JPS56108781A - Preparation of glycidyl ether - Google Patents

Preparation of glycidyl ether

Info

Publication number
JPS56108781A
JPS56108781A JP1111580A JP1111580A JPS56108781A JP S56108781 A JPS56108781 A JP S56108781A JP 1111580 A JP1111580 A JP 1111580A JP 1111580 A JP1111580 A JP 1111580A JP S56108781 A JPS56108781 A JP S56108781A
Authority
JP
Japan
Prior art keywords
alcohol
epihalohydrin
reacting
integer
aqueous solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1111580A
Other languages
Japanese (ja)
Other versions
JPS603392B2 (en
Inventor
Naotake Takaishi
Koichi Urata
Yoshiaki Inamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp filed Critical Kao Corp
Priority to JP1111580A priority Critical patent/JPS603392B2/en
Priority to ES499016A priority patent/ES8201149A1/en
Priority to DE19813103181 priority patent/DE3103181A1/en
Publication of JPS56108781A publication Critical patent/JPS56108781A/en
Publication of JPS603392B2 publication Critical patent/JPS603392B2/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/22—Ethers with hydroxy compounds containing no oxirane rings with monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds

Abstract

PURPOSE: To prepare the titled compound, economically, in high yield, by reacting an alcohol with an epihalohydrin in the presence of an aqueous solution of an alkaline substance and a quaternary ammonium compound having (poly)oxyalkylene group in the molecule.
CONSTITUTION: The titled compound having a wide range of industrial applications as intermediates of glycerol derivatives, etc., is prepared easily, in one step from the starting materials, in high yield and an industrial scale, by reacting an alcohol with an epihalohydrin in the presence of an aqueous solution of an alkaline substance such as an alkali metal hydroxide or a weak acid salt of an alkali metal and a catalytic amount (pref. 0.01W0.1mol, based on the alcohol) of a quaternary ammonium compound of formula I or II (R1WR3 are alkyl, aralkyl or cycloalkyl; A is alkylene; a is an integer of ≥1); b and c are an integer of ≥0, and b+c≥2; X is anion) at 0W100°C.
COPYRIGHT: (C)1981,JPO&Japio
JP1111580A 1980-02-01 1980-02-01 Manufacturing method of glycidyl ether Expired JPS603392B2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP1111580A JPS603392B2 (en) 1980-02-01 1980-02-01 Manufacturing method of glycidyl ether
ES499016A ES8201149A1 (en) 1980-02-01 1981-01-30 Preparation of glycidyl ether
DE19813103181 DE3103181A1 (en) 1980-02-01 1981-01-30 Process for the preparation of glycidyl ethers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1111580A JPS603392B2 (en) 1980-02-01 1980-02-01 Manufacturing method of glycidyl ether

Publications (2)

Publication Number Publication Date
JPS56108781A true JPS56108781A (en) 1981-08-28
JPS603392B2 JPS603392B2 (en) 1985-01-28

Family

ID=11769003

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1111580A Expired JPS603392B2 (en) 1980-02-01 1980-02-01 Manufacturing method of glycidyl ether

Country Status (3)

Country Link
JP (1) JPS603392B2 (en)
DE (1) DE3103181A1 (en)
ES (1) ES8201149A1 (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3341366A1 (en) * 1982-11-16 1984-05-17 Kao Corp., Tokyo POLYOLETHER COMPOUND, METHOD FOR PRODUCING THE SAME AND COSMETIC AGENTS WITH A CONTENT THEREOF
WO2017077846A1 (en) * 2015-11-05 2017-05-11 日産化学工業株式会社 Epoxy-based reactive diluent and epoxy resin composition including same
WO2018207735A1 (en) * 2017-05-09 2018-11-15 日産化学株式会社 Method for producing epoxy compound
CN109280038A (en) * 2018-09-17 2019-01-29 大丰跃龙化学有限公司 A kind of synthetic method of Sensiva SC50 ether

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3803213C1 (en) * 1988-02-04 1989-02-23 Th. Goldschmidt Ag, 4300 Essen, De

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6022414B2 (en) * 1978-04-10 1985-06-01 日立マクセル株式会社 magnetic recording medium
JPS54141708A (en) * 1978-04-26 1979-11-05 Osaka Soda Co Ltd Preparation of glycidyl ether

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3341366A1 (en) * 1982-11-16 1984-05-17 Kao Corp., Tokyo POLYOLETHER COMPOUND, METHOD FOR PRODUCING THE SAME AND COSMETIC AGENTS WITH A CONTENT THEREOF
DE3341366C2 (en) * 1982-11-16 1993-03-25 Kao Corp., Tokio/Tokyo, Jp
WO2017077846A1 (en) * 2015-11-05 2017-05-11 日産化学工業株式会社 Epoxy-based reactive diluent and epoxy resin composition including same
WO2018207735A1 (en) * 2017-05-09 2018-11-15 日産化学株式会社 Method for producing epoxy compound
CN110662740A (en) * 2017-05-09 2020-01-07 日产化学株式会社 Method for producing epoxy compound
CN109280038A (en) * 2018-09-17 2019-01-29 大丰跃龙化学有限公司 A kind of synthetic method of Sensiva SC50 ether

Also Published As

Publication number Publication date
JPS603392B2 (en) 1985-01-28
DE3103181A1 (en) 1981-11-26
ES499016A0 (en) 1981-12-01
ES8201149A1 (en) 1981-12-01
DE3103181C2 (en) 1989-10-05

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