JPH0674389B2 - Lubricating coating composition - Google Patents

Lubricating coating composition

Info

Publication number
JPH0674389B2
JPH0674389B2 JP63311216A JP31121688A JPH0674389B2 JP H0674389 B2 JPH0674389 B2 JP H0674389B2 JP 63311216 A JP63311216 A JP 63311216A JP 31121688 A JP31121688 A JP 31121688A JP H0674389 B2 JPH0674389 B2 JP H0674389B2
Authority
JP
Japan
Prior art keywords
weight
friction coefficient
coating composition
parts
friction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP63311216A
Other languages
Japanese (ja)
Other versions
JPH02155958A (en
Inventor
欣之 廣川
伊三男 外村
博文 道岡
良雄 不破
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Takata Corp
Toyota Motor Corp
Original Assignee
Takata Corp
Toyota Motor Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takata Corp, Toyota Motor Corp filed Critical Takata Corp
Priority to JP63311216A priority Critical patent/JPH0674389B2/en
Priority to DE8989122596T priority patent/DE68902305T2/en
Priority to EP89122596A priority patent/EP0372559B1/en
Publication of JPH02155958A publication Critical patent/JPH02155958A/en
Priority to US08/246,398 priority patent/US5427698A/en
Publication of JPH0674389B2 publication Critical patent/JPH0674389B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
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    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
    • C10M103/02—Carbon; Graphite
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    • C10M103/06—Metal compounds
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    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/56—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing nitrogen
    • C10M105/70—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing nitrogen as ring hetero atom
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    • C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
    • C10M107/02—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation
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    • C10M107/20—Lubricating compositions characterised by the base-material being a macromolecular compound containing oxygen
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    • C10M107/20—Lubricating compositions characterised by the base-material being a macromolecular compound containing oxygen
    • C10M107/30—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M107/32—Condensation polymers of aldehydes or ketones; Polyesters; Polyethers
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    • C10M107/50—Lubricating compositions characterised by the base-material being a macromolecular compound containing silicon
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    • C10M125/26—Compounds containing silicon or boron, e.g. silica, sand
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    • C10M125/26—Compounds containing silicon or boron, e.g. silica, sand
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    • C10M145/40—Polysaccharides, e.g. cellulose
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    • C10M169/04—Mixtures of base-materials and additives
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/0435—Siloxanes with specific structure containing carbon-to-carbon double bonds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/044—Siloxanes with specific structure containing silicon-to-hydrogen bonds
    • C10M2229/0445—Siloxanes with specific structure containing silicon-to-hydrogen bonds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/045—Siloxanes with specific structure containing silicon-to-hydroxyl bonds
    • C10M2229/0455—Siloxanes with specific structure containing silicon-to-hydroxyl bonds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/046—Siloxanes with specific structure containing silicon-oxygen-carbon bonds
    • C10M2229/0465—Siloxanes with specific structure containing silicon-oxygen-carbon bonds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/047—Siloxanes with specific structure containing alkylene oxide groups
    • C10M2229/0475—Siloxanes with specific structure containing alkylene oxide groups used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/048—Siloxanes with specific structure containing carboxyl groups
    • C10M2229/0485—Siloxanes with specific structure containing carboxyl groups used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/0505—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/051—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing halogen
    • C10M2229/0515—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing halogen used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/052—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing nitrogen
    • C10M2229/0525—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing nitrogen used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/053—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing sulfur
    • C10M2229/0535—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing sulfur used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
    • C10M2229/0545—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus used as base material

Description

【発明の詳細な説明】 ［産業上の利用分野］ 本発明は潤滑用被覆組成物に係り、特に適用箇所に必要
な最適の摩擦係数を付与することが可能でしかも摩耗量
を低減することができる潤滑用被覆組成物に関する。TECHNICAL FIELD The present invention relates to a coating composition for lubrication, and in particular, it is possible to give an optimum friction coefficient necessary for an application site and to reduce the amount of wear. To a possible lubricating coating composition.

