JPH10508637A - 保護用組成物とその製造方法 - Google Patents
保護用組成物とその製造方法Info
- Publication number
- JPH10508637A JPH10508637A JP8515511A JP51551196A JPH10508637A JP H10508637 A JPH10508637 A JP H10508637A JP 8515511 A JP8515511 A JP 8515511A JP 51551196 A JP51551196 A JP 51551196A JP H10508637 A JPH10508637 A JP H10508637A
- Authority
- JP
- Japan
- Prior art keywords
- substrate
- boron
- coating
- mixture
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 180
- 230000001681 protective effect Effects 0.000 title description 12
- 238000004519 manufacturing process Methods 0.000 title description 7
- 229920000642 polymer Polymers 0.000 claims abstract description 69
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 14
- 238000000576 coating method Methods 0.000 claims description 152
- 239000000758 substrate Substances 0.000 claims description 152
- 239000011248 coating agent Substances 0.000 claims description 131
- 238000000034 method Methods 0.000 claims description 98
- 239000000463 material Substances 0.000 claims description 77
- 239000003570 air Substances 0.000 claims description 47
- 229910052580 B4C Inorganic materials 0.000 claims description 41
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 claims description 41
- 229910052751 metal Inorganic materials 0.000 claims description 41
- 239000002184 metal Substances 0.000 claims description 41
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 39
- 229910052796 boron Inorganic materials 0.000 claims description 39
- 239000000919 ceramic Substances 0.000 claims description 36
- 239000000945 filler Substances 0.000 claims description 30
- 239000007800 oxidant agent Substances 0.000 claims description 27
- 238000010438 heat treatment Methods 0.000 claims description 21
- -1 whiskers Substances 0.000 claims description 21
- 239000000843 powder Substances 0.000 claims description 19
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 16
- 229910052760 oxygen Inorganic materials 0.000 claims description 16
- 239000001301 oxygen Substances 0.000 claims description 16
- 239000000835 fiber Substances 0.000 claims description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 13
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- 239000002131 composite material Substances 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 8
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- 239000000126 substance Substances 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
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- 239000006260 foam Substances 0.000 claims description 3
- 239000004005 microsphere Substances 0.000 claims description 3
- BGECDVWSWDRFSP-UHFFFAOYSA-N borazine Chemical compound B1NBNBN1 BGECDVWSWDRFSP-UHFFFAOYSA-N 0.000 claims description 2
- 238000004132 cross linking Methods 0.000 claims description 2
- 229910000765 intermetallic Inorganic materials 0.000 claims description 2
- 150000003254 radicals Chemical class 0.000 claims description 2
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims 1
- KPSZQYZCNSCYGG-UHFFFAOYSA-N [B].[B] Chemical compound [B].[B] KPSZQYZCNSCYGG-UHFFFAOYSA-N 0.000 claims 1
- BRTALTYTFFNPAC-UHFFFAOYSA-N boroxin Chemical compound B1OBOBO1 BRTALTYTFFNPAC-UHFFFAOYSA-N 0.000 claims 1
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 1
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- 239000011707 mineral Substances 0.000 claims 1
- 239000004753 textile Substances 0.000 claims 1
- 230000003647 oxidation Effects 0.000 abstract description 26
- 238000007254 oxidation reaction Methods 0.000 abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 22
- 238000005260 corrosion Methods 0.000 abstract description 19
