JPS54157546A - Preparation of 3-cyclohexenecarboxylic acid - Google Patents

Preparation of 3-cyclohexenecarboxylic acid

Info

Publication number
JPS54157546A
JPS54157546A JP6380078A JP6380078A JPS54157546A JP S54157546 A JPS54157546 A JP S54157546A JP 6380078 A JP6380078 A JP 6380078A JP 6380078 A JP6380078 A JP 6380078A JP S54157546 A JPS54157546 A JP S54157546A
Authority
JP
Japan
Prior art keywords
acrylic acid
preparation
butadiene
catalyst
cyclohexenecarboxylic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP6380078A
Other languages
Japanese (ja)
Inventor
Shinji Takenaka
Kosuke Yamamoto
Takeshi Nishida
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP6380078A priority Critical patent/JPS54157546A/en
Publication of JPS54157546A publication Critical patent/JPS54157546A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE: To prepare the title compound in high yield and high volumetric efficiency, by reacting acrylic acid containing TiCl4 as a catalyst, with 1,3-butadiene.
CONSTITUTION: Acrylic acid and TiCl4 catalyst are dissolved in a solvent such as benzene (1.0W6.5 parts by weight, pref. 3 parts by weight based on 1 part of acrylic acid). 1.3-Butadiene is introduced into the solution at room temperature, and made to react at 50W70°C to afford the objective 3-cyclohexenecarboxylic acid.
COPYRIGHT: (C)1979,JPO&Japio
JP6380078A 1978-05-30 1978-05-30 Preparation of 3-cyclohexenecarboxylic acid Pending JPS54157546A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP6380078A JPS54157546A (en) 1978-05-30 1978-05-30 Preparation of 3-cyclohexenecarboxylic acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6380078A JPS54157546A (en) 1978-05-30 1978-05-30 Preparation of 3-cyclohexenecarboxylic acid

Publications (1)

Publication Number Publication Date
JPS54157546A true JPS54157546A (en) 1979-12-12

Family

ID=13239801

Family Applications (1)

Application Number Title Priority Date Filing Date
JP6380078A Pending JPS54157546A (en) 1978-05-30 1978-05-30 Preparation of 3-cyclohexenecarboxylic acid

Country Status (1)

Country Link
JP (1) JPS54157546A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000046174A1 (en) * 1999-02-05 2000-08-10 Korea Kumho Petrochemical Co., Ltd. A method of preparing cyclohexanecaraboxylic acid using [2+4] diels-alder reaction

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000046174A1 (en) * 1999-02-05 2000-08-10 Korea Kumho Petrochemical Co., Ltd. A method of preparing cyclohexanecaraboxylic acid using [2+4] diels-alder reaction

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