［従来の技術］ 各種機械装置の摩擦面間には、適当な潤滑剤を供給し、
乾燥摩擦を流体摩擦又は境界摩擦に置き変えることによ
り、焼付き、摩耗の防止を図っている。[Prior Art] An appropriate lubricant is supplied between friction surfaces of various mechanical devices,
By replacing dry friction with fluid friction or boundary friction, seizure and wear are prevented.

従来提供されている潤滑剤のうち、塗料タイプのもの
は、例えば特開昭63−86764号、特開昭55−157664号、
特開昭57−200463号、特公昭55−1314号等に見られるよ
うに、合成樹脂及び固体潤滑剤よりなり、特に次のよう
な性能を目的として製造され、使用されている。Among the lubricants conventionally provided, those of the paint type are, for example, JP-A-63-86764, JP-A-55-157664,
As disclosed in JP-A-57-200463 and JP-B-55-1314, it is composed of a synthetic resin and a solid lubricant, and is manufactured and used especially for the purpose of the following performance.

潤滑性の向上。即ち、摩擦面の摩擦係数の低減、摩
耗量の低減。Improved lubricity. That is, the friction coefficient of the friction surface is reduced and the wear amount is reduced.

かじり防止。 Prevents galling.

耐食性の向上。 Improved corrosion resistance.

ところで、摩擦部材には比較的高い、適度な摩擦係数を
有し、かつ摩耗は低く抑えられることが要求される部材
がある。例えば、ベルトプーリでは、ベルトとベルトプ
ーリとの間で過度に摩擦係数が小さいと、ベルトの滑り
が起こる。また、ボルト、ネジ等はその噛み合せ面間の
摩擦係数が過度に小さいと、緩みが生じ易い。その他、
湿式で使用されるクラッチ板や差動制限デファレンシャ
ルギヤの摩擦板等についても、耐摩耗性と共に比較的高
い摩擦係数が必要とされる。By the way, there is a friction member that has a relatively high coefficient of friction and is required to be kept low in wear. For example, in a belt pulley, when the coefficient of friction between the belt and the belt pulley is too small, the belt slips. Further, bolts, screws and the like are apt to be loosened when the friction coefficient between the meshing surfaces is too small. Other,
A clutch plate used in a wet type, a friction plate of a differential limited differential gear, and the like are required to have wear resistance and a relatively high friction coefficient.

［発明が解決しようとする課題］ このように、適度な比較的高い摩擦係数を必要とし、か
つ、摩耗は低く抑えることが要求される部材に、従来提
供されている潤滑用被覆組成物を塗布使用すると、前述
のの性能のために、摩耗は低く抑えられるが、摩擦係
数が低くなり過ぎる。特に湿式下で用いられるクラッチ
板や、差動制限デファレンシャルギヤ用摩擦板等に従来
の潤滑用被覆組成物を用いた場合には、摺動面間の摩擦
係数が小さくなり過ぎて（摩擦係数μ＝0.05程度）、ト
ルク伝達に必要な摩擦力が得られず、そのため、摩擦板
の枚数の増加や、押しつけ荷重の増加によって、必要な
摩擦力を得なければならないという不具合があった。[Problems to be Solved by the Invention] As described above, the conventionally provided lubricating coating composition is applied to a member that requires a moderately high friction coefficient and that requires low wear. When used, wear is kept low due to the aforementioned performance, but the coefficient of friction is too low. In particular, when a conventional lubricating coating composition is used for a clutch plate used under wet conditions, a friction plate for a differential limited differential gear, etc., the friction coefficient between sliding surfaces becomes too small (friction coefficient μ = 0.05), the frictional force necessary for torque transmission cannot be obtained. Therefore, there is a problem that the necessary frictional force must be obtained by increasing the number of friction plates or the pressing load.

本発明は、上記従来の問題点を解決し、摩擦係数を適度
な大きさ（摩擦係数μ＝0.06以上）にすることができ、
かつ、摩耗量を低減することができる潤滑用被覆組成物
を提供することを目的とする。The present invention solves the above-mentioned conventional problems, and can make the friction coefficient an appropriate size (friction coefficient μ = 0.06 or more).
Moreover, it is an object of the present invention to provide a coating composition for lubrication capable of reducing the amount of wear.

