JPH05267269A - Method and apparatus for vacuum drying - Google Patents

Method and apparatus for vacuum drying

Info

Publication number
JPH05267269A
JPH05267269A JP6173892A JP6173892A JPH05267269A JP H05267269 A JPH05267269 A JP H05267269A JP 6173892 A JP6173892 A JP 6173892A JP 6173892 A JP6173892 A JP 6173892A JP H05267269 A JPH05267269 A JP H05267269A
Authority
JP
Japan
Prior art keywords
semiconductor wafer
drying
work
vacuum
iced
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP6173892A
Other languages
Japanese (ja)
Inventor
Toshihiko Sakurai
俊彦 桜井
Tetsuya Takagaki
哲也 高垣
Kazuhiro Hata
和博 秦
Yuji Noguchi
雄二 野口
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Ltd
Original Assignee
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Ltd filed Critical Hitachi Ltd
Priority to JP6173892A priority Critical patent/JPH05267269A/en
Publication of JPH05267269A publication Critical patent/JPH05267269A/en
Pending legal-status Critical Current

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  • Drying Of Solid Materials (AREA)
  • Cleaning Or Drying Semiconductors (AREA)

Abstract

PURPOSE:To dry a semiconductor wafer with high cleanliness, to eliminate that a foreign body adheres in a drying operation as a problem in conventional cases and to enhance the safety of the drying operation in a vacuum drying apparatus. CONSTITUTION:A vacuum drying apparatus has the following structure: in a state that a semiconductor wafer 11 is kept clean by a cleaning operation, waterdrops 13 which have adhered to the semiconductor wafer 11 are cooled rapidly and iced; the atmosphere of the semiconductor wafer 11 which has been iced is set to a vacuum state; ice 14 which has been iced is sublimated; and the semiconductor wafer 11 is dried.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、乾燥技術に関し、特
に、たとえば半導体集積回路装置の製造工程で用いられ
るウエハ乾燥技術に適用して有効な技術に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a drying technique, and more particularly to a technique effectively applied to a wafer drying technique used in a manufacturing process of a semiconductor integrated circuit device, for example.

【0002】[0002]

【従来の技術】従来の乾燥装置としては、たとえば、ス
ピン乾燥装置およびベーパ乾燥装置が使用されている。
2. Description of the Related Art For example, spin dryers and vapor dryers are used as conventional dryers.

【0003】前記スピン乾燥装置は、半導体ウエハを高
速回転させ、半導体ウエハに付着した水滴を遠心力で除
去する構造となっている。
The spin dryer has a structure in which a semiconductor wafer is rotated at a high speed and water droplets attached to the semiconductor wafer are removed by centrifugal force.

【0004】また、前記ベーパ乾燥装置は、半導体ウエ
ハに付着した水滴をイソプロピルアルコールの蒸気で置
換して乾燥する構造となっている。
Further, the vapor drying device has a structure in which water droplets attached to a semiconductor wafer are replaced with vapor of isopropyl alcohol and dried.

【0005】[0005]

【発明が解決しようとする課題】しかし、前記した従来
のスピン乾燥装置の構造では、半導体ウエハを高速回転
させるため、回転機構部のシールの劣化や静電気の発生
により、半導体ウエハに異物が付着し易いという問題が
あった。
However, in the structure of the conventional spin drying apparatus described above, since the semiconductor wafer is rotated at a high speed, foreign matter adheres to the semiconductor wafer due to deterioration of the seal of the rotating mechanism and generation of static electricity. There was a problem that it was easy.

【0006】また、前記した従来のベーパ乾燥装置の構
造では、半導体ウエハを高清浄化できる点で優れている
が、可燃性のイソプロピルアルコールの蒸気を使用する
ため、火災を発生し易く、危険性が高いという問題があ
った。
Further, the structure of the conventional vapor dryer described above is excellent in that the semiconductor wafer can be highly cleaned, but since it uses the vapor of combustible isopropyl alcohol, it easily causes a fire and is dangerous. There was a problem of being expensive.

【0007】本発明の目的は、ワークを高清浄に乾燥す
ることのできる乾燥技術を提供することにある。
An object of the present invention is to provide a drying technique capable of drying a work with high cleanliness.

【0008】本発明の他の目的は、従来、問題となって
いた乾燥の際の異物の付着をなくし、安全性を向上させ
ることのできる乾燥技術を提供することにある。
Another object of the present invention is to provide a drying technique capable of eliminating the adhesion of foreign matter during drying, which has been a problem in the past, and improving safety.

【0009】本発明の前記ならびにその他の目的と新規
な特徴は、本明細書の記述および添付図面から明らかに
なるであろう。
The above and other objects and novel features of the present invention will be apparent from the description of this specification and the accompanying drawings.

【0010】[0010]

【課題を解決するための手段】本願において開示される
発明のうち、代表的なものの概要を簡単に説明すれば、
以下の通りである。
Among the inventions disclosed in the present application, a brief description will be given to the outline of typical ones.
It is as follows.

【0011】本発明における真空乾燥装置は、ワークに
付着した水滴もしくは水分を急冷却して氷化させる冷却
手段と、前記氷化したワークの雰囲気を真空状態にする
真空手段とを備えた構造としたものである。
The vacuum drying apparatus according to the present invention has a structure including cooling means for rapidly cooling water droplets or water adhering to a work to be frozen, and vacuum means for bringing the atmosphere of the frozen work into a vacuum state. It was done.