- 230000007797 corrosion Effects 0.000 abstract description 19
- 239000011253 protective coating Substances 0.000 abstract description 18
- 230000015556 catabolic process Effects 0.000 abstract description 2
- 238000006731 degradation reaction Methods 0.000 abstract description 2
- 239000008199 coating composition Substances 0.000 description 32
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 28
- 229910010271 silicon carbide Inorganic materials 0.000 description 27
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 21
- 229910001928 zirconium oxide Inorganic materials 0.000 description 21
- 239000010410 layer Substances 0.000 description 18
- 239000010935 stainless steel Substances 0.000 description 18
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- 238000005516 engineering process Methods 0.000 description 16
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- 238000006243 chemical reaction Methods 0.000 description 15
- 239000004173 sunset yellow FCF Substances 0.000 description 14
- 239000002904 solvent Substances 0.000 description 13
- 229920001709 polysilazane Polymers 0.000 description 12
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 11
- 239000007789 gas Substances 0.000 description 11
- 229910052749 magnesium Inorganic materials 0.000 description 11
- 239000011777 magnesium Substances 0.000 description 11
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 10
- 229910052710 silicon Inorganic materials 0.000 description 10
- 239000010703 silicon Substances 0.000 description 10
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000011247 coating layer Substances 0.000 description 9
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- 238000002360 preparation method Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 8
- 239000002585 base Substances 0.000 description 8
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- 239000002002 slurry Substances 0.000 description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 7
- 239000012159 carrier gas Substances 0.000 description 7
- 238000005229 chemical vapour deposition Methods 0.000 description 7
- 238000007739 conversion coating Methods 0.000 description 7
- 229910002804 graphite Inorganic materials 0.000 description 7
- 239000010439 graphite Substances 0.000 description 7
- 229910052782 aluminium Inorganic materials 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- 238000005299 abrasion Methods 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 230000004580 weight loss Effects 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 229910052581 Si3N4 Inorganic materials 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 4
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 description 4
- 229910052759 nickel Inorganic materials 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 4
- 239000011343 solid material Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- 229920000049 Carbon (fiber) Polymers 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 3
- UMVBXBACMIOFDO-UHFFFAOYSA-N [N].[Si] Chemical compound [N].[Si] UMVBXBACMIOFDO-UHFFFAOYSA-N 0.000 description 3
- 238000013459 approach Methods 0.000 description 3
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- 150000002739 metals Chemical class 0.000 description 3
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- 239000011541 reaction mixture Substances 0.000 description 3
- ZRBFEDMQRDRUDG-UHFFFAOYSA-N silicon hexaboride Chemical compound B12B3[Si]45B3B2B4B51 ZRBFEDMQRDRUDG-UHFFFAOYSA-N 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 238000010561 standard procedure Methods 0.000 description 3