［課題を解決するための手段］ 本発明の潤滑用被覆組成物は、合成樹脂及び固体潤滑剤
を含む潤滑用被覆組成物であって、摩擦係数調整剤とし
て炭素繊維を含むことを特徴とする。[Means for Solving the Problems] A lubricating coating composition of the present invention is a lubricating coating composition containing a synthetic resin and a solid lubricant, and contains carbon fibers as a friction coefficient adjusting agent. .

以下に本発明を詳細に説明する。The present invention will be described in detail below.

本発明の潤滑用被覆組成物を構成する成分のうち、合成
樹脂としては、特に制限はなく、加熱硬化型、常温硬化
型及び２液硬化型のいずれであっても良く、また油性、
水性を問わない。Of the components constituting the lubricating coating composition of the present invention, the synthetic resin is not particularly limited, and may be any of a heat-curable type, a room-temperature curable type, and a two-component curable type.
It does not matter whether it is water-based or not.

具体的には、エポキシ樹脂、フェニル系樹脂、アミノ系
樹脂、ポリエステル・アルキッド系樹脂、ポリウレタン
系樹脂、ビニル系樹脂、ポリアミドイミド系樹脂、シリ
コン系樹脂等を挙げることができる。Specific examples include epoxy resins, phenyl resins, amino resins, polyester / alkyd resins, polyurethane resins, vinyl resins, polyamideimide resins, and silicone resins.

これらの合成樹脂は１種を単独で用いても、２種以上を
組み合わせて用いても良い。特に、本発明においては、
潤滑剤塗膜の密着性、耐食性、耐油性等に優れることか
ら、エポキシ樹脂とアミノ系樹脂との併用が好ましい。
この場合、エポキシ樹脂とアミノ系樹脂との配合割合
は、エポキシ樹脂100重量部に対して、アミノ系樹脂20
〜100重量部程度とすることが好適である。These synthetic resins may be used alone or in combination of two or more. In particular, in the present invention,
It is preferable to use the epoxy resin and the amino resin in combination because the lubricant coating film has excellent adhesion, corrosion resistance, oil resistance and the like.
In this case, the mixing ratio of the epoxy resin and the amino resin is 20 parts by weight of the amino resin with respect to 100 parts by weight of the epoxy resin.
It is preferably about 100 parts by weight.

このような合成樹脂の配合割合は、調製される潤滑剤に
対して20〜80重量％、特に30〜60重量％であることが好
ましい。合成樹脂の配合割合が20重量％未満では潤滑剤
塗膜の密着製、耐食性、耐油性等において十分な特性が
得られず、80重量％を超えると摩擦係数の制御が難しく
なる。The blending ratio of such a synthetic resin is preferably 20 to 80% by weight, particularly 30 to 60% by weight, based on the prepared lubricant. When the compounding ratio of the synthetic resin is less than 20% by weight, sufficient properties such as adhesion of the lubricant coating film, corrosion resistance and oil resistance cannot be obtained, and when it exceeds 80% by weight, it becomes difficult to control the friction coefficient.

また、固体潤滑剤としても特に制限はなく、二硫化モリ
ブデン、二硫化タングステン等の硫化物；ポリテトラフ
ルオロエチレン、フッ化黒鉛等のフッ素化合物；黒鉛；
メラミン−シアヌル酸付加物；窒化ホウ素等を用いるこ
とができる。これらの固体潤滑剤は１種を単独で用いて
も、２種以上を組み合わせて用いても良い。特に、本発
明においては、耐荷重性、なじみ性、フィーリング性に
優れることから、硫化物とフッ素化合物との併用が好ま
しい。この場合、硫化物とフッ素化合物との配合割合
は、硫化物100重量部に対してフッ素化合物50〜200重量
部程度とするのが好適である。The solid lubricant is also not particularly limited, and sulfides such as molybdenum disulfide and tungsten disulfide; fluorine compounds such as polytetrafluoroethylene and fluorinated graphite; graphite;
Melamine-cyanuric acid adduct; boron nitride or the like can be used. These solid lubricants may be used alone or in combination of two or more. In particular, in the present invention, it is preferable to use a sulfide and a fluorine compound in combination because they are excellent in load resistance, conformability and feeling. In this case, the mixing ratio of the sulfide and the fluorine compound is preferably about 50 to 200 parts by weight of the fluorine compound with respect to 100 parts by weight of the sulfide.

