JPH02155958A - Lubricating coating composition - Google Patents

Lubricating coating composition

Info

Publication number
JPH02155958A
JPH02155958A JP63311216A JP31121688A JPH02155958A JP H02155958 A JPH02155958 A JP H02155958A JP 63311216 A JP63311216 A JP 63311216A JP 31121688 A JP31121688 A JP 31121688A JP H02155958 A JPH02155958 A JP H02155958A
Authority
JP
Japan
Prior art keywords
friction
coefficient
coating composition
lubricating coating
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP63311216A
Other languages
Japanese (ja)
Other versions
JPH0674389B2 (en
Inventor
Yoshiyuki Hirokawa
廣川　欣之
Isao Tonomura
外村　伊三男
Hirobumi Michioka
博文 道岡
Yoshio Fuwa
良雄 不破
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Takata Corp
Toyota Motor Corp
Original Assignee
Takata Corp
Toyota Motor Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takata Corp, Toyota Motor Corp filed Critical Takata Corp
Priority to JP63311216A priority Critical patent/JPH0674389B2/en
Priority to DE8989122596T priority patent/DE68902305T2/en
Priority to EP89122596A priority patent/EP0372559B1/en
Publication of JPH02155958A publication Critical patent/JPH02155958A/en
Priority to US08/246,398 priority patent/US5427698A/en
Publication of JPH0674389B2 publication Critical patent/JPH0674389B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
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    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
    • C10M103/02—Carbon; Graphite
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    • C10M103/06—Metal compounds
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    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/56—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing nitrogen
    • C10M105/70—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing nitrogen as ring hetero atom
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    • C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
    • C10M107/02—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation
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    • C10M107/20—Lubricating compositions characterised by the base-material being a macromolecular compound containing oxygen
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    • C10M107/30—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M107/32—Condensation polymers of aldehydes or ketones; Polyesters; Polyethers
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    • C10M145/40—Polysaccharides, e.g. cellulose
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    • C10M2229/04—Siloxanes with specific structure
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    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
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    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/0455—Siloxanes with specific structure containing silicon-to-hydroxyl bonds used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/046—Siloxanes with specific structure containing silicon-oxygen-carbon bonds
    • C10M2229/0465—Siloxanes with specific structure containing silicon-oxygen-carbon bonds used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/047—Siloxanes with specific structure containing alkylene oxide groups
    • C10M2229/0475—Siloxanes with specific structure containing alkylene oxide groups used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/0485—Siloxanes with specific structure containing carboxyl groups used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/04—Siloxanes with specific structure
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    • C10M2229/0515—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing halogen used as base material
    • C—CHEMISTRY; METALLURGY
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    • C10M2229/0525—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing nitrogen used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2229/0535—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing sulfur used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
    • C10M2229/0545—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus used as base material

Abstract

PURPOSE:To obtain the title composition which can give a necessary coefficient of friction to the applied part and can reduce the extent of friction by mixing a synthetic resin with a solid lubricant an a friction coefficient modifier. CONSTITUTION:The title composition is obtained by mixing 20-80wt.% synthetic resin, desirably a mixture of 100pts.wt. epoxy resin with 20-100pts.wt. amino resin, with 20-80wt.% solid lubricant, desirably a mixture of 100pts.wt. sulfide with 50-200pts.wt. fluorine compound, and at most 50wt.% frictional coefficient modifier (e.g. carbon fiber) having a fiber length of 10mum-1mm and a fiber diameter of 10-50m in the case of a fiber and having a particle diameter <=100mum in the case of a particle. This comparison is optionally mixed with 100-300pts.wt., per 100pts.wt. composition, solvent and 20wt.% or below additives such as modifiers.

Description

【発明の詳細な説明】 ［産業上の利用分野］ 本発明は潤滑用被覆組成物に係り、特に適用箇所に必要
な最適の摩擦係数を付与することが可能でしかも摩耗量
を低減することができる潤滑用被覆組成物に関する。[Detailed Description of the Invention] [Industrial Application Field] The present invention relates to a lubricating coating composition, and particularly to a lubricating coating composition that is capable of imparting the optimum coefficient of friction required to the application area and reducing the amount of wear. The present invention relates to a lubricating coating composition that can be used as a lubricating coating composition.

