JPH05277346A - Detection of failure of separating membrane of membrane filter device - Google Patents

Detection of failure of separating membrane of membrane filter device

Info

Publication number
JPH05277346A
JPH05277346A JP8013092A JP8013092A JPH05277346A JP H05277346 A JPH05277346 A JP H05277346A JP 8013092 A JP8013092 A JP 8013092A JP 8013092 A JP8013092 A JP 8013092A JP H05277346 A JPH05277346 A JP H05277346A
Authority
JP
Japan
Prior art keywords
pressure
membrane
air
separation membrane
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP8013092A
Other languages
Japanese (ja)
Inventor
Katsuro Ishihara
勝郎 石原
Kanji Tokushima
幹治 徳島
Yoshihisa Narukami
善久 鳴上
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kubota Corp
Original Assignee
Kubota Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kubota Corp filed Critical Kubota Corp
Priority to JP8013092A priority Critical patent/JPH05277346A/en
Publication of JPH05277346A publication Critical patent/JPH05277346A/en
Pending legal-status Critical Current

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  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

PURPOSE:To enable he easy and sure detection of the failutre of the separating membrane of a membrane filter device without individual differences by bringing liquid into contact with one surface of the separating membrane, supplying air under pressurization to the inside of the pipe on a filtrate recovery side from an air supply device for back washing, then detecting a pressure change after hermetically holding the pipe inside. CONSTITUTION:The membrane filter device 1 is immersed into the liquid to be treated and the air is supplied under pressurization to the device 1 from an air compressor C for back washing in order to feed bubbles into the liquid through the separating membrane. The gauge pressure drops sharply first, then gradually slowly, and the generation of the bubbles stops when the air is stopped and the inside of the pipe on the filtrate recovery side is hermetically maintained. The relation between the lapse of the time and the pressure drop is qualitatively plotted on a graph. Judgment is made that there is no abnormality if the pressure does not fall below the min. supply pressure for back washing, and that there is the abnormality of the pressure falls.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、分離膜と、その分離膜
に対する逆洗用エアー供給装置とを備えた膜濾過装置に
おいて、前記分離膜の破損を検知する方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for detecting breakage of a separation membrane in a membrane filtration device equipped with the separation membrane and an air supply device for backwashing the separation membrane.

【0002】[0002]

【従来の技術】従来、この種の膜濾過装置の分離膜の破
損を検知するには、濾液の濁度を目視で観察する方法に
頼っていた。
2. Description of the Related Art Conventionally, in order to detect breakage of a separation membrane of this type of membrane filtration device, a method of visually observing the turbidity of the filtrate has been used.

【0003】[0003]

【発明が解決しようとする課題】ところが、この方法で
は、濁度の判定に個人差があり、そのため分離膜破損の
有無の判断ミスが伴いやすい欠点があった。そこで、本
発明の目的は、個人差なく簡単で確実な膜濾過装置の分
離膜破損検知方法を提供することにある。
However, this method has a drawback in that there is an individual difference in the determination of the turbidity, and thus it is easy to make an error in determining whether or not the separation membrane is damaged. Therefore, an object of the present invention is to provide a simple and reliable method for detecting separation membrane breakage of a membrane filtration device without individual differences.

【課題を解決するための手段】この目的を達成するため
の本発明による膜濾過装置の分離膜の破損検知方法の特
徴手段は、分離膜の一方の面が液に接触している状態
で、逆洗用エアー供給装置から前記分離膜に対する濾液
回収側の管内にエアーを加圧供給し、前記管内を、予め
測定してある前記分離膜に対する逆洗のための最低限供
給圧よりも高い圧力にした状態で、上記逆洗用エアー供
給装置からのエアーの供給を止めて前記管内を気密に保
持し、この時点から設定時間後の前記管内における圧力
変化を検出して、その検出圧力が前記逆洗のための最低
限供給圧よりも下がらなかった場合は異常がないものと
判断し、その検出圧力が前記逆洗のための最低限供給圧
よりも下がった場合は異常があるものと判断するところ
にある。
[Means for Solving the Problems] A characteristic means of a method for detecting damage to a separation membrane of a membrane filtration device according to the present invention for achieving this object is that one surface of the separation membrane is in contact with a liquid. Air is supplied under pressure from the backwashing air supply device into the tube on the filtrate recovery side for the separation membrane, and the inside pressure of the tube is higher than the minimum supply pressure for backwashing the separation membrane that has been measured in advance. In this state, the air supply from the backwash air supply device is stopped to keep the inside of the pipe airtight, and from this time, the pressure change in the pipe after a set time is detected, and the detected pressure is If it does not fall below the minimum supply pressure for backwashing, it is judged that there is no abnormality, and if the detected pressure falls below the minimum supply pressure for backwashing, it is judged that there is abnormality. There is a place to do it.