このような固体潤滑剤の配合割合は、調製される潤滑用
被覆組成物に対して20〜80重量％、特に30〜60重量％で
あることが好ましい。固体潤滑剤の配合割合が20重量％
未満では、耐荷重性、なじみ性、フィーリング性等にお
いて十分な特性が得られず、80重量％を超えると潤滑塗
膜の密着性、耐食性、耐油性が低下する。The blending ratio of such a solid lubricant is preferably 20 to 80% by weight, and particularly preferably 30 to 60% by weight, based on the prepared lubricating coating composition. 20% by weight of solid lubricant
If it is less than 80% by weight, sufficient properties such as load resistance, conformability and feeling are not obtained, and if it exceeds 80% by weight, the adhesion, corrosion resistance and oil resistance of the lubricating coating are deteriorated.

本発明において、摩擦係数調整剤としては、摩擦係数の
調整機能が高くしかも耐摩耗性の向上に有効であること
から、炭素繊維を用いる。摩擦係数調整剤としては炭素
繊維のみでも良く、炭素繊維と、カーボンブラック；二
酸化ケイ素、炭化ケイ素、チッ化ケイ素、ガラス繊維等
のケイ素化合物；酸化アルミニウム；チタン酸カリウム
繊維；セルロース系繊維等の１種又は２種以上とを組み
合わせて用いても良い。In the present invention, carbon fiber is used as the friction coefficient adjusting agent because it has a high function of adjusting the friction coefficient and is effective in improving wear resistance. As the friction coefficient adjusting agent, only carbon fiber may be used, and carbon fiber and carbon black; silicon compounds such as silicon dioxide, silicon carbide, silicon nitride, glass fiber; aluminum oxide; potassium titanate fiber; cellulosic fiber and the like 1 You may use it in combination of 1 type or 2 or more types.

炭素繊維、その他の摩擦係数調整剤は、繊維状のものに
あっては、その繊維長さが10μｍ〜1m/m、繊維径が10〜
50μｍ程度のものが好適である。また、粒状のものにあ
っては、その粒径が100μｍ以下程度のものが好適であ
る。Carbon fibers and other friction coefficient adjusting agents, if they are fibrous, have a fiber length of 10 μm to 1 m / m and a fiber diameter of 10 to
It is preferably about 50 μm. Further, as the granular material, it is preferable that the particle diameter is about 100 μm or less.

このような炭素繊維のみからなる、又は、炭素繊維を含
む摩擦係数調整剤の配合割合は、調製される潤滑剤に対
して50重量％以下、特に５〜30重量％とするのが好まし
い。摩擦係数調整剤の配合割合が50重量％を超える場合
には、潤滑剤塗膜の密着性、耐食性が低下し、また耐摩
耗性の改善効果も低下する。The blending ratio of such a friction coefficient adjusting agent consisting of carbon fibers alone or containing carbon fibers is preferably 50% by weight or less, and particularly preferably 5 to 30% by weight based on the prepared lubricant. When the blending ratio of the friction coefficient adjusting agent exceeds 50% by weight, the adhesiveness and corrosion resistance of the lubricant coating film decrease, and the effect of improving wear resistance also decreases.