［従来の技術］ 各種機械装置の摩擦面間には、適当な潤滑剤を供給し、
乾燥摩擦を流体摩擦又は境界摩擦に置き変えることによ
り、焼付き、摩耗の防止を図っている。[Prior art] Appropriate lubricant is supplied between the friction surfaces of various mechanical devices,
By replacing dry friction with fluid friction or boundary friction, seizure and wear are prevented.

従来提供されている潤滑剤のうち、塗料タイプのものは
、例えば特開昭６３−８６７６４号、特開昭５５−１５
７６６４号、特開昭５７−２００４６３号、特公昭５５
−１３１４号等に見られるように、合成樹脂及び固体潤
滑剤よりなり、特に次のような性能を目的として製造さ
れ、使用されている。Among the lubricants conventionally provided, paint-type ones are disclosed in, for example, Japanese Patent Application Laid-open No. 63-86764 and Japanese Patent Application Laid-open No. 55-15.
No. 7664, JP-A-57-200463, JP-A-55
As seen in No. 1314, etc., it is made of synthetic resin and solid lubricant, and is manufactured and used specifically for the following performance purposes.

■　潤滑性の向上、即ち、摩擦面の摩擦係数の低減、摩
耗量の低減。■ Improved lubricity, that is, reduced friction coefficient of friction surfaces and reduced amount of wear.

■　かじり防止。■ Prevents galling.

■　耐食性の向上。■ Improved corrosion resistance.

ところで、摩擦部材には比較的高い、適度な摩擦係数を
有し、かつ摩耗は低く抑えられることが要求される部材
がある。例えば、ベルトプーリでは、ベルトとベルトプ
ーリとの間で過度に摩擦係数が小さいと、ベルトの滑り
が起こる。また、ボルト、ネジ等はその噛み合せ面間の
摩擦係数が過度に小さいと、緩みが生じ易い。その他、
湿式で使用されるクラッチ板や差動制限デファレンシャ
ルギヤの摩擦板等についても、耐摩耗性と共に比較的高
い摩擦係数が必要とされる。By the way, some friction members are required to have a relatively high, moderate coefficient of friction, and to suppress wear to a low level. For example, in a belt pulley, if the coefficient of friction between the belt and the belt pulley is too small, the belt will slip. Furthermore, if the coefficient of friction between the mating surfaces of bolts, screws, etc. is too small, they tend to loosen. others,
Clutch plates used in wet systems, friction plates for limited-slip differential gears, etc. are also required to have wear resistance and a relatively high coefficient of friction.

［発明が解決しようとする課題］ このように、適度な比較的高い摩擦係数を必要とし、か
つ、摩耗は低く抑えることが要求される部材に、従来提
供されている潤滑用被覆組成物を塗布使用すると、前述
の■の性能のために、摩耗は低く抑えられるが、摩擦係
数が低くなり過ぎる。特に湿式下で用いられるクラッチ
板や、差動制限デファレンシャルギヤ用摩擦板等に従来
の潤滑用被覆組成物を用いた場合には、摺動面間の摩擦
係数が小さくなり過ぎて（摩擦係数μ＝０．０５程度）
、トルク伝達に必要な摩擦力が得られず、そのため、摩
擦板の枚数の増加や、押しつけ荷重の増加によって、必
要な摩擦力を得なければならないという不具合があった
。[Problems to be Solved by the Invention] As described above, it is possible to apply a conventionally provided lubricating coating composition to a member that requires a relatively high coefficient of friction and low wear. When used, wear can be kept low due to the above-mentioned performance (2), but the friction coefficient becomes too low. In particular, when conventional lubricating coating compositions are used for clutch plates used in wet conditions, friction plates for differential gears, etc., the coefficient of friction between sliding surfaces becomes too small (friction coefficient μ = about 0.05)
However, there was a problem in that the frictional force necessary for torque transmission could not be obtained, and therefore the necessary frictional force had to be obtained by increasing the number of friction plates or increasing the pressing load.

本発明は、上記従来の問題点を解決し、摩擦係数を適度
な大きさ（摩擦係数μ＝０．０６以上）にすることがで
き、かつ、摩耗量を低減することができる潤滑用被覆組
成物を提供することを目的とする。The present invention solves the above-mentioned conventional problems, and provides a lubricating coating composition that can have an appropriate friction coefficient (friction coefficient μ=0.06 or more) and reduce the amount of wear. The purpose is to provide something.

