JPS63180948A - Base for photographic paper - Google Patents
Base for photographic paperInfo
- Publication number
- JPS63180948A JPS63180948A JP1283387A JP1283387A JPS63180948A JP S63180948 A JPS63180948 A JP S63180948A JP 1283387 A JP1283387 A JP 1283387A JP 1283387 A JP1283387 A JP 1283387A JP S63180948 A JPS63180948 A JP S63180948A
- Authority
- JP
- Japan
- Prior art keywords
- paper
- photographic paper
- alkyl ketene
- ketene dimer
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- -1 alkyl ketene dimer Chemical compound 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 10
- 229920005989 resin Polymers 0.000 claims description 19
- 239000011347 resin Substances 0.000 claims description 19
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 12
- 238000004513 sizing Methods 0.000 abstract description 10
- 125000004432 carbon atom Chemical group C* 0.000 abstract description 4
- 239000000654 additive Substances 0.000 abstract description 2
- 125000000217 alkyl group Chemical group 0.000 abstract description 2
- 239000002216 antistatic agent Substances 0.000 abstract description 2
- 239000000975 dye Substances 0.000 abstract description 2
- 239000000945 filler Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract 2
- 229910021502 aluminium hydroxide Inorganic materials 0.000 abstract 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 abstract 1
- 229910001679 gibbsite Inorganic materials 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000003755 preservative agent Substances 0.000 abstract 1
- 230000002335 preservative effect Effects 0.000 abstract 1
- 239000012744 reinforcing agent Substances 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000002585 base Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 3
- 238000010894 electron beam technology Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 229920005672 polyolefin resin Polymers 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 229910001864 baryta Inorganic materials 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 238000007765 extrusion coating Methods 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 229920001684 low density polyethylene Polymers 0.000 description 2
- 239000004702 low-density polyethylene Substances 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000001055 blue pigment Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229920001903 high density polyethylene Polymers 0.000 description 1
- 239000004700 high-density polyethylene Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/76—Photosensitive materials characterised by the base or auxiliary layers
- G03C1/775—Photosensitive materials characterised by the base or auxiliary layers the base being of paper
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
Abstract
Description
【発明の詳細な説明】
（産業上の利用分野）
本発明は写真印画紙用支持体に関するものであり、ざら
に詳しくは原紙の両面を樹脂で被覆した写真印画紙用支
持体において、印画紙端部の裁断面からの現像処理液（
以下現像液と記す）の浸み込みによるエッチ汚れを防止
した写真印画紙用支持体に関するものである。Detailed Description of the Invention (Field of Industrial Application) The present invention relates to a support for photographic paper, and more specifically, in a support for photographic paper in which both sides of a base paper are coated with a resin, the present invention relates to a support for photographic paper. The developing solution from the cut surface of the edge (
The present invention relates to a support for photographic paper that prevents etch stains caused by penetration of a developer (hereinafter referred to as developer).
（従来技術）
従来印画紙用支持体としては、紙の片面に硫酸バリウム
を主体とするバライタ層を被覆した、いわゆるバライタ
紙が使用されていたが、最近では現像処理の自動化迅速
化を図る為に原紙の両面を樹脂で被覆した防水印画紙が
使用される様になってきた。しかしながら上記防水印画
紙を使用した場合でも、印画紙端部の切断面からの現像
液の浸透は防止できない。端部の切断面から浸透した現
像液は短時間の写真処理では除去できず、熱あるいは経
時により茶色に変色し、写真のエッチ部の汚れとなり、
写真としての価値を著しく損う。このエッチ汚れを防止
する為に原紙層に高いサイズ性を付与する方法が試みら
れている。(Prior art) Conventionally, so-called baryta paper, in which one side of the paper is coated with a baryta layer mainly composed of barium sulfate, has been used as a support for photographic paper, but recently, in order to automate and speed up the development process, Waterproof photographic paper, in which both sides of the base paper are coated with resin, has come into use. However, even when the waterproof photographic paper is used, it is not possible to prevent the developer from permeating through the cut edges of the photographic paper. The developer that permeates through the cut edges cannot be removed by short-term photo processing, and will turn brown due to heat or over time, staining the etched areas of the photo.
The value as a photograph is significantly diminished. In order to prevent this etching stain, attempts have been made to provide the base paper layer with a high degree of size.