本発明の潤滑用被覆組成物は、例えば、合成樹脂及び固
体潤滑剤を所定の割合で配合し、更にこれに所定量の摩
擦係数調整剤を混合することにより容易に調整すること
ができる。しかも、各成分の配合割合を調整することに
より、摩擦係数を広い範囲で調整することができ、摩耗
量は、低く抑える高性能潤滑剤が提供される。The coating composition for lubrication of the present invention can be easily adjusted by, for example, blending a synthetic resin and a solid lubricant in a predetermined ratio, and further mixing a predetermined amount of a friction coefficient adjusting agent therein. Moreover, by adjusting the blending ratio of each component, the friction coefficient can be adjusted in a wide range, and a high-performance lubricant that suppresses the wear amount is provided.

なお、合成樹脂と、固体潤滑剤を配合する際、及び、各
成分を配合した後において、適量の溶剤を用いることに
より、配合工程を容易にし、かつ、容易に使用できる粘
度に調整することができる。Incidentally, when the synthetic resin and the solid lubricant are blended, and after blending the respective components, by using an appropriate amount of a solvent, the blending process can be facilitated, and the viscosity can be adjusted to be easily usable. it can.

使用する溶剤は、合成樹脂を溶解可能なものであれば特
に制限はなく、使用量も、合成樹脂の粘度、配合比が種
々異なるため、特に制限はないが、組成物100重量部に
対して、溶剤100〜300重量部程度が適量である。また使
用する溶剤は、１種の単独溶剤でも、２種以上の混合溶
剤でも良い。The solvent to be used is not particularly limited as long as it can dissolve the synthetic resin, the amount used, the viscosity of the synthetic resin, since the compounding ratio is different, there is no particular limitation, relative to 100 parts by weight of the composition. An appropriate amount is about 100 to 300 parts by weight of the solvent. The solvent used may be a single solvent or a mixture of two or more solvents.

さらに、本発明の潤滑剤は、上記３成分の他に、必要に
応じて各種改質剤等の添加剤を含有していても良い。こ
の場合、添加剤配合量は調製される潤滑剤に対して20重
量％以下とする。Furthermore, the lubricant of the present invention may contain additives such as various modifiers, if necessary, in addition to the above three components. In this case, the additive content is 20% by weight or less based on the prepared lubricant.

［作用］ 本発明の潤滑用被覆組成物は、固体潤滑剤により優れた
潤滑性が付与され、一方、炭素繊維のみからなる、又
は、炭素繊維を含む摩擦係数調整剤より、この潤滑性能
が調整され、耐摩耗性を損なうことなく、摩擦係数が所
望とする適度な値にされる。[Operation] In the coating composition for lubrication of the present invention, excellent lubricity is imparted to the solid lubricant, while the lubricating performance is adjusted by the friction coefficient adjusting agent which is made of only carbon fiber or contains carbon fiber. Therefore, the friction coefficient is set to a desired moderate value without impairing the wear resistance.

［実施例］ 以下、実施例及び比較例を挙げて本発明をより具体的に
説明するが、本発明はその要旨を超えない限り、以下の
実施例に限定されるものではない。[Examples] Hereinafter, the present invention will be described more specifically with reference to Examples and Comparative Examples, but the present invention is not limited to the following Examples unless it exceeds the gist.

実施例１〜15,比較例１〜６ 第１表に示す原料を用いて第２表中の配合にて、潤滑用
被覆組成物を調整し、製造する。Examples 1 to 15 and Comparative Examples 1 to 6 Using the raw materials shown in Table 1, the lubricating coating compositions were prepared according to the formulations shown in Table 2 and manufactured.

具体的には、合成樹脂を100重量部に対して、100〜200
重量部の溶剤（Ｍ・Ｅ・K,キシレン等）で溶解したもの
に、固体潤滑剤を加え、ボールミルにて３時間粉砕を行
なう。それに対し、所定量の摩擦係数調整剤を加え撹拌
を行なったものを試料とする。Specifically, 100 to 200 parts by weight of synthetic resin
A solid lubricant is added to what is dissolved in parts by weight of a solvent (ME, K, xylene, etc.), and the mixture is pulverized with a ball mill for 3 hours. On the other hand, a sample is prepared by adding a predetermined amount of friction coefficient adjusting agent and stirring.