［課題を解決するための手段］ 本発明の潤滑用被覆組成物は、合成樹脂及び固体潤滑剤
を含む潤滑用被覆組成物であって、摩擦係数調整剤を含
むことを特徴とする。[Means for Solving the Problems] The lubricating coating composition of the present invention is a lubricating coating composition containing a synthetic resin and a solid lubricant, and is characterized by containing a friction coefficient modifier.

以下に本発明の詳細な説明する。The present invention will be explained in detail below.

本発明の潤滑用被覆組成物を構成する成分のうち、合成
樹脂としては、特に制限看なく、加熱硬化型、常温硬化
型及び２液硬化型のいずれであっても良（、また油性、
水性を問わない。Among the components constituting the lubricating coating composition of the present invention, the synthetic resin may be of any heat-curing type, room-temperature curing type, or two-component curing type (also oil-based,
Doesn't matter whether it's water-based or not.

具体的には、エポキシ樹脂、フェニル系樹脂、アミノ系
樹脂、ポリエステル・アルキッド系樹脂、ポリウレタン
系樹脂、ビニル系樹脂、ポリアミドイミド系樹脂、シリ
コン系樹脂等を挙げることができる。Specifically, epoxy resins, phenyl resins, amino resins, polyester/alkyd resins, polyurethane resins, vinyl resins, polyamideimide resins, silicone resins, etc. can be mentioned.

これらの合成樹脂は１種を単独で用いても、２種以上を
組み合わせて用いても良い。特に、本発明においては、
潤滑剤塗膜の密着性、耐食性、耐油性等に優れることか
ら、エポキシ樹脂とアミノ系樹脂との併用が好ましい。These synthetic resins may be used alone or in combination of two or more. In particular, in the present invention,
Since the lubricant coating film has excellent adhesion, corrosion resistance, oil resistance, etc., it is preferable to use an epoxy resin and an amino resin in combination.

この場合、エポキシ樹脂とアミノ系樹脂との配合割合は
、エポキシ樹脂１００重量部に対して、アミン系樹脂２
０〜８０重量部程度とするのが好適である。In this case, the blending ratio of the epoxy resin and the amino resin is 2 parts by weight of the amine resin to 100 parts by weight of the epoxy resin.
The amount is preferably about 0 to 80 parts by weight.

このような合成樹脂の配合割合は、調製される潤滑剤に
対して２０〜８０重量％、特に３０〜６０重量％である
ことが好ましい０合成樹脂の配合割合が２０重量％未満
では潤滑剤塗膜の密着性、耐食性、耐油性等において十
分な特性が得られず、８０重量％を超えると摩擦係数の
制御が難しくなる。The blending ratio of such synthetic resin is preferably 20 to 80% by weight, particularly 30 to 60% by weight based on the lubricant to be prepared. If the blending ratio of synthetic resin is less than 20% by weight, the lubricant coating will be difficult. Sufficient properties in film adhesion, corrosion resistance, oil resistance, etc. cannot be obtained, and if it exceeds 80% by weight, it becomes difficult to control the coefficient of friction.

また、固体潤滑剤としても特＆：　１１限はなく。In addition, there are no special restrictions as a solid lubricant.

二硫化モリブデン、二硫化タングステン等の硫化物：ポ
リテトラフルオロエチレン、フッ化黒鉛等のフッ素化合
物：黒鉛：メラミン−シアヌル酸付加物：窒化ホウ素等
を用いることができる。これらの固体潤滑剤は１種を単
独で用いても、２ｆ！以上を組み合わせて用いても良い
。特に、本発明においては、耐荷重性、なじみ性、フィ
ーリング性に優れることから、硫化物とフッ素化合物と
の併用が好ましい。この場合、硫化物とフッ素化合物と
の配合割合は、硫化物１００重量部に対してフッ素化合
物５０〜２００重量部程度とするのが好適である。Sulfides such as molybdenum disulfide and tungsten disulfide; fluorine compounds such as polytetrafluoroethylene and graphite fluoride; graphite; melamine-cyanuric acid adduct; boron nitride, etc. can be used. Even if one of these solid lubricants is used alone, 2f! The above may be used in combination. In particular, in the present invention, it is preferable to use a sulfide and a fluorine compound in combination because they have excellent load resistance, conformability, and feel. In this case, the mixing ratio of the sulfide and the fluorine compound is preferably about 50 to 200 parts by weight per 100 parts by weight of the sulfide.