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- 229910052725 zinc Inorganic materials 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
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- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
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- 229920002396 Polyurea Polymers 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 2
- JXOOCQBAIRXOGG-UHFFFAOYSA-N [B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[Al] Chemical compound [B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[B].[Al] JXOOCQBAIRXOGG-UHFFFAOYSA-N 0.000 description 2
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- 238000000354 decomposition reaction Methods 0.000 description 2
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- 230000002378 acidificating effect Effects 0.000 description 1
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- QDWJUBJKEHXSMT-UHFFFAOYSA-N boranylidynenickel Chemical compound [Ni]#B QDWJUBJKEHXSMT-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
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- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/007—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character containing a dispersed phase, e.g. particles, fibres or flakes, in a continuous phase
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- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
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- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/225—Nitrides
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/42—Coatings containing inorganic materials
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- C04B41/4505—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application
- C04B41/455—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application the coating or impregnating process including a chemical conversion or reaction
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- C04B41/4554—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application the coating or impregnating process including a chemical conversion or reaction the coating or impregnating material being an organic or organo-metallic precursor of an inorganic material
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- C04B41/46—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
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- C04B41/4905—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon
- C04B41/495—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon applied to the substrate as oligomers or polymers
- C04B41/4983—Polycarbosilanes, i.e. polymers with a -Si-C-Si-chain; Polysilazanes, i.e. polymers with a -Si-N-Si-chain; Polysilathianes, i.e. polymers with a -Si-S-Si-chain
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5006—Boron compounds
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5053—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials non-oxide ceramics
- C04B41/5057—Carbides
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
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- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/82—Coating or impregnation with organic materials
- C04B41/84—Compounds having one or more carbon-to-metal of carbon-to-silicon linkages
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- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
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- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/87—Ceramics
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/60—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which all the silicon atoms are connected by linkages other than oxygen atoms