特公昭４７ ２６９６１＠に示すごとく脂肪酸石けんタ
イプのサイズ剤や、特開昭５１−１３２８２２号に示す
ごとくアルキルケテンダイマー等が写真印画紙用支持体
のサイズ剤として用いられているが、それぞれ欠点を有
し、十分なものではない。すなわち、脂肪酸石けんタイ
プのサイズ剤は現像液中のアルカリに対してサイズ効果
が低く、原紙を製造する際、用水の硬度の影響を受は易
い等の欠点がある。一方、アルキルケテンダイマーの場
合は現像液中のアルコールに対してサイズ効果が低く、
又定着剤として公知のポリアミドポリアミンエピクロル
ヒドリン樹脂を比較的多量に使用しないと十分なサイズ
性が得られないという欠点を有しており、いずれのサイ
ズ剤も写真印画紙用として十分満足すべきものではない
。Fatty acid soap type sizing agents as shown in JP-B No. 47-26961 @ and alkyl ketene dimers as shown in JP-A-51-132822 have been used as sizing agents for photographic paper supports, but each has drawbacks. have, but are not sufficient. That is, fatty acid soap type sizing agents have drawbacks such as having a low sizing effect on alkali in the developer and being easily affected by the hardness of water when producing base paper. On the other hand, alkyl ketene dimers have a low size effect on the alcohol in the developer,
Furthermore, it has the disadvantage that sufficient sizing properties cannot be obtained unless a relatively large amount of polyamide polyamine epichlorohydrin resin, which is known as a fixing agent, is used, and neither sizing agent is fully satisfactory for use in photographic paper. .
（発明が解決しようとする問題点）
したがって本発明の目的は、樹脂被覆された写真印画紙
用支持体の端部へ現像液が浸み込んで発生するエッチ汚
れを防止する事である。(Problems to be Solved by the Invention) Therefore, it is an object of the present invention to prevent etch stains caused by a developer seeping into the edges of a resin-coated photographic paper support.
（問題点を解決するための手段および作用）本発明者は
、前述の欠点を克服する為鋭意研究の結果、原紙の両面
を樹脂被覆した写真印画紙用支持体において、該原紙中
にアルキルケテンダイマーおよびポリ水酸化アルミニウ
ムを含有することを特徴とする写真印画紙用支持体によ
り達成された。(Means and effects for solving the problem) In order to overcome the above-mentioned drawbacks, the inventor of the present invention, as a result of intensive research, discovered that alkyl ketene is present in the base paper in a support for photographic paper in which both sides of the base paper are coated with resin. This was achieved with a support for photographic paper characterized by containing dimer and polyaluminum hydroxide.
本発明に使用されるアルキルケテンダイマーは例えば前
述の特開昭５１−１３２８２２号、およびＴａ１）Ｄｉ
ＶＯｌ、３９．ＮＯｌ （１９５６＞等に開示されて
いるもので、アルキル基の炭素数が８〜３０、好ましく
は１２〜１８のものが良い。The alkyl ketene dimer used in the present invention is, for example, disclosed in the above-mentioned JP-A-51-132822 and Ta1) Di
VOl, 39. NOl (1956> etc.), and the alkyl group has 8 to 30 carbon atoms, preferably 12 to 18 carbon atoms.
本発明に使用されるポリ水酸化アルミニウムとしては、
（Ａｊ （ＯＨ）３｝ｎ−ＡｌｌＣｆ３の構造を持ち、
ｎ＝２０±１であるものが好ましい。The polyaluminum hydroxide used in the present invention includes:
It has the structure (Aj (OH)3}n-AllCf3,
Preferably, n=20±1.
上記の本発明の効果は、アルキルケテンダイマーとポリ
水酸化アルミニウムを併用することによりはじめて得ら
れるものであり、各単独の添加では得られないものであ
る。The above-mentioned effects of the present invention can only be obtained by using the alkyl ketene dimer and polyaluminum hydroxide together, and cannot be obtained by adding each alone.
本発明においてアルキルケテンダイマー、ポリ水酸化ア
ルミニウムは内添として使用する方が好ましい。又、こ
の他に一般に製紙で用いられているサイズ剤１、紙力増
強剤、定着剤、保持剤、填料、染料、帯電防止剤等の内
部添叩剤および表面サイズ剤を適宜含有させることも可
能である。In the present invention, it is preferable to use the alkyl ketene dimer and polyaluminum hydroxide as internal additions. In addition, internal additives and surface sizing agents such as sizing agents 1, paper strength enhancers, fixing agents, retention agents, fillers, dyes, and antistatic agents, which are generally used in paper manufacturing, may be appropriately included. It is possible.