このような固体潤滑剤の配合割合は、調製される潤滑用
被覆組成物に対して２０〜８０重量％、特に３０〜６０
重量％であることが好ましい。固体潤滑剤の配合割合が
２０重量％未満では、耐荷重性、なじみ性、フィーリン
グ性等において十分な特性が得られず、８０重量％を超
えると潤滑塗膜の密着性、耐食性、耐油性が低下する。The blending ratio of such a solid lubricant is 20 to 80% by weight, particularly 30 to 60% by weight, based on the lubricating coating composition to be prepared.
Preferably, it is % by weight. If the proportion of the solid lubricant is less than 20% by weight, sufficient properties such as load resistance, conformability, and feel cannot be obtained, and if it exceeds 80% by weight, the adhesion, corrosion resistance, and oil resistance of the lubricant coating will be impaired. decreases.

また、摩擦係数調整剤としては、炭素繊維：カーボンブ
ラック：二酸化ケイ素、炭化ケイ素、チッ化ケイ素、ガ
ラス繊維等のケイ素化合物；酸化アルミニウム；チタン
酸カリウム繊維：セルロース系繊維等を用いることがで
きる。Further, as the friction coefficient modifier, carbon fibers, carbon black, silicon compounds such as silicon dioxide, silicon carbide, silicon nitride, glass fibers, aluminum oxide, potassium titanate fibers, cellulose fibers, etc. can be used.

これらの摩擦係数調整剤は、１　ｆｌを単独で用いても
、２種以上を組み合わせて用いても良い。特に、本発明
においては摩擦係数の調整機能が高くしかも耐摩耗性の
向上に有効であることから、炭素繊維を用いるのが好ま
しい。These friction coefficient modifiers may be used alone at 1 fl or in combination of two or more types. In particular, in the present invention, carbon fiber is preferably used because it has a high ability to adjust the coefficient of friction and is effective in improving wear resistance.

摩擦係数調整剤は、繊維状のものにあっては、その繊維
長さが１０μｍ〜ｉｍ／ｍ、１ａ維径が１０〜５０μｍ
程度のものが好適である。また、粒状のものにあっては
、その粒径が１００μｍ以下程度のものが好適である。If the friction coefficient modifier is in the form of a fiber, the fiber length is 10 μm to im/m and the 1a fiber diameter is 10 to 50 μm.
It is preferable that the Further, in the case of particles, those having a particle size of about 100 μm or less are suitable.

このような摩擦係数調整剤の配合割合は、調製される潤
滑剤に対して５０重量％以下、特に５〜３０重量％とす
るのが好ましい。摩擦係数調整剤の配合割合が５０重量
％を超える場合には、潤滑剤塗膜の密着性、耐食性が低
下し、また耐摩耗性の改善効果も低下する。The blending ratio of such a friction coefficient modifier is preferably 50% by weight or less, particularly 5 to 30% by weight, based on the lubricant to be prepared. If the blending ratio of the friction coefficient modifier exceeds 50% by weight, the adhesion and corrosion resistance of the lubricant coating will decrease, and the effect of improving wear resistance will also decrease.

本発明の潤滑用被覆組成物は、例えば、合成樹脂及び固
体潤滑剤を所定の割合で配合し、更にこれに摩擦係数調
整剤の所定量を混合することにより容易に調整すること
ができる。しかも、各成分の配合割合を調整することに
より、摩擦係数を広い範囲で調整することができ、摩耗
量は、低く抑える高性能潤滑剤が提供される。The lubricating coating composition of the present invention can be easily prepared by, for example, blending a synthetic resin and a solid lubricant in a predetermined ratio, and further mixing a predetermined amount of a friction coefficient modifier thereto. Moreover, by adjusting the blending ratio of each component, the coefficient of friction can be adjusted over a wide range, and a high-performance lubricant with a low amount of wear can be provided.