- C08G77/62—Nitrogen atoms
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/16—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers in which all the silicon atoms are connected by linkages other than oxygen atoms
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/28—Other inorganic materials
- C03C2217/281—Nitrides
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/28—Other inorganic materials
- C03C2217/283—Borides, phosphides
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/40—Coatings comprising at least one inhomogeneous layer
- C03C2217/43—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase
- C03C2217/44—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase characterized by the composition of the continuous phase
- C03C2217/45—Inorganic continuous phases
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- C03C2217/00—Coatings on glass
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- C03C2217/46—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase characterized by the dispersed phase
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Abstract
Description
Claims (1)
- 【特許請求の範囲】 1.1)少なくとも1種のホウ素源物質と、金属−窒素結合を有する少なくとも 1種のポリマーを混合して混合物を作成し、 2)少なくとも1つの基材の少なくとも一部の上にその混合物を施し、 3)その上にその混合物を有するその少なくとも1つの基材を加熱し、その 混合物を反応させ、その少なくとも1つの基材の少なくとも一部の上にコーティ ングを形成する、 各工程を含む少なくとも1つの基材の上にコーティングを形成する方法。 2.1)広範囲のホウ素−ホウ素結合の連結を有する少なくとも1種のホウ素源 物質と、少なくともある金属−窒素結合を有する少なくとも1種のポリマーを混 合して混合物を作成し、 2)少なくとも1つの基材の少なくとも一部の上にその混合物を施し、 3)少なくとも1種の酸化剤の存在中で、その上にその混合物を有するその 少なくとも1つの基材を加熱し、そのコーティングを形成する、 各工程を含む少なくとも1つの基材の少なくとも一部の上にコーティングを形成 する方法。 3.その加熱を、少なくとも1種の酸化剤の存在中で行う請求項1に記載の方 法。 4.その少なくとも1つの基材の少なくとも一部の上にコーティングを施す仕 方が、塗布、噴霧、及び浸漬からなる群より選択された仕方である請求項2に記 載の方法。 5.少なくともあるケイ素−窒素結合を有する少なくとも1種の ポリマーが繰り返し構造単位を有し、その繰り返し構造単位の少なくとも約50% がケイ素−窒素結合を含む請求項2に記載の方法。 6.その少なくともあるケイ素−窒素結合を有する少なくとも1種のポリマー が、少なくとも部分的に架橋性である少なくとも1種のポリマーを含む請求項2 に記載の方法。 7.その少なくとも1種のポリマーが、熱と紫外線からなる群より選択された 少なくとも1種のエネルギー形態のエネルギーを与えることによって少なくとも 部分的に架橋される請求項6に記載の方法。 8.その少なくともあるケイ素−窒素結合を有する少なくとも1種のポリマー の架橋を促進するため、その組成物に少なくとも1種のフリーラジカル発生剤が 添加される請求項7に記載の方法。 9.その少なくともあるケイ素−窒素結合を有する少なくとも1種のポリマー が、液体と固体からなる群より選択された少なくとも1種のポリマーである請求 項2に記載の方法。 10.そのケイ素−窒素結合を有する少なくとも1種のポリマーが、ポリシラ ザン、ポリユリアシラザン、及びポリチオユリアシラザンからなる群より選択さ れた少なくとも1種のポリマーを含む請求項2に記載の方法。 11.その少なくとも1種のホウ素源物質が、広範囲のホウ素−ホウ素結合の 連結を有する請求項1に記載の方法。 12.その広範囲のホウ素−ホウ素結合を有するホウ素源が、鎖構造、シート 構造、及びかご構造からなる群より選択された少なくとも1種の構造を有する請 求項2に記載の方法。 13.その少なくとも1種のホウ素源が炭化ホウ素を含む請求項2に記載の方 法。 14.その少なくとも1種の酸化剤が、固体酸化剤、液体酸化剤 、及び気相酸化剤からなる群より選択された少なくとも1種の相を有する請求項 2に記載の方法。 15.その少なくとも1種の酸化剤が、酸素、空気、酸素と少なくとも1種の 不活性雰囲気の混合物、及び酸化性雰囲気からなる群より選択された少なくとも 1種の雰囲気を形成する請求項2に記載の方法。 16.その少なくとも1種の酸化剤が、水蒸気と水蒸気含有空気の少なくとも 1種を含む請求項2に記載の方法。 17.その加熱が少なくとも250℃の温度で行われる請求項2に記載の方法。 18.その加熱が約400℃〜約800℃の温度で行われる請求項2に記載の方法。 19.その少なくとも1つの基材が、金属、金属合金、金属マトリックス複合 材料、金属間化合物、鉱物、炭素、無機と有機のオリゴマーとポリマー、混成ポ リマー、ガラス、セラミック、セラミック複合材料からなる群より選択された少 なくとも1種の材料を含む請求項2に記載の方法。 20.その少なくとも1つの基材が、一体物、粒子、連続繊維、ヤーン、トウ 、細断繊維、ウィスカー、繊維マット、及び三次元の織物構造体からなる群より 選択された少なくとも1種の形状を有する請求項2に記載の方法。 21.そのコーティングがさらに少なくとも1種のフィラー材料を含む請求項 2に記載の方法。 22.そのフィラー材料が、セラミック、ガラス、金属、金属合金、無機と有 機のオリゴマーとポリマー、及び混成ポリマーからなる群より選択された少なく とも1種の材料を含む請求項21に記載の方法。 23.そのフィラー材料が、粉末、フレーク、板状体、球、マイクロスフェア ー、ウィスカー、気泡体、連続繊維、ヤーン、トウ、細断繊維、繊維マット、及 び三次元の織物構造体からなる群より選択された少なくとも1種の形状を有する 請求項21に記載の方法。 24.その基材が、その混合物をその基材に施す前に室温より高い温度に加熱 される請求項2に記載の方法。 25.その基材が、その混合物をその基材に施す前に約100℃より高い温度に 加熱される請求項2に記載の方法。 26.広範囲のホウ素−ホウ素結合を有する少なくとも1種のホウ素源と、少 なくともあるケイ素−窒素結合を有する少なくとも1種のポリマーを含む混合物 を、少なくとも1種の酸化剤の存在中で加熱することを含む方法によって製造さ れた組成物。 