ただし、第２表において、※１〜※３は下記の通りであ
る。However, in Table 2, * 1 to * 3 are as follows.

※１ A:200℃,30分加熱 B:常 温,4時間 C:常 温,1時間（２液） D:250℃,1時間加熱 ※２ EP＋AM:エポキシ樹脂100重量部＋アミノ系樹脂80重量部 VI＋AM:ビニル系樹脂100重量部＋アミノ系樹脂100重量
部 PU:ポリウレタン系樹脂 EP:エポキシ樹脂 EP＋PH:エポキシ樹脂100重量部＋フェニル系樹脂80重量
部 AM＋ES:アミノ系樹脂100重量部＋ポリエステル・アルキ
ッド樹脂80重量部 PAMIM:ポリアミドイミド樹脂 SI:シリコン系樹脂 ※３ I:二硫化モリブデン100重量部＋ポリテトラフルオロエ
チレン100重量部 II:二硫化モリブデン100重量部＋ポリテトラフルオロエ
チレン70重量部＋黒鉛30重量部 III:二硫化モリブデン100重量部＋メラミン−シアヌル
酸付加物100重量部 IV:窒化ホウ素100重量部＋ポリテトラフルオロエチレン
100重量部 各試料の摩擦係数及び摩耗量の改善効果を下記方法によ
り調べ、その結果を第２表に示す。* 1 A: 200 ° C, 30 minutes heating B: Normal temperature, 4 hours C: Normal temperature, 1 hour (2 solutions) D: 250 ° C, 1 hour heating * 2 EP + AM: Epoxy resin 100 parts by weight + Amino resin 80 Parts by weight VI + AM: 100 parts by weight of vinyl resin + 100 parts by weight of amino resin PU: Polyurethane resin EP: Epoxy resin EP + PH: 100 parts by weight of epoxy resin + 80 parts by weight of phenyl resin AM + ES: 100 parts by weight of amino resin + polyester・ Alkyd resin 80 parts by weight PAMIM: Polyamideimide resin SI: Silicon resin * 3 I: 100 parts by weight of molybdenum disulfide + 100 parts by weight of polytetrafluoroethylene II: 100 parts by weight of molybdenum disulfide + 70 parts by weight of polytetrafluoroethylene + 30 parts by weight of graphite III: 100 parts by weight of molybdenum disulfide + 100 parts by weight of melamine-cyanuric acid adduct IV: 100 parts by weight of boron nitride + polytetrafluoroethylene
100 parts by weight The effect of improving the friction coefficient and the wear amount of each sample was examined by the following method, and the results are shown in Table 2.

摩擦係数の測定 下記の試験機、テストピース、テスト条件にて行なっ
た。即ち、一定速度で回転するリングにブロックを一定
の荷重で押し付け、両テストピース間の摩擦係数を測定
した。なお、ブロック及びリングの当接面にはそれぞれ
リン酸亜鉛皮膜処理等の下地処理を行った上、エアスプ
レーにて約20μｍの塗膜厚になるように吹き付け、その
後各硬化条件にて硬化させて塗膜を形成した。Measurement of friction coefficient The friction coefficient was measured under the following tester, test piece, and test conditions. That is, the block was pressed against a ring rotating at a constant speed with a constant load, and the coefficient of friction between both test pieces was measured. The abutting surfaces of the block and ring are each subjected to a surface treatment, such as a zinc phosphate coating, and then sprayed with an air sprayer to a coating thickness of about 20 μm, and then cured under each curing condition. To form a coating film.

また、リングの非当接面側は差動制限デファレンシャル
ギヤ用オイル（鉱物油）に浸漬した状態と、浸漬しない
状態とにした。The non-contact surface side of the ring was immersed in the oil for differential limited differential gear (mineral oil) and was not immersed.