【0004】[0004]

【作用】破損のない新しい分離膜の一方の面を液に接触
させた状態で、分離膜を通して液中に気泡が送り込まれ
るように、前記分離膜に対する濾液回収側からエアーを
加圧供給し、エアーの供給を止めて上述の分離膜に対す
る濾液回収側の管内を気密に保つと、前記気泡の発生が
次第に少なくなり、前記管内の空気圧がある程度下がっ
たところで気泡の発生が止まる。このときの管内圧力、
即ち前記分離膜に対する逆洗のための最低限供給圧を測
定しておく。破損の有無を調べようとする分離膜がもし
も破損のない正常な状態にあるならば、同様の手順を踏
み、エアーの供給を止めて上述の分離膜に対する濾液回
収側の管内を気密に保つと、前記管内の圧力が前記最低
限供給圧よりも下がることはないが、分離膜に破損があ
れば、破損箇所からエアーが漏れるので前記管内が前記
最低限供給圧よりも低い圧力になる。従って、エアーを
止めた時点から設定時間後の前記管内における圧力変化
を検出して、その検出圧力が前記逆洗のための最低限供
給圧よりも下がらなかった場合は異常がないものと判断
し、その検出圧力が前記逆洗のための最低限供給圧より
も下がった場合は異常があるものと判断することができ
る。
[Function] With one surface of a new undamaged separation membrane in contact with a liquid, air is pressure-supplied from the filtrate recovery side of the separation membrane so that air bubbles are sent into the liquid through the separation membrane, When the supply of air is stopped and the inside of the filtrate recovery side tube with respect to the separation membrane is kept airtight, the generation of the bubbles is gradually reduced, and the generation of bubbles is stopped when the air pressure in the tube is lowered to some extent. Pipe pressure at this time,
That is, the minimum supply pressure for backwashing the separation membrane is measured. If the separation membrane whose damage is to be examined is in a normal state without breakage, follow the same procedure and stop the air supply to keep the inside of the filtrate collection side tube for the separation membrane airtight. Although the pressure in the pipe does not fall below the minimum supply pressure, if the separation membrane is damaged, air leaks from the damaged portion, so that the pressure in the pipe becomes lower than the minimum supply pressure. Therefore, it is judged that there is no abnormality if the pressure change in the pipe after the set time from the time when the air is stopped is detected and the detected pressure does not fall below the minimum supply pressure for the backwash. If the detected pressure falls below the minimum supply pressure for backwashing, it can be determined that there is an abnormality.

【0005】[0005]

【発明の効果】個人差なく簡単で確実な膜濾過装置の分
離膜破損検知方法を提供することができた。尚、前記設
定時間を長くとれば、実操業に差し支えない程度の小さ
な破損でも検知することができるので、破損が大きくな
って支障が生じる前にその予測が付きやすく、例えば、
高価な固形分や、微量でも有害な固形分を分離する等、
特に確実な濾過が要求される場合であっても、これを流
出するような事態が起こる前に、早期に正常な分離膜と
交換し、確実な濾過処理を期することができる。
EFFECTS OF THE INVENTION It is possible to provide a simple and reliable method for detecting damage to a separation membrane of a membrane filtration device that does not differ among individuals. It should be noted that if the set time is set to be long, it is possible to detect even a small breakage that does not interfere with actual operation, so it is easy to predict the damage before it becomes large and troubles occur, for example,
Separation of expensive solids and harmful solids even in trace amounts
Even in the case where particularly reliable filtration is required, it is possible to replace the normal separation membrane with a normal separation membrane at an early stage to ensure a reliable filtration process before such a situation occurs.