27.1)広範囲のホウ素−ホウ素結合の連結を有する少なくとも1種のホウ素 源物質と、少なくともあるケイ素−窒素結合を有する少なくとも1種のポリマー を混合して第1混合物を作成し、 2)その第1混合物を、少なくとも1つの基材の少なくとも一部の上に施 してその少なくとも1つの基材の上に第1層を形成し、 3)広範囲のホウ素−ホウ素結合の連結を有する少なくとも1種の第2の ホウ素源物質と、少なくともあるケイ素−窒素結合を有する少なくとも1種の第 2ポリマーを混合して少なくとも1種の追加混合物を作成し、 4)その少なくとも1種の第2混合物を、その第1層の少なくとも一部の 上に施し、その少なくとも1つの基材の上に少なくとも1つの追加層を作成し、 5)少なくとも1種の酸化剤の存在中で、その第1層とその少なくとも1 つの追加層を有する少なくとも1つの基材を加熱して そのコーティングを形成させる、 各工程を含む、少なくとも1つの基材の上に第1層と少なくとも1つの追加層を 有するコーティングを形成する方法。 28.その少なくとも1つの追加層を少なくとも施す前に、少なくとも1種の 酸化剤の存在中でその基材を加熱する請求項27に記載の方法。 29.その第1層と、その少なくとも1つの追加層の少なくとも1つが、互い に実質的に異なる組成を有する請求項27に記載の方法。 30.その第1層とその少なくとも1つの追加層の少なくとも1つが少なくと も1種のフィラーを更に含む請求項27に記載の方法。 31.(1)広範囲のホウ素−ホウ素結合の連結を有する少なくとも1種のホウ 素源を含む少なくとも1種の成分、 (2)少なくとも2つのケイ素−窒素結合を有する少なくとも1種の成分 、 (2)酸素を含む少なくとも1種の成分、 を含んでなる組成物。 32.少なくとも1種のフィラー材料をさらに含む請求項31に記載の組成物 。 33.その少なくとも1種のフィラー材料が、セラミック、ガラス、金属合金 、無機と有機のオリゴマーとポリマー、及び混成ポリマーからなる群より選択さ れた少なくとも1種の材料を含む請求項32に記載の組成物。 34.その少なくとも1種のフィラー材料が、粉末、フレーク、板状体、球、 マイクロスフェアー、ウィスカー、気泡体、連続繊維、ヤーン、トウ、細断繊維 、繊維マット、及び三次元の織物構造体 からなる群より選択された少なくとも1種の形状を有する請求項32に記載の組 成物。 35.その少なくとも1種のホウ素源物質がホウ酸塩以外のホウ素源物質を含 む請求項1に記載の方法。 36.その少なくとも1種のホウ素源物質がボラジン以外のホウ素源物質を含 む請求項1に記載の方法。 37.その少なくとも1種のホウ素源物質がボロキシン以外のホウ素源物質を 含む請求項1に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US08/335,536 | 1994-11-07 | ||
US08/335,536 US5558908A (en) | 1994-11-07 | 1994-11-07 | Protective compositions and methods of making same |
PCT/US1995/014566 WO1996014353A1 (en) | 1994-11-07 | 1995-11-07 | Protective compositions and methods of making same |
Publications (1)
Publication Number | Publication Date |
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JPH10508637A true JPH10508637A (ja) | 1998-08-25 |
Family
ID=23312188
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP8515511A Ceased JPH10508637A (ja) | 1994-11-07 | 1995-11-07 | 保護用組成物とその製造方法 |
Country Status (6)
Country | Link |
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US (3) | US5558908A (ja) |
EP (1) | EP0791029B1 (ja) |
JP (1) | JPH10508637A (ja) |
CA (1) | CA2199804A1 (ja) |
DE (1) | DE69531552T2 (ja) |
WO (1) | WO1996014353A1 (ja) |
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1994
- 1994-11-07 US US08/335,536 patent/US5558908A/en not_active Expired - Lifetime
-
1995
- 1995-11-07 JP JP8515511A patent/JPH10508637A/ja not_active Ceased
- 1995-11-07 DE DE69531552T patent/DE69531552T2/de not_active Expired - Fee Related
- 1995-11-07 CA CA002199804A patent/CA2199804A1/en not_active Abandoned
- 1995-11-07 EP EP95939857A patent/EP0791029B1/en not_active Expired - Lifetime
- 1995-11-07 WO PCT/US1995/014566 patent/WO1996014353A1/en active IP Right Grant
-
1997
- 1997-10-29 US US08/960,613 patent/US5843526A/en not_active Expired - Lifetime
-
1998
- 1998-11-30 US US09/201,432 patent/US6165551A/en not_active Expired - Lifetime
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006503969A (ja) * | 2002-08-20 | 2006-02-02 | ザ リージェンツ オブ ザ ユニヴァーシティ オブ コロラド | ポリマー誘導セラミック材料 |
JP2013534900A (ja) * | 2010-07-01 | 2013-09-09 | エスゲーエル カーボン ソシエタス ヨーロピア | 蒸気発生を伴うHCl合成装置 |
WO2016047500A1 (ja) * | 2014-09-25 | 2016-03-31 | 東洋アルミニウム株式会社 | コンクリート成形用型枠、それにより成形されたコンクリート成形体、コンクリート成形体を用いたコンクリート構造体、コンクリート成形体の製造方法ならびにコンクリート構造体の製造方法 |
CN106457606A (zh) * | 2014-09-25 | 2017-02-22 | 东洋铝株式会社 | 混凝土成形用框架、利用其成形而成的混凝土成形体、使用了混凝土成形体的混凝土结构物、混凝土成形体的制造方法以及混凝土结构物的制造方法 |
JP2020097225A (ja) * | 2018-10-25 | 2020-06-25 | ザ・ボーイング・カンパニーThe Boeing Company | ポリシラザン及び炭素繊維強化ポリマーの積層板 |
Also Published As
Publication number | Publication date |
---|---|
EP0791029B1 (en) | 2003-08-20 |
EP0791029A1 (en) | 1997-08-27 |
US5558908A (en) | 1996-09-24 |
DE69531552T2 (de) | 2004-06-17 |
DE69531552D1 (de) | 2003-09-25 |
US5843526A (en) | 1998-12-01 |
US6165551A (en) | 2000-12-26 |
CA2199804A1 (en) | 1996-05-17 |
WO1996014353A1 (en) | 1996-05-17 |
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