アルキルケテンダイマーの添加量は対パルプ絶乾重量当
り０．２〜３．０重量％であることが望ましく又、アル
キルケテンダイマーに対するポリ水酸イヒアルミニウム
の比率は１／１０〜２／１、好ましくは１１５〜１／１
である。The amount of the alkyl ketene dimer added is preferably 0.2 to 3.0% by weight based on the absolute dry weight of the pulp, and the ratio of the aluminum polyhydroxide to the alkyl ketene dimer is preferably 1/10 to 2/1. is 115~1/1
It is.
本発明により製造される原紙に於て使用するパルプは、
通常の製紙で用いられるパルプは勿論のこと合成パルプ
も“用いることが出来る。The pulp used in the base paper produced by the present invention is
Not only pulps used in normal papermaking, but also synthetic pulps can be used.
本発明に使用される樹脂としては、ポリオレフィン樹脂
や電子線により硬化する樹脂を用いることができる。ポ
リオレフィン樹脂としては、ポリエチレン、ポリプロピ
レン等が好ましい。又樹脂に酸化チタン、アルミナ等の
白色顔料、青色顔料、通常樹脂に混合される安定剤、酸
化防止剤、分散剤、滑剤等を加えても良い。As the resin used in the present invention, polyolefin resins and resins that can be cured by electron beams can be used. As the polyolefin resin, polyethylene, polypropylene, etc. are preferable. Furthermore, white pigments such as titanium oxide and alumina, blue pigments, stabilizers, antioxidants, dispersants, lubricants, etc. that are usually mixed with resins may be added to the resin.
本発明により製造される樹脂被覆紙は、走行する原紙上
にポリオレフイ・ン樹脂の場合は、加熱溶融した樹脂を
流延するいわゆる押出コーティング法によって製造され
、その両面が樹脂により被覆される。又電子線により硬
化する樹脂の場合は、グラビアコーター、ブレードコー
ター等一般に用いられるコーターにより樹脂を塗布した
後、電子線を照射し、樹脂を硬化させて被覆する。The resin-coated paper produced according to the present invention is produced by a so-called extrusion coating method in which a heated molten resin is cast onto a running base paper in the case of a polyolefin resin, and both sides of the paper are coated with the resin. In the case of a resin that can be cured by electron beams, the resin is applied with a commonly used coater such as a gravure coater or a blade coater, and then the resin is irradiated with electron beams to cure the resin and cover the resin.
本発明により製造される写真印画紙用支持体は、カラー
印画紙用紙、白黒印画紙用紙、写植印画紙用紙、複写印
画紙用紙等に使用される。The support for photographic paper produced according to the present invention is used for color photographic paper, black and white photographic paper, typesetting photographic paper, duplicating photographic paper, and the like.
（発明の実施例） 以下に実施例を挙げ本発明の詳細な説明を行う。(Example of the invention) The present invention will be described in detail below with reference to Examples.
なお、本発明はこれらの実施例に限定されるものではな
い。Note that the present invention is not limited to these examples.
木材パルプ（ＬＢＫＰ／ＮＢＫＰ、１／１ ）繊維をビ
ータ−により、カナダ標Ｑ濾水度で３５０ｄまで叩解し
、第１表および第２表に示す内添配合に従って、通常の
抄紙法により１６０ｇ／ＴＩｌの紙を抄紙した。Wood pulp (LBKP/NBKP, 1/1) fibers were beaten with a beater to a Canadian standard Q freeness of 350d, and according to the internal addition ratio shown in Tables 1 and 2, 160g/ TIL paper was made.
次にこの原紙の表面に酸化チタン１０％を含む低密度ポ
リエチレンを、裏面２には低密度ポリエチレン／高密度
ポリエチレン＝１７１をそれぞれ樹脂温度３３０’Ｃで
押出塗工機により３０譚の厚さにコーティングし、写真
印画紙用支持体を得た。Next, low-density polyethylene containing 10% titanium oxide is applied to the front side of this base paper, and low-density polyethylene/high-density polyethylene = 171 is applied to the back side 2 to a thickness of 30 mm using an extrusion coating machine at a resin temperature of 330'C. A support for photographic paper was obtained by coating.
