02-13 2013-11-19 Mcneff Research Consultants, Inc. Devices for selective removal of contaminants from a composition
KR100864298B1 (ko) * 2007-02-21 2008-10-20 엄성일 고순도 메틸에스테르 제조방법
US7918905B2 (en) * 2007-05-17 2011-04-05 Baker Hughes Incorporated Method for improving biodiesel fuel
US20090023808A1 (en) * 2007-06-29 2009-01-22 Martek Biosciences Corporation Production and Purification of Esters of Polyunsaturated Fatty Acids
US7754905B2 (en) 2007-08-08 2010-07-13 Arisdyne Systems, Inc. Apparatus and method for producing biodiesel from fatty acid feedstock
US7935157B2 (en) 2007-08-08 2011-05-03 Arisdyne Systems, Inc. Method for reducing free fatty acid content of biodiesel feedstock
US7943791B2 (en) * 2007-09-28 2011-05-17 Mcneff Research Consultants, Inc. Methods and compositions for refining lipid feed stocks
US20090119979A1 (en) * 2007-11-08 2009-05-14 Imperial Petroleum, Inc. Catalysts for production of biodiesel fuel and glycerol
US8865080B2 (en) * 2008-06-09 2014-10-21 Renewable Energy Group, Inc. Devices, processes and methods for the production of lower alkyl esters
JP4876111B2 (ja) * 2008-09-18 2012-02-15 富士フイルム株式会社 脂肪酸石鹸含有量の調整法
US8361174B2 (en) * 2008-10-07 2013-01-29 Sartec Corporation Catalysts, systems, and methods for producing fuels and fuel additives from polyols
US9102877B2 (en) * 2008-11-12 2015-08-11 Sartec Corporation Systems and methods for producing fuels from biomass
US8637689B2 (en) 2010-08-31 2014-01-28 Biosynthetic Technologies, Llc Catalytic processes for preparing estolide base oils
US8624073B1 (en) * 2013-02-05 2014-01-07 Cpc Corporation, Taiwan Homogeneous catalysts for biodiesel production
CN106281723A (zh) * 2016-08-31 2017-01-04 菏泽尧舜牡丹生物科技有限公司 一种高酸价牡丹籽油乙酯化工艺
US10239812B2 (en) 2017-04-27 2019-03-26 Sartec Corporation Systems and methods for synthesis of phenolics and ketones
US10544381B2 (en) 2018-02-07 2020-01-28 Sartec Corporation Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid
US10696923B2 (en) 2018-02-07 2020-06-30 Sartec Corporation Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids
BR112021018808A8 (pt) * 2019-03-21 2022-07-05 Visionary Fiber Tech Inc Processo e sistema para produzir biodiesel
CN110790668B (zh) * 2019-10-22 2020-12-08 浙江工业大学 一种基于生物柴油制备脂肪酸丁酯的连续化生产方法
WO2022013278A1 (de) 2020-07-17 2022-01-20 Werner & Mertz Gmbh Verfahren zur herstellung eines biobasierten produkts, entsprechendes produkt und verwendungen
DE102020119024A1 (de) 2020-07-17 2022-01-20 Werner & Mertz Gmbh Verfahren zur Herstellung eines biobasierten Produkts, entsprechendes Produkt und Verwendungen

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US4371470A (en) * 1980-02-28 1983-02-01 Lion Corporation Method for manufacturing high quality fatty acid esters
EP0391485A1 (en) * 1989-04-05 1990-10-10 Unilever N.V. Process for producing fatty-acid lower-alkyl monoesters
US5354878A (en) * 1992-03-26 1994-10-11 Joosten Connemann Process for the continuous production of lower alkyl esters of higher fatty acids
US6127560A (en) * 1998-12-29 2000-10-03 West Central Cooperative Method for preparing a lower alkyl ester product from vegetable oil
KR20020028120A (ko) * 2000-10-07 2002-04-16 최재경 금속산화물 촉매를 이용한 지방산 에스테르의 제조방법

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JPS6025478B2 (ja) * 1977-03-17 1985-06-18 花王株式会社 脂肪酸低級アルコ−ルエステルの製造法
DE3421217A1 (de) * 1984-06-07 1985-09-05 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von fettsaeureestern kurzkettiger alkohole
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
AT399336B (de) * 1993-07-14 1995-04-25 Martin Mag Dr Mittelbach Verfahren zur herstellung von fettsäurealkylestern
JP3533061B2 (ja) * 1996-12-27 2004-05-31 有限会社染谷商店 廃食用油等から高級脂肪酸のメチルエステルとグリセリンとを連続的に製造する方法および装置
US20030032826A1 (en) * 2001-07-20 2003-02-13 The Board Of Regents Of The University Of Nebraska Transesterification process for production of biodiesel

Patent Citations (5)

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Publication number Priority date Publication date Assignee Title
US4371470A (en) * 1980-02-28 1983-02-01 Lion Corporation Method for manufacturing high quality fatty acid esters
EP0391485A1 (en) * 1989-04-05 1990-10-10 Unilever N.V. Process for producing fatty-acid lower-alkyl monoesters
US5354878A (en) * 1992-03-26 1994-10-11 Joosten Connemann Process for the continuous production of lower alkyl esters of higher fatty acids
US6127560A (en) * 1998-12-29 2000-10-03 West Central Cooperative Method for preparing a lower alkyl ester product from vegetable oil
KR20020028120A (ko) * 2000-10-07 2002-04-16 최재경 금속산화물 촉매를 이용한 지방산 에스테르의 제조방법

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101034324B1 (ko) * 2008-04-30 2011-05-16 주식회사 한두아이펨 방제용 약제 살포 장치
KR101034323B1 (ko) * 2010-08-10 2011-05-16 주식회사 한두아이펨 방제용 약제 및 약제 살포 장치
KR101028660B1 (ko) 2010-12-28 2011-04-12 주식회사 한두아이펨 방제용 약제 살포 장치
KR101368047B1 (ko) 2013-07-22 2014-02-27 윤정용 고순도 메틸에스테르 제조 방법

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US20050080280A1 (en) 2005-04-14
JP4297267B2 (ja) 2009-07-15
JP2005517002A (ja) 2005-06-09
AU2002248054A1 (en) 2003-09-02
CN1318380C (zh) 2007-05-30
WO2003066567A1 (en) 2003-08-14
CN1622933A (zh) 2005-06-01
KR20030066246A (ko) 2003-08-09

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