なお、合成樹脂と、固体潤滑剤を配合する際、及び、各
成分を配合した後において、適量の溶剤を用いることに
より、配合工程を容易にし、かつ、容易に使用できる粘
度に調整することができる。In addition, by using an appropriate amount of solvent when blending the synthetic resin and solid lubricant and after blending each component, it is possible to facilitate the blending process and adjust the viscosity to a level that can be easily used. can.

使用する溶剤は、合成樹脂を溶解可能なものであれば特
に制限はなく、使用量も、合成樹脂の粘度、配合比が種
々異なるため、特に制限はないが、組成物１００重量部
に対して、溶剤１００〜３００重量部程度が適量である
。また使用する溶剤は、１種の単独溶剤でも、２種以上
の混合溶剤でも良い。The solvent to be used is not particularly limited as long as it can dissolve the synthetic resin, and the amount used is also not particularly limited as the viscosity and blending ratio of the synthetic resin vary, but based on 100 parts by weight of the composition. The appropriate amount is about 100 to 300 parts by weight of the solvent. The solvent used may be one type of single solvent or a mixture of two or more types of solvents.

さらに、本発明の潤滑剤は、上記３成分の他に、必要に
応じて各種改質剤等の添加剤を含有していても良い。こ
の場合、添加剤配合量は調製される潤滑剤に対して２０
重量％以下とする。Furthermore, the lubricant of the present invention may contain additives such as various modifiers, if necessary, in addition to the above three components. In this case, the additive content is 20% of the lubricant to be prepared.
% by weight or less.

［作用］ 本発明の潤滑用被覆組成物は、固体潤滑剤により優れた
潤滑性が付与され、一方、摩擦係数調整剤により、この
潤滑性能が調整され、耐摩耗性を損なうことなく、摩擦
係数が所望とする適度な値にされる。[Function] The lubricating coating composition of the present invention is provided with excellent lubricity by the solid lubricant, while this lubrication performance is adjusted by the friction coefficient modifier, and the friction coefficient is improved without impairing wear resistance. is set to a desired appropriate value.

［実施例］ 以下、実施例及び比較例を挙げて本発明をより具体的に
説明するが、本発明はその要旨を超えない限り、以下の
実施例に限定されるものではない。[Examples] Hereinafter, the present invention will be described in more detail with reference to Examples and Comparative Examples, but the present invention is not limited to the following Examples unless it exceeds the gist thereof.

実施例１〜２１．比較例１ 第１表に示す原料を用いて第２表中の配合にて、潤滑用
被覆組成物を調整し、製造する。Examples 1-21. Comparative Example 1 A lubricating coating composition is prepared and produced using the raw materials shown in Table 1 and the formulations shown in Table 2.

具体的には、合成樹脂を１００重量部に対して、１００
〜２００重量部の溶剤（Ｍ　−Ｅ　−Ｋ。Specifically, 100 parts by weight of synthetic resin
~200 parts by weight of solvent (M-E-K.

キシレン等）で溶解したものに、固体潤滑剤を加え、ボ
ールミルにて３時間粉砕を行なう、それに対し、所定量
の摩擦係数調整剤を加え攪拌を行なったものを試料とす
る。A solid lubricant was added to the solution dissolved in xylene, etc.), and the mixture was ground in a ball mill for 3 hours.A predetermined amount of a friction coefficient modifier was added to the solution and stirred to prepare a sample.

各試料の摩擦係数及び摩耗量の改善効果を下記方法によ
り調べ、その結果を第２表に示す。The effect of improving the friction coefficient and wear amount of each sample was investigated by the following method, and the results are shown in Table 2.

■　摩擦係数の測定 下記の試験機、テストピース、テスト条件にて行なった
。即ち、一定速度で回転するリングにブロックを一定の
荷重で押し付け、両テストピース間の摩擦係数を測定し
た。なお、ブロック及びリングの当接面にはそれぞれリ
ン酸亜鉛皮膜処理等の下地処理を行った上、エアスプレ
ーにて約２０μｍの塗膜厚になるように吹き付け、その
後各硬化条件にて硬化させて塗膜を形成した。■Measurement of friction coefficient The test was carried out using the following testing machine, test piece, and test conditions. That is, a block was pressed with a constant load against a ring rotating at a constant speed, and the coefficient of friction between both test pieces was measured. The abutment surfaces of the block and ring were treated with a zinc phosphate coating, etc., and then air sprayed to a coating thickness of approximately 20 μm, and then cured under various curing conditions. A coating film was formed.