試験機 FALEX＃1, Ring ＆ Block TEST MACHINE［Faville−Le Vally社製
（ASTM D 2714）］ テストピース リング:SAE4620 STEEL, HRc58〜63,6〜12rms ブロック:SAEO−1STEEL, HRc58〜63,4〜8rms テスト条件 荷 重:100lЕbs 回転速度:30rpm 摩耗量の測定 鋼製プレートの表面にの摩擦係数の測定の時と同様な
方法により各々の潤滑用被覆組成物を塗布した摩擦板Ａ
と、鋼製（材質:JIS規格SK5M）で、焼入れ焼戻しを施し
た鋼板（硬度HV460）よりなりその表面粗さが0.5μRaの
摩擦板Ｂ（外径120mm,内径100mm,厚さ1.8mm）を組み合
わせて、スラスト試験機により摩擦試験を行なった。Tester FALEX # 1, Ring & Block TEST MACHINE [Faville-Le Vally (ASTM D 2714)] Test Piece Ring: SAE4620 STEEL, HRc58 ~ 63, 6 ~ 12rms Block: SAEO-1STEEL, HRc58 ~ 63, 4 ~ 8 rms test conditions Load: 100 lЕbs Rotation speed: 30 rpm Measurement of wear amount Friction plate A coated with each lubricating coating composition by the same method as when measuring the friction coefficient on the surface of a steel plate
And a friction plate B (outer diameter 120 mm, inner diameter 100 mm, thickness 1.8 mm) made of steel (material: JIS standard SK5M) and made of quenched and tempered steel plate (hardness HV460) with a surface roughness of 0.5 μRa. In combination, a friction test was conducted with a thrust tester.

即ち、差動制限デファレンシャルギヤ用オイル中で約50
rpmにて回転している摩擦板Ｂに対し、摩擦板Ａを荷重5
00kgfで押しつけ、200時間後の摩耗量（摩耗深さ）を調
べた。That is, about 50 in the oil for differential limited differential gears.
The friction plate A is loaded against the friction plate B rotating at 5 rpm.
The amount of wear (wear depth) after 200 hours was examined by pressing with 00 kgf.

第２表より明らかなように、本発明の潤滑用被覆組成物
は、摩擦係数が従来品（比較例１）に比べて高く、しか
もその値を広い範囲で調整することができる。一方、摩
耗量は著しく少ない。これに対し、従来品（比較例１）
では、摩擦係数が低過ぎる上に、摩耗量が大きい。As is clear from Table 2, the coating composition for lubrication of the present invention has a higher friction coefficient than that of the conventional product (Comparative Example 1), and the value can be adjusted in a wide range. On the other hand, the amount of wear is extremely small. In contrast, conventional products (Comparative example 1)
Then, the friction coefficient is too low and the wear amount is large.

なお、この比較例１の場合には塗膜が摩滅して一部下地
が露出していたのに対し、本発明品の場合は、いずれも
塗膜はほぼ完全に残っていた。In the case of Comparative Example 1, the coating film was abraded and a part of the undercoat was exposed, whereas in the case of the products of the present invention, the coating film was almost completely left.

更に、本発明の潤滑用被覆組成物を用いた場合、試験方
法で示すスラスト試験機での試験において、μｓ（静
摩擦係数）がμｄ（動摩擦係数）よりも常に低くなり、
スティックスリップ現象による異音の発生を抑制するの
にも効果があることがわかった。それに対し、従来品
（比較例１）では、μｓとμｄがほぼ同等かμｓよりμ
ｄがやや低い傾向を示し、しかも耐摩耗性が不足してい
るため、試験中下地が露出することから、スティックス
リップ現象による異音が発生した。Further, when the lubricating coating composition of the present invention is used, in the test using the thrust tester shown in the test method, μs (static friction coefficient) is always lower than μd (dynamic friction coefficient),
It was also found to be effective in suppressing the generation of abnormal noise due to the stick-slip phenomenon. On the other hand, in the conventional product (Comparative Example 1), μs and μd are almost equal to each other.
Since d showed a slightly low tendency and the abrasion resistance was insufficient, the underlayer was exposed during the test, and abnormal noise was generated due to the stick-slip phenomenon.

