JPS6169924A - Method for heating electromagnetic steel slab - Google Patents

Method for heating electromagnetic steel slab

Info

Publication number
JPS6169924A
JPS6169924A JP18502585A JP18502585A JPS6169924A JP S6169924 A JPS6169924 A JP S6169924A JP 18502585 A JP18502585 A JP 18502585A JP 18502585 A JP18502585 A JP 18502585A JP S6169924 A JPS6169924 A JP S6169924A
Authority
JP
Japan
Prior art keywords
slab
heating
steel
steel slab
atmosphere
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP18502585A
Other languages
Japanese (ja)
Other versions
JPH0524202B2 (en
Inventor
Morio Shiozaki
塩崎 守雄
Tomohiko Sakai
酒井 知彦
Yoshitoshi Nishikawa
西川 俊寿
Tamotsu Kawakami
川上 保
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP18502585A priority Critical patent/JPS6169924A/en
Publication of JPS6169924A publication Critical patent/JPS6169924A/en
Publication of JPH0524202B2 publication Critical patent/JPH0524202B2/ja
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1205Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties involving a particular fabrication or treatment of ingot or slab

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Manufacturing & Machinery (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing Of Steel Electrode Plates (AREA)

Abstract

PURPOSE:To prevent the generation of scale of low melt point on the surface of a steel slab and the lowering of yield with a molten scale of the steel slab by performing a high-temperature heating in a conduction furnace which is made to adjust an incorporated amount of O2 at the specified amount at the heating for hot-rolling the electromagnetic slab. CONSTITUTION:A connecting cast slab of an electromagnetic steel is heated by a fuel combustion heater at 1,250 deg.C for hot rolling at 1,250-1,400 deg.C. Further, the slab is incorporated in an conductive heater of atmosphere, which is adjusted <=10% O2 at higher temperature of hot rolling. The steel slab is heated rapidly so that the temperature of the surface of the steel slab can be >=1,325 deg.C. The small amount of O2 of atmosphere in the electrical furnace prevents the lowering of yield of the steel slab due to the generation of scale of low melt point by oxidation on the surface of the steel plate. Further, the magnetism of the steel plate obtained by the slab is superior.

Description

【発明の詳細な説明】 本発明は連続鋳造法によシ得た電磁鋼スラブの加熱方法
に係)、その目的は加熱時の溶融スケールの生成を抑え
て鉄歩留υの向上を図ると共に成品の表面疵を防止する
ところにある。
[Detailed Description of the Invention] The present invention relates to a method for heating an electrical steel slab obtained by a continuous casting method), and its purpose is to suppress the formation of molten scale during heating and improve the iron yield υ. Its purpose is to prevent surface flaws on the product.

周知の如く一方向性電磁鋼板の製造においては、−次男
結晶粒の正常粒成長を抑制するために、MnS、AA!
N等の析出分散相が用いられている口これらの析出分散
相を制御するために、熱延加熱温度は1250〜140
0℃の高温加熱が必要であシ、そのため、一方向性電磁
鋼板のスラブ加熱では、普通の鋼材と比較して、 (1)  溶損による鉄ロスで歩留低下が大きい。
As is well known, in the production of unidirectional electrical steel sheets, MnS, AA!
When a precipitated dispersed phase such as N is used, the hot rolling heating temperature is set at 1250 to 140° C. to control the precipitated dispersed phase.
High-temperature heating of 0°C is required, and therefore, in slab heating of unidirectional electrical steel sheets, compared to ordinary steel materials, (1) Yield reduction is greater due to iron loss due to melting damage.

(2)加熱炉内の堆積70の除去が必要である。(2) It is necessary to remove the deposit 70 in the heating furnace.

従来の熱延加熱炉内の溶損についてのべれば鉄の融点(
1535°C)以下の温度で表面が溶融するのけ、加熱
中にスラブ表面が酸化して、Siを含有する低融点のス
ケールを形成するからである。
Regarding melting loss in a conventional hot rolling heating furnace, the melting point of iron (
This is because although the surface melts at temperatures below 1535°C, the slab surface oxidizes during heating to form a low melting point scale containing Si.

連続鋳造法により得られた電磁鋼スラブを燃料燃焼炉で
1250〜1300°Cの間の温度に加熱し、続いて誘
導加熱又は抵抗加熱の如き電気加熱によ、91350〜
1400℃の間に加熱する方法が特公昭47−1462
7号公報で提案されており、これよ)磁気特性が向上し
、又電気加熱方式による急速短時間加熱により材料の損
失が減少することが示されている口 本発明者らは電磁鋼スラブの加熱に電気加熱方式を採用
することについて詳細に検討を行った。
Electrical steel slabs obtained by continuous casting are heated in a fuel-burning furnace to a temperature between 1250 and 1300°C, followed by electrical heating such as induction heating or resistance heating to a temperature between 91350 and 1300°C.
The method of heating to 1400℃ was published in Japanese Patent Publication No. 47-1462.
The present inventors have proposed an electrical steel slab that improves magnetic properties and reduces material loss due to rapid short-term heating using an electric heating method. We conducted a detailed study on adopting an electric heating method for heating.