また、リングの非当接面側は差動制限デファレンシャル
ギヤ用オイル（鉱物油）に浸漬した状態と、浸漬しない
状態とにした。In addition, the non-contact surface side of the ring was immersed in differential limiting differential gear oil (mineral oil) and was not immersed.

試験機 ＦＡＬＥＸ＃１゜ Ｒｉｎｇ　　＆　　Ｂｌｏｃｋ　　ＴＥＳＴＭＡＣＨＩ
ＮＥ　［Ｆａｖｉ　１１ｅ−ＬｅＶａｌｌｙ社製（ＡＳ
ＴＭ　　Ｄ　　２７１４）］テテストピー スング：５ＡＥ４６２０　５ＴＥＥＬ。Testing machine FALEX#1゜Ring & Block TESTMACHI
NE [Favi 11e-Manufactured by LeVally (AS
TM D 2714)] Test Piecing: 5AE4620 5TEEL.

ＨＲｃ５８〜６３，６〜１２ｒｍＳ ブロック：５ＡＥＯ−ＩＳＴＥＥＬ。HRc58~63,6~12rmS Block: 5AEO-ISTEEL.

ＨＲＣ５８〜６３．４〜８ｒｍＳ テスト条件 荷　　　重：　　１　００Ｊ２ｂｓ 回転速度：３０ｒｐｍ ■　摩耗量の測定 鋼製プレートの表面に■の摩擦係数の測定の時と同様な
方法により各々の潤滑用被覆組成物を塗布した摩擦板Ａ
と、鋼製（材質：ＪＩＳ規格ＳＫ５Ｍ）で、焼入れ焼戻
しを施した鋼板（硬度ＨＶ４６０）よりなりその表面粗
さが０．５μＲａの摩擦板Ｂ（外径１２０ｍｍ、内径１
００ｍｍ、厚さ１．８ｍｍ）を組み合わせて、スラスト
試験機により摩擦試験を行なった。HRC58-63.4-8rmS Test conditions Load: 1 00 J2bs Rotation speed: 30 rpm ■ Measurement of wear amount Each lubricating coating composition was applied to the surface of the steel plate by the same method as in the measurement of friction coefficient (■). Coated friction plate A
Friction plate B (outer diameter 120 mm, inner diameter 1
00 mm, thickness 1.8 mm), and a friction test was conducted using a thrust tester.

即ち、差動制限デファレンシャルギヤ用オイル中で約５
Ｏｒｐｍにて回転している摩擦板Ｂに対し、摩擦板Ａを
荷重５００ｋｇｆで押しつけ、２００時間後の摩耗量（
摩耗深さ）を調べた。That is, approximately 5
Friction plate A is pressed against friction plate B rotating at Orpm with a load of 500 kgf, and the wear amount after 200 hours (
Wear depth) was investigated.

第２表より明らかなように、本発明の潤滑用被覆組成物
は、摩擦係数が従来品（比較例１）に比べて高く、しか
もその値を広い範囲で調整することができる。一方、摩
耗量は著しく少ない、これに対し、従来品（比較例１）
では、摩擦係数が低過ぎる上に、摩耗量が大きい。As is clear from Table 2, the lubricating coating composition of the present invention has a higher coefficient of friction than the conventional product (Comparative Example 1), and its value can be adjusted within a wide range. On the other hand, the amount of wear is extremely small, whereas the conventional product (Comparative Example 1)
In this case, the coefficient of friction is too low and the amount of wear is large.

なお、この比較例１の場合には塗膜が摩滅して一部下地
が露出していたのに対し、本発明品の場合は、いずれも
塗膜はほぼ完全に残っていた。In addition, in the case of Comparative Example 1, the coating film was worn away and a portion of the base was exposed, whereas in the case of the products of the present invention, the coating film remained almost completely in all cases.