【0006】[0006]

【実施例】以下、本発明による膜濾過装置の分離膜破損
検知方法の実施例を図に基づいて説明する。図1は、膜
濾過装置1を活性汚泥による汚水処理槽2内の被処理液
に浸漬して、ポンプPの負圧により槽内の被処理液を吸
引濾過する汚水処理装置の概要を示す説明図である。膜
濾過装置1は多孔質のセラミックパイプからなる前記分
離膜の膜エレメントを複数並列に接続して構成してあ
る。図中Cは逆洗用エアー供給装置たるエアーコンプレ
ッサーであり、3、4は開閉バルブである。通常の濾過
を行うときは、バルブ4を閉じ、バルブ3を開いて、ポ
ンプPの負圧により槽内の被処理液を膜濾過装置1の前
記分離膜を通して吸引濾過し、濾液だけを槽外に排出で
きるようにしてある。又、バルブ3を閉じ、バルブ4を
開いてエアーコンプレッサーCによりエアーを加圧供給
し、加圧エアーを通常の濾過時とは逆方向に分離膜を通
過させて、主に分離膜の被処理液側に付着した固形分を
剥離させる所謂逆洗(逆圧洗浄)を行うことができる。
Sは、エアーコンプレッサーCから膜濾過装置1に通ず
る配管の膜濾過装置1に近い管内のエアー圧を検出する
ための圧力ゲージである。上記の構成によって、分離膜
の破損の有無を次のようにして検知することができた。
破損のない新しい分離膜を備えた膜濾過装置1を被処理
液中に浸漬し、分離膜を通して液中に気泡が送り込まれ
るように、エアーコンプレッサーCから膜濾過装置1に
エアーをゲージ圧2kg/cm2(以後、圧力は全てゲ
ージ圧で示す)で加圧供給し、エアーの供給を止めて分
離膜に対する濾液回収側の管内を気密に保つと、約30
秒で前記管内の空気圧が1kg/cm2に下がり、更に
そのまま放置すると前記気泡の発生が次第に少なくな
り、約5分後に、前記圧力ゲージSの示すゲージ圧が
0.9kg/cm2まで下がったところで気泡の発生が
止まった。この圧力以下では逆洗を行うことができな
い。つまり、この仕様の分離膜に対する逆洗を行うため
のエアーの最低限供給圧は約0.9kg/cm2であ
る。上述の逆洗用エアー供給装置からのエアーの供給を
止めて前記管内を気密に保持した時点からの経過時間t
とこれに対応する前記管内における圧力pを、前者を横
軸に、後者を縦軸にとって、定性的にグラフ化すると図
2に示すごとく表すことができる。図中Nは新しい分離
膜における場合を示し、Lは逆洗を行うための最低限供
給圧を示す。例えば上述の新しい分離膜では、Lは約
0.9kg/cm 2である。破損の有無を調べようとす
る使用中の分離膜が上述の分離膜と同じ仕様であって、
破損のない正常な状態にあるときには、上述の手順と同
様の手順を踏み、エアーの供給を止めて上述の分離膜に
対する濾液回収側の管内を気密に保つと、前記管内の圧
力が前記最低限供給圧よりも下がることはなく、図2の
曲線Gで示されるように、一般的にはLよりもやや高い
管内圧力で平衡状態が得られる。分離膜に破損があった
り、或いは分離膜の取り付け箇所等に異常があれば、破
損箇所等からエアーが漏れるので前記管内が前記最低限
供給圧よりも低い圧力となり、漏れが大きい場合は、図
2の曲線Wで示されるように、例えば、約30秒で0.
1kg/cm2付近まで下がる急激な圧力降下が確認さ
れた。前記エアー漏れの少ない場合は、エアー漏れの大
きい場合に比べると上述の管内における圧力低下が少な
い。しかし、実際の濾過を行うには差し支えのない程度
の小さな破損を生じた分離膜の場合であっても、多少と
も前記エアー漏れがあれば、図2の曲線Bで示されるよ
うに、例えば50〜180秒後には前記最低供給圧より
も明らかに低い圧力に至る圧力降下が認められる。従っ
て、エアーを止めた時点から設定時間、例えば30秒後
の前記管内における圧力変化を前記圧力ゲージSで検出
し、その検出圧力が前記逆洗のための最低限供給圧より
も下がらなかった場合は異常がないものと判断し、その
検出圧力が前記逆洗のための最低限供給圧よりも下がっ
た場合は異常があるものと判断することができる。分離
膜の異常の有無は前記圧力ゲージSの目盛りを直接読み
取ることにより判断してもよいが、例えば、逆洗完了後
エアーを止めて前記管内を気密に保ち、一定時間経過後
の前記管内における圧力変化を自動的に検出して、その
検出圧力が前記逆洗のための最低限供給圧よりも下がっ
た場合は警報が発せられるようにする等、異常の有無を
自動的に検知する構成にしてもよい。
EXAMPLES Hereinafter, separation membrane damage of the membrane filtration device according to the present invention
An embodiment of the detection method will be described with reference to the drawings. Figure 1 is a membrane
Liquid to be treated in the sewage treatment tank 2 using activated sludge
And soak the liquid to be treated in the tank with the negative pressure of the pump P.
It is explanatory drawing which shows the outline of the sewage treatment apparatus which carries out drawing filtration. film
The filtering device 1 is composed of a porous ceramic pipe.
It consists of multiple membrane elements connected in parallel.
It C in the figure is an air compressor that is an air supply device for backwashing.
It is a susa and 3 and 4 are opening / closing valves. Normal filtration
Valve, close valve 4, open valve 3, and
The negative pressure of the pump P causes the liquid to be treated in the tank to flow in front of the membrane filtration device 1.
Suction-filter through the separation membrane and discharge only the filtrate out of the tank.
I can do it. Also, close valve 3 and valve 4.
Open and pressurize air by air compressor C
Then, pressurize air through the separation membrane in the opposite direction to the normal filtration.
To remove the solids that adhere to the treated liquid side of the separation membrane.
So-called back washing (back pressure washing) for peeling can be performed.
S does not pass from the air compressor C to the membrane filtration device 1.
The air pressure in the pipe close to the membrane filtration device 1 of the pipe
Is a pressure gauge for. With the above configuration, the separation membrane
It was possible to detect the presence or absence of breakage in the following manner.
Treat the membrane filtration device 1 with a new separation membrane without damage