比較例，実施例中の各組成物の商標名及びメーカー名を
第１表に示すが、今回の試験に用いた原料であり、実使
用についてはこの限りでない。Table 1 shows the brand name and manufacturer name of each composition in Comparative Examples and Examples, but these are the raw materials used in the test this time, and the actual use is not limited to this.

［発明の効果］ 以上詳述した通り、本発明の潤滑用被覆組成物によれ
ば、摩擦係数を比較的高い値にまで所望に応じて制御す
ることができ、しかも摩耗量は大幅に低減することがで
きる。 [Effects of the Invention] As described in detail above, according to the coating composition for lubrication of the present invention, the friction coefficient can be controlled to a relatively high value as desired, and the amount of wear is greatly reduced. be able to.

従って、本発明の潤滑用被覆組成物によれば油中で用い
られる差動制限デファレンシャルギヤや、クラッチ板及
びプーリー等の、トルクの伝達が確実に行なわれるため
の適度に高い摩擦係数を必要とし、かつ摩耗量は低く抑
えることが必要とされる部材、及びボルト等の緩みが生
じにくい程度の適度に高い摩擦係数を必要とする部材の
摺動性能、摩擦性能、潤滑性能を大幅に向上させること
ができる。Therefore, according to the lubricating coating composition of the present invention, a moderately high friction coefficient for reliably transmitting torque, such as a differential limited differential gear used in oil, a clutch plate and a pulley, is required. In addition, the sliding performance, friction performance, and lubrication performance of a member that requires a low wear amount and a member that requires a moderately high friction coefficient such that bolts are unlikely to come loose are significantly improved. be able to.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 不破 良雄 愛知県豊田市トヨタ町１番地 トヨタ自動 車株式会社内 (56)参考文献 特開 昭49−30421（ＪＰ，Ａ) 特開 昭51−67332（ＪＰ，Ａ) 特開 昭50−10380（ＪＰ，Ａ) 実開 昭63−22266（ＪＰ，Ｕ) 実開 昭56−164819（ＪＰ，Ｕ) ─────────────────────────────────────────────────── ─── Continuation of front page (72) Inventor Yoshio Fuwa 1 Toyota Town, Toyota City, Aichi Prefecture Toyota Automobile Co., Ltd. (56) Reference JP-A-49-30421 (JP, A) JP-A-51-67332 (JP, A) JP-A-50-10380 (JP, A) Actually opened 63-22266 (JP, U) Actually opened 56-164819 (JP, U)

Claims (1)

【特許請求の範囲】[Claims] 【請求項１】合成樹脂及び固体潤滑剤を含む潤滑用被覆
組成物であって、摩擦係数調整剤として炭素繊維を含む
ことを特徴とする潤滑用被覆組成物。1. A lubricating coating composition containing a synthetic resin and a solid lubricant, wherein the lubricating coating composition contains carbon fibers as a friction coefficient adjusting agent.
JP63311216A 1988-12-09 1988-12-09 Lubricating coating composition Expired - Fee Related JPH0674389B2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP63311216A JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition
DE8989122596T DE68902305T2 (en) 1988-12-09 1989-12-07 LUBRICATION COMPOSITION.
EP89122596A EP0372559B1 (en) 1988-12-09 1989-12-07 Coating composition for lubrication
US08/246,398 US5427698A (en) 1988-12-09 1994-05-18 Coating composition for lubrication

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP63311216A JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition

Publications (2)

Publication Number Publication Date
JPH02155958A JPH02155958A (en) 1990-06-15
JPH0674389B2 true JPH0674389B2 (en) 1994-09-21

Family

ID=18014498

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JP63311216A Expired - Fee Related JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition

Country Status (3)

Country Link
EP (1) EP0372559B1 (en)
JP (1) JPH0674389B2 (en)
DE (1) DE68902305T2 (en)

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Also Published As

Publication number Publication date
JPH02155958A (en) 1990-06-15
EP0372559A1 (en) 1990-06-13
EP0372559B1 (en) 1992-07-29
DE68902305D1 (en) 1992-09-03
DE68902305T2 (en) 1992-12-10

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