更に、本発明の潤滑用被覆組成物を用いた場合、試験方
法■で示すスラスト試験機での試験において、μＳ（静
摩擦係数）がμｄ（動摩擦係数）よりも常に低くなり、
スティックスリップ現象による異音の発生を抑制するの
にも効果があることがわかった。それに対し、従来品（
比較例１）では、μＳとμｄがほぼ同等かμＳよりμｄ
がやや低い傾向を示し、しかも耐摩耗性が不足している
ため、試験中下地が露出することから、スティックスリ
ップ現象による異音が発生した。Furthermore, when the lubricating coating composition of the present invention is used, μS (static friction coefficient) is always lower than μd (dynamic friction coefficient) in the test using a thrust tester shown in test method ①.
It was also found to be effective in suppressing the generation of abnormal noises caused by the stick-slip phenomenon. In contrast, conventional products (
In Comparative Example 1), μS and μd are almost equal or μd is smaller than μS.
Because it showed a slightly low tendency to wear and had insufficient abrasion resistance, the base material was exposed during the test, which caused abnormal noises due to the stick-slip phenomenon.

比較例、実施例中の各組成物の商標名及びメーカー名を
第１表に示すが、今回の試験に用いた原［発明の効果］ 以上詳述した通り、本発明の潤滑用被覆組成物によれば
、摩擦係数を比較的高い値にまで所望に応じて制御する
ことができ、しかも摩耗量は大幅に低減することができ
る。Table 1 shows the trade name and manufacturer name of each composition in Comparative Examples and Examples. According to the invention, the coefficient of friction can be controlled to a relatively high value as desired, and the amount of wear can be significantly reduced.

従って、本発明の潤滑用被覆組成物によれば油中で用い
られる差動制限デファレンシャルギヤや、クラッチ板及
びプーリー等の、トルクの伝達が確実に行なわれるため
の適度に高い摩擦係数を必要とし、かつ摩耗量は低く抑
えることが必要とされる部材、及びボルト等の緩みが生
じにくい程度の適度に高い摩擦係数を必要とする部材の
摺動性能、摩擦性能、潤滑性能を大幅に向上させること
ができる。Therefore, the lubricating coating composition of the present invention can be used in limited slip differential gears, clutch plates, pulleys, etc. used in oil, which require a moderately high coefficient of friction to ensure torque transmission. , and significantly improves the sliding performance, friction performance, and lubrication performance of parts that need to keep the amount of wear low, and parts that require a moderately high coefficient of friction to prevent bolts from loosening. be able to.

代理人　　弁理士　　重　野　　剛Agent: Patent attorney Tsuyoshi Shigeno

Claims (1)

【特許請求の範囲】[Claims] （１）合成樹脂及び固体潤滑剤を含む潤滑用被覆組成物
であって、摩擦係数調整剤を含むことを特徴とする潤滑
用被覆組成物。(1) A lubricating coating composition containing a synthetic resin and a solid lubricant, characterized in that it contains a friction coefficient modifier.
JP63311216A 1988-12-09 1988-12-09 Lubricating coating composition Expired - Fee Related JPH0674389B2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP63311216A JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition
DE8989122596T DE68902305T2 (en) 1988-12-09 1989-12-07 LUBRICATION COMPOSITION.
EP89122596A EP0372559B1 (en) 1988-12-09 1989-12-07 Coating composition for lubrication
US08/246,398 US5427698A (en) 1988-12-09 1994-05-18 Coating composition for lubrication

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP63311216A JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition

Publications (2)

Publication Number Publication Date
JPH02155958A true JPH02155958A (en) 1990-06-15
JPH0674389B2 JPH0674389B2 (en) 1994-09-21

Family

ID=18014498

Family Applications (1)

Application Number Title Priority Date Filing Date
JP63311216A Expired - Fee Related JPH0674389B2 (en) 1988-12-09 1988-12-09 Lubricating coating composition

Country Status (3)

Country Link
EP (1) EP0372559B1 (en)
JP (1) JPH0674389B2 (en)
DE (1) DE68902305T2 (en)

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Also Published As

Publication number Publication date
JPH0674389B2 (en) 1994-09-21
EP0372559A1 (en) 1990-06-13
EP0372559B1 (en) 1992-07-29
DE68902305D1 (en) 1992-09-03
DE68902305T2 (en) 1992-12-10

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