その結果、雰囲気制御した誘導加熱炉を用いてスラブの
加熱実験を繰り返して、大気中(02約20%)で加熱
した場合には、スラブ表面温度が1325°Cを越える
と、溶融スケールが発生し溶損が始まること、および雰
囲気中の02濃度を10%以下に制御することによp、
1375℃の高温でも溶融スケールが発生しないことを
確めた。
As a result, we repeatedly conducted slab heating experiments using an atmosphere-controlled induction heating furnace, and found that when the slab surface temperature exceeded 1325°C, melting scale occurred when the slab was heated in the atmosphere (approximately 20%). By controlling the 02 concentration in the atmosphere to 10% or less,
It was confirmed that no melting scale was generated even at a high temperature of 1375°C.

第1図は誘導加熱炉で、一方同性電磁鋼スラブを加熱し
た場合のスラブ表面温度及び炉内雰囲気中02濃度とス
ラブ酸化減量の関係を示したものである。
FIG. 1 shows the relationship between slab surface temperature, 02 concentration in the furnace atmosphere, and slab oxidation loss when a homogeneous electrical steel slab is heated in an induction heating furnace.

即ち、スラブ加熱炉として、従来の燃料燃焼炉では、雰
囲気中の02flk度を10%以下に制御することは困
難であるが、霞導加熱等の電気加熱方式音用いた炉では
雰囲気制御が容易で、MnS * AZN等のインヒビ
ターを完全に固溶させる温度条件下で、溶融スケールの
発生をよシ完全に防止することが可能となった。
In other words, it is difficult to control the 02flk degree in the atmosphere to 10% or less in a conventional fuel combustion furnace as a slab heating furnace, but it is easy to control the atmosphere in a furnace that uses electric heating and sound such as haze conduction heating. Therefore, it has become possible to completely prevent the occurrence of melted scale under temperature conditions that completely dissolve the inhibitor such as MnS*AZN.

本発明に於いて対象とする加熱方式としては、前掲の特
公昭47−14627号公報記載の燃料燃焼炉と誘導加
熱炉との組合せにより、燃料燃焼炉では1250℃まで
の加熱を行ない、誘導加熱炉では1250℃〜1400
℃の加熱を行なうことが好ましい。本発明においてはこ
の誘導加熱炉で、表面温度が1325℃を越える高温に
加熱する場合にその雰囲気中の02濃度を10%以下に
抑えるものである。
The heating method targeted by the present invention is a combination of a fuel combustion furnace and an induction heating furnace described in the above-mentioned Japanese Patent Publication No. 47-14627. In the furnace 1250℃~1400℃
It is preferable to perform heating at .degree. In the present invention, when heating to a high surface temperature exceeding 1325° C. in this induction heating furnace, the 02 concentration in the atmosphere is suppressed to 10% or less.

以下実施例を説明する。Examples will be described below.

実施例1 転炉で溶製し、真空脱ガス装置で脱ガスおよび成分微調
整を行ったCQ、04%、 Si 3.19% 、 M
n0.06係、80.02%の組下成分の溶錦を250
mm厚スラブに連続鋳造し、鋳造完了後、1250℃に
設定した燃料燃焼加熱炉に装入した。1250℃に均熱
されたスラブを更にN2ガス/4′−ノによシ02量を
10%以下に雰囲気制御した誘導加熱炉に装入し、急速
加熱をして、表面温度1350℃X30分の均熱をさせ
た後熱延を行った。その他のスラブはそのままの状態で
、従来方式の燃料燃焼加熱炉に装入し、1350’(、
に均熱した後、熱延を行った。これらのホットコイルを
中間焼鈍を含む2回圧延性工程で通板し、板厚0.30
団の成品とした結果を第1表に示す 第 1 表 実施例2 転炉で溶製し、真空脱ガス装置で脱ガス2よび成分微調
整を行った C0,05%、 St 3.i 3% 、
 Mn0.07%、30.02%の組下成分の溶鋼t 
250 mmmススラブ連続鋳造し、鋳造完了後、12
50℃に設定した燃料燃焼炉に装入し、1250℃に均
熱されたスラブを更にNffff−ジによシ0□量を1
%以下に雰囲気制御した誘導加熱炉に装入し、急速加熱
して、表面温度1370℃×30分の均熱をさせた後、
熱延を行った。残シのスラブは、従来方式の燃料燃焼加
熱炉に装入し、1350℃に均熱した後、熱延を行った
。これらのホットコイルを中間焼鈍を含む2回圧延性工
程で通板し、板厚0.30mzの成品とした結果を第2
表に示す。
Example 1 CQ, 04%, Si 3.19%, M melted in a converter, degassed in a vacuum degassing device, and finely adjusted the components.
250% n0.06, molten brocade with 80.02% composition
It was continuously cast into a mm thick slab, and after the casting was completed, it was charged into a fuel combustion heating furnace set at 1250°C. The slab soaked at 1250°C was further charged into an induction heating furnace in which the atmosphere was controlled to 10% or less with N2 gas/4'-NO gas, and rapidly heated to a surface temperature of 1350°C for 30 minutes. After soaking, hot rolling was performed. The other slabs were charged as they were into a conventional fuel-fired heating furnace.
After soaking, hot rolling was performed. These hot coils were passed through a two-time rolling process including intermediate annealing to a plate thickness of 0.30.
The results are shown in Table 1.Table 1 Example 2 Molten in a converter, degassed in a vacuum degassing device and fine-tuned the components.C0.05%, St 3. i 3%,
Molten steel with Mn components of 0.07% and 30.02%
Continuously cast 250 mm slabs, and after completion of casting, 12
The slab was charged into a fuel combustion furnace set at 50°C and soaked at 1250°C.
After charging into an induction heating furnace whose atmosphere was controlled to below %, rapidly heating it, and soaking it for 30 minutes at a surface temperature of 1370°C,
Hot rolling was performed. The remaining slab was charged into a conventional fuel combustion heating furnace, heated to 1350°C, and then hot rolled. These hot coils were passed through a two-time rolling process including intermediate annealing, and the results of the finished product with a thickness of 0.30 mz are shown in the second table.
Shown in the table.