Immerse in the liquid, and bubbles are sent into the liquid through the separation membrane.
So that from the air compressor C to the membrane filtration device 1
Air pressure gauge 2kg / cm2(After that, all pressure
Pressure) to stop the air supply and
If the inside of the tube on the filtrate recovery side of the membrane is kept airtight, it will be about 30
The air pressure in the pipe is 1 kg / cm per second.2Down to
If left as it is, the generation of bubbles will gradually decrease.
After about 5 minutes, the gauge pressure indicated by the pressure gauge S is
0.9 kg / cm2Bubbles are generated when it goes down to
Stopped. Backwash cannot be performed below this pressure
Yes. In other words, in order to backwash the separation membrane of this specification
The minimum supply pressure of air is about 0.9 kg / cm2And
It Supply the air from the above-mentioned backwash air supply device.
Elapsed time t from the time when the tube is stopped and the inside of the tube is kept airtight
And the pressure p in the pipe corresponding to this
The graph is qualitatively plotted with the latter on the axis and the latter on the vertical axis.
It can be expressed as shown in 2. N in the figure is a new separation
In the case of membrane, L is the minimum supply for backwashing.
Indicates the supply pressure. For example, in the above-mentioned new separation membrane, L is about
0.9 kg / cm 2Is. Trying to check for damage
The separation membrane in use has the same specifications as the separation membrane described above,
When in normal condition with no damage, follow the procedure above.
Follow the same procedure to stop the air supply and use the above separation membrane.
On the other hand, if the inside of the tube on the filtrate recovery side is kept airtight, the pressure inside the tube will be
The force does not fall below the minimum supply pressure shown in Fig. 2.
Generally slightly higher than L, as shown by curve G
An equilibrium state is obtained by the pressure in the pipe. The separation membrane was damaged
If there is something wrong with the
Since air leaks from damaged parts, the inside of the pipe is at the minimum
If the pressure is lower than the supply pressure and the leak is large,
As shown by the curve W of 2, for example, 0.
1 kg / cm2A sudden pressure drop to the vicinity was confirmed.
It was If the air leakage is small, the air leakage is large.
The pressure drop in the pipe is smaller than that in the threshold
Yes. However, there is no problem in performing actual filtration.
Even if the separation membrane has a small breakage,
If there is air leakage, it will be shown by curve B in FIG.
As described above, for example, after 50 to 180 seconds,
However, a pressure drop to a clearly low pressure is recognized. Obey
Then, after the air is stopped, the set time, for example 30 seconds later
Of pressure change in the pipe of the
However, the detected pressure is lower than the minimum supply pressure for backwashing.
If it does not go down, it is judged that there is no abnormality, and the
The detected pressure is lower than the minimum supply pressure for backwashing.
If it does, it can be judged that there is an abnormality. Separation
Read the scale of the pressure gauge S directly to see if there is any abnormality in the membrane.
It may be judged by taking it, for example, after backwashing is completed.
Turn off the air to keep the inside of the tube airtight, and after a certain period of time
The pressure change in the pipe of
The detected pressure is lower than the minimum supply pressure for backwashing.
If there is an abnormality, make sure that an alarm is issued
You may make it the structure which detects automatically.