エッチ汚れの評価は次の方法により行った。すなわち、
巾８．２５ ｃｍに裁断した写真印画紙用支持体を連続
自動現像ＩＪ！（ＦＣ製作所製、カラーロールプロセッ
サー）によって現仰処理した。処理を終った支持体端部
の裁断面からの現像液の浸み込み深さを拡大鏡を用いて
読み取った。その結果を第１表および第２表に示す。Etch stains were evaluated by the following method. That is,
Continuous automatic development of photographic paper supports cut to a width of 8.25 cm using IJ! (Color Roll Processor, manufactured by FC Seisakusho). The depth of penetration of the developer from the cut surface of the end of the support after the treatment was read using a magnifying glass. The results are shown in Tables 1 and 2.
第１表および第２表の結果より明らかな様に、本発明に
より製造された支持体はエッチ汚れが改良され、写真印
画紙用支持体として優れていることがわかる。As is clear from the results in Tables 1 and 2, the supports produced according to the present invention have improved etch stains and are excellent as supports for photographic paper.
（以下余白）(Margin below)
Claims (3)
において、該原紙中にアルキルケテンダイマーおよびポ
リ水酸化アルミニウムを含有することを特徴とする写真
印画紙用支持体。(1) A support for photographic paper comprising a base paper coated on both sides with resin, characterized in that the base paper contains an alkyl ketene dimer and polyaluminum hydroxide.
ｎ・ＡｌＣｌ＿３の構造でｎ＝２０±１である特許請求
の範囲第１項記載の写真印画紙用支持体。(2) Poly aluminum hydroxide {Al(OH)_3}
The support for photographic paper according to claim 1, which has a structure of n.AlCl_3 and n=20±1.
テンダイマー添加量に対して、その比率が１／１０〜２
／１である特許請求 の範囲第１項記載の写真印画紙用支持体。(3) The ratio of the amount of polyaluminum hydroxide added to the amount of alkyl ketene dimer added is 1/10 to 2
1. The support for photographic paper according to claim 1, wherein: /1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1283387A JPS63180948A (en) | 1987-01-21 | 1987-01-21 | Base for photographic paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1283387A JPS63180948A (en) | 1987-01-21 | 1987-01-21 | Base for photographic paper |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS63180948A true JPS63180948A (en) | 1988-07-26 |
Family
ID=11816374
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1283387A Pending JPS63180948A (en) | 1987-01-21 | 1987-01-21 | Base for photographic paper |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS63180948A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1990013707A1 (en) * | 1989-04-28 | 1990-11-15 | Arakawa Kagaku Kogyo Kabushiki Kaisha | Papermaking size based on ketene dimer |
| US10982391B2 (en) | 2016-06-01 | 2021-04-20 | Ecolab Usa Inc. | High-efficiency strength program used for making paper in higher charge demand system |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56109343A (en) * | 1980-02-01 | 1981-08-29 | Mitsubishi Paper Mills Ltd | Photographic paper |
| JPS57197539A (en) * | 1981-05-29 | 1982-12-03 | Fuji Photo Film Co Ltd | Support for waterproof photographic paper |
| JPS6034698A (en) * | 1983-07-01 | 1985-02-22 | プロデコ・ソチエタ・ペル・アチオニ | Paper sizing method |
-
1987
- 1987-01-21 JP JP1283387A patent/JPS63180948A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56109343A (en) * | 1980-02-01 | 1981-08-29 | Mitsubishi Paper Mills Ltd | Photographic paper |
| JPS57197539A (en) * | 1981-05-29 | 1982-12-03 | Fuji Photo Film Co Ltd | Support for waterproof photographic paper |
| JPS6034698A (en) * | 1983-07-01 | 1985-02-22 | プロデコ・ソチエタ・ペル・アチオニ | Paper sizing method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1990013707A1 (en) * | 1989-04-28 | 1990-11-15 | Arakawa Kagaku Kogyo Kabushiki Kaisha | Papermaking size based on ketene dimer |
| US10982391B2 (en) | 2016-06-01 | 2021-04-20 | Ecolab Usa Inc. | High-efficiency strength program used for making paper in higher charge demand system |
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