JPS5767571A - Production of thiol carbamate derivative - Google Patents
Production of thiol carbamate derivativeInfo
- Publication number
- JPS5767571A JPS5767571A JP55142582A JP14258280A JPS5767571A JP S5767571 A JPS5767571 A JP S5767571A JP 55142582 A JP55142582 A JP 55142582A JP 14258280 A JP14258280 A JP 14258280A JP S5767571 A JPS5767571 A JP S5767571A
- Authority
- JP
- Japan
- Prior art keywords
- thiolcarbamate
- production
- produce
- added
- aqueous solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
PURPOSE: The same amine as that constituting the thiolcarbamate salt as well as a basic substance are added to the reaction system and a thiolcarbamic acid and an α,β-dimethylbenzylchloride are made to react in an aqueous solvent to produce the titled compound, inhibiting side-reactions.
CONSTITUTION: When the reaction of a thiolcarbamate salt of formulaI(R is H, methyl, ethyl; m is 1W2; n is 4W6; M is alkali metal) with α,α-dimethylbenzyl chloride is effected in an aqueous solvent to produce a thiolcarbamate derivative of formula II such as N-(α,α-dimethylbenzylthiolcarbonyl)pyrrolidine, a basic substance such as sodium hydroxide and an amine of formula III, which is the starting material of the thiolcarbamic acid, such as hexamethyleneimine are added by 0.5W1.5mol and 2.0W30mol%/mol of the thiolcarbamate respectively.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55142582A JPS5767571A (en) | 1980-10-13 | 1980-10-13 | Production of thiol carbamate derivative |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55142582A JPS5767571A (en) | 1980-10-13 | 1980-10-13 | Production of thiol carbamate derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5767571A true JPS5767571A (en) | 1982-04-24 |
Family
ID=15318653
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55142582A Pending JPS5767571A (en) | 1980-10-13 | 1980-10-13 | Production of thiol carbamate derivative |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5767571A (en) |
-
1980
- 1980-10-13 JP JP55142582A patent/JPS5767571A/en active Pending
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