【0007】尚、特許請求の範囲の項に図面との対照を
便利にするために符号を記すが、該記入により本発明は
添付図面の構成に限定されるものではない。
It should be noted that reference numerals are added to the claims for convenience of comparison with the drawings, but the present invention is not limited to the configurations of the accompanying drawings by the entry.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明による膜濾過装置の分離膜破損検知方法
の手順を示すための説明図
FIG. 1 is an explanatory diagram showing a procedure of a separation membrane damage detection method of a membrane filtration device according to the present invention.

【図2】分離膜の破損が管内の圧力降下に及ぼす影響を
定性的に示す曲線グラフ
FIG. 2 is a curve graph qualitatively showing the influence of the breakage of the separation membrane on the pressure drop in the tube.

【符号の説明】[Explanation of symbols]

1 膜濾過装置 C 逆洗用エアー供給装置 1 Membrane Filtration Device C Back Washing Air Supply Device

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 分離膜と、その分離膜に対する逆洗用エ
アー供給装置とを備えた膜濾過装置(1)において、前
記分離膜の破損を検知する方法であって、 前記分離膜の一方の面が液に接触している状態で、前記
逆洗用エアー供給装置(C)から前記分離膜に対する濾
液回収側の管内にエアーを加圧供給し、前記管内を、予
め測定してある前記分離膜に対する逆洗のための最低限
供給圧よりも高い圧力にした状態で、上記逆洗用エアー
供給装置(C)からのエアーの供給を止めて前記管内を
気密に保持し、この時点から設定時間後の前記管内にお
ける圧力変化を検出して、その検出圧力が前記逆洗のた
めの最低限供給圧よりも下がらなかった場合は異常がな
いものと判断し、その検出圧力が前記逆洗のための最低
限供給圧よりも下がった場合は異常があるものと判断す
る膜濾過装置の分離膜破損検知方法。
1. A method for detecting breakage of the separation membrane in a membrane filtration device (1) comprising a separation membrane and an air supply device for backwashing the separation membrane, comprising: In the state where the surface is in contact with the liquid, air is pressure-supplied from the backwashing air supply device (C) into the filtrate recovery side pipe with respect to the separation membrane, and the inside of the pipe is subjected to the previously measured separation. With the pressure higher than the minimum supply pressure for backwashing the membrane, the air supply from the backwashing air supply device (C) is stopped to keep the inside of the pipe airtight, and set from this point. After detecting the pressure change in the pipe after a lapse of time, if the detected pressure does not fall below the minimum supply pressure for the backwash, it is judged that there is no abnormality, and the detected pressure is the same as that of the backwash. If it falls below the minimum supply pressure for Separation membrane damage detection method of membrane filtration device for determining that there is always.
JP8013092A 1992-04-02 1992-04-02 Detection of failure of separating membrane of membrane filter device Pending JPH05277346A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP8013092A JPH05277346A (en) 1992-04-02 1992-04-02 Detection of failure of separating membrane of membrane filter device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8013092A JPH05277346A (en) 1992-04-02 1992-04-02 Detection of failure of separating membrane of membrane filter device

Publications (1)

Publication Number Publication Date
JPH05277346A true JPH05277346A (en) 1993-10-26

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JP8013092A Pending JPH05277346A (en) 1992-04-02 1992-04-02 Detection of failure of separating membrane of membrane filter device

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2781782A1 (en) * 1998-07-28 2000-02-04 Polymem METHOD AND DEVICE FOR FILTERING WATER BY A SUBMERSIBLE MEMBRANE
FR2781781A1 (en) * 1998-07-28 2000-02-04 Polymem Submerged membrane filtration of potable water, re-using redundant sand filtration sites

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6094105A (en) * 1983-10-27 1985-05-27 Kurita Water Ind Ltd Membrane separator

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6094105A (en) * 1983-10-27 1985-05-27 Kurita Water Ind Ltd Membrane separator

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2781782A1 (en) * 1998-07-28 2000-02-04 Polymem METHOD AND DEVICE FOR FILTERING WATER BY A SUBMERSIBLE MEMBRANE
FR2781781A1 (en) * 1998-07-28 2000-02-04 Polymem Submerged membrane filtration of potable water, re-using redundant sand filtration sites
WO2000006500A1 (en) * 1998-07-28 2000-02-10 S.A. Polymem Method and device for membrane filtering of water
US6838003B1 (en) 1998-07-28 2005-01-04 S.A. Polymem Method and device for membrane filtering of water

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