第 2 表 上記実施例1及び2からも明らかな様に、本発明方法に
よシ鉄歩留ロス及び磁性共に良好な結果が得られた。
Table 2 As is clear from Examples 1 and 2 above, the method of the present invention yielded good results in terms of iron yield loss and magnetism.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は誘導加熱炉で一方向性電磁鋼スラブを加熱した
場合のスラブ表面温度及び炉内雰囲気中0□濃度とスラ
ブ酸化減量の関係を示したものである。
FIG. 1 shows the relationship between the slab surface temperature, the 0□ concentration in the furnace atmosphere, and the slab oxidation weight loss when a unidirectional electrical steel slab is heated in an induction heating furnace.

Claims (1)

【特許請求の範囲】[Claims] 連続鋳造された電磁鋼スラブを1250〜1400℃の
温度に加熱後圧延する方法において、スラブ表面温度が
1325℃以上の高温域の加熱を、雰囲気中のO_2濃
度を10%以下に調整した誘導加熱炉により行なうこと
を特徴とする電磁鋼スラブの加熱方法。
In a method in which a continuously cast electromagnetic steel slab is heated to a temperature of 1250 to 1400°C and then rolled, heating in a high temperature range where the slab surface temperature is 1325°C or higher is performed by induction heating in which the O_2 concentration in the atmosphere is adjusted to 10% or less. A method of heating an electromagnetic steel slab characterized by heating it using a furnace.
JP18502585A 1985-08-24 1985-08-24 Method for heating electromagnetic steel slab Granted JPS6169924A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP18502585A JPS6169924A (en) 1985-08-24 1985-08-24 Method for heating electromagnetic steel slab

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP18502585A JPS6169924A (en) 1985-08-24 1985-08-24 Method for heating electromagnetic steel slab

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
JP15396481A Division JPS5858228A (en) 1981-09-30 1981-09-30 Heating method for electrical steel slab

Publications (2)

Publication Number Publication Date
JPS6169924A true JPS6169924A (en) 1986-04-10
JPH0524202B2 JPH0524202B2 (en) 1993-04-07

Family

ID=16163461

Family Applications (1)

Application Number Title Priority Date Filing Date
JP18502585A Granted JPS6169924A (en) 1985-08-24 1985-08-24 Method for heating electromagnetic steel slab

Country Status (1)

Country Link
JP (1) JPS6169924A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0543936A (en) * 1991-08-12 1993-02-23 Nippon Steel Corp Method for heating grain oriented electrical steel slab
JPH06212247A (en) * 1993-01-11 1994-08-02 Nippon Steel Corp Method for controlling atmosphere in induction heating furnace
KR100259400B1 (en) * 1994-07-22 2000-06-15 에모또 간지 Method of manufacturing grain oriented silicon steel exhibiting excellent magnetic characteristics over the entire length of coil thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0543936A (en) * 1991-08-12 1993-02-23 Nippon Steel Corp Method for heating grain oriented electrical steel slab
JP2563695B2 (en) * 1991-08-12 1996-12-11 新日本製鐵株式会社 Method of heating grain-oriented electrical steel slabs
JPH06212247A (en) * 1993-01-11 1994-08-02 Nippon Steel Corp Method for controlling atmosphere in induction heating furnace
KR100259400B1 (en) * 1994-07-22 2000-06-15 에모또 간지 Method of manufacturing grain oriented silicon steel exhibiting excellent magnetic characteristics over the entire length of coil thereof

Also Published As

Publication number Publication date
JPH0524202B2 (en) 1993-04-07

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