【0012】[0012]

【作用】洗浄済のワークを乾燥させる場合、まず、洗浄
によりワークを清浄に保った状態でワークに付着した水
滴もしくは水分を急冷却して氷化させ、次いで、ワーク
の雰囲気を真空状態にして氷化した氷を昇華させてワー
クを乾燥する。
[Function] When the washed work is dried, first, the water droplets or water attached to the work is rapidly cooled to be iced while the work is kept clean by washing, and then the work atmosphere is vacuumed. Sublimate the frozen ice and dry the work.

【0013】このように、洗浄によりワークに付着した
水滴を急冷却して氷化させ、この氷化した氷を昇華させ
ることにより、ワークの表面にウォーターマークと呼ば
れるシミ等を残さずにワークを高清浄に乾燥することが
できる。
As described above, the water droplets attached to the work by the washing are rapidly cooled to be iced, and the iced ice is sublimated to leave the work without leaving a stain called a watermark on the surface of the work. Highly clean and dry.

【0014】したがって、従来、問題となっていた乾燥
の際の異物の付着をなくし、可燃性のイソプロピルアル
コールの使用を不要にし、安全性を向上させることがで
きる。
Therefore, it is possible to improve the safety by eliminating the adhesion of foreign matter during drying, which has been a problem in the past, and by eliminating the use of flammable isopropyl alcohol.

【0015】[0015]

【実施例】図1は本発明の一実施例である真空乾燥装置
を備えた洗浄乾燥システムを示す断面図である。
FIG. 1 is a sectional view showing a cleaning / drying system equipped with a vacuum dryer according to an embodiment of the present invention.

【0016】半導体ウエハの洗浄乾燥を行う洗浄乾燥シ
ステムは、ケーシングCの内部に順次隣接して配置され
るローダ部1と、洗浄部2と、乾燥部3と、アンローダ
部4とから構成されている。
The cleaning / drying system for cleaning / drying a semiconductor wafer is composed of a loader section 1, a cleaning section 2, a drying section 3 and an unloader section 4 which are sequentially arranged inside the casing C so as to be adjacent to each other. There is.

【0017】前記ローダ部1は搬送機構または作業者に
より搬送される半導体ウエハ11を1枚以上収納する収
納治具10aがアッパフロア16上にセットされる構造
となっている。
The loader unit 1 has a structure in which a storage jig 10a for storing one or more semiconductor wafers 11 transferred by a transfer mechanism or an operator is set on the upper floor 16.

【0018】前記洗浄部2は、超純水5をオーバーフロ
ーさせる洗浄槽6がロアフロア17上に配置され、この
洗浄槽6内の超純水5に搬送機構により半導体ウエハ1
1を浸積させて洗浄を行う構造となっている。
In the cleaning unit 2, a cleaning tank 6 for overflowing the ultrapure water 5 is arranged on the lower floor 17, and the semiconductor wafer 1 is transferred to the ultrapure water 5 in the cleaning tank 6 by a transfer mechanism.
1 has been soaked for cleaning.

【0019】前記アンローダ部4は、搬送機構または作
業者により搬送される高清浄なウエハ収納治具10bが
アッパフロア16上にセットされており、乾燥が終了し
た高清浄な半導体ウエハ11は搬送機構により高清浄な
ウエハ収納治具10bに収納される構造となっている。
In the unloader section 4, a highly clean wafer storage jig 10b transported by a transport mechanism or an operator is set on the upper floor 16, and a highly clean semiconductor wafer 11 which has been dried is transported by the transport mechanism. The structure is such that the wafer is stored in a highly clean wafer storage jig 10b.

【0020】本実施例における真空乾燥装置は、前記洗
浄部2に隣接した設けられた乾燥部3に適用したもので
ある。
The vacuum drying apparatus in this embodiment is applied to the drying section 3 provided adjacent to the cleaning section 2.

【0021】すなわち、この乾燥部3は、ロアフロア1
7に配置される乾燥チャンバ3aを備え、この乾燥チャ
ンバ3aの開口端部は蓋で覆われ、乾燥中は密閉される
構造となっている。
That is, the drying section 3 is the lower floor 1
7 is provided with a drying chamber 3a, the open end of the drying chamber 3a is covered with a lid, and the drying chamber 3a is sealed during drying.

【0022】また、乾燥チャンバ3aには、液化N2
液化He等の不活性ガス12を供給する液化不活性ガス
供給部7および真空ポンプ8が配管15を介して接続さ
れ、洗浄により半導体ウエハ11を清浄に保った状態で
半導体ウエハ11に付着した水滴13を急冷却して氷化
させ、半導体ウエハ11の雰囲気を真空状態にして氷化
した氷14を昇華させて半導体ウエハ11を乾燥する構
造となっている。
Further, a liquefied inert gas supply unit 7 for supplying an inert gas 12 such as liquefied N 2 or liquefied He and a vacuum pump 8 are connected to the drying chamber 3a through a pipe 15, and the semiconductor wafer is cleaned by cleaning. While keeping 11 clean, the water droplets 13 attached to the semiconductor wafer 11 are rapidly cooled to be iced, and the atmosphere of the semiconductor wafer 11 is brought to a vacuum state to sublimate the iced ice 14 to dry the semiconductor wafer 11. It has a structure.

【0023】次に、本実施例の作用について説明する。Next, the operation of this embodiment will be described.

【0024】半導体ウエハ11の洗浄乾燥処理を行う場
合、半導体ウエハ11を1枚以上収納したウエハ収納治
具10aが搬送機構によりローダ部1にセットされると
前記ウエハ収納治具10aから半導体ウエハ11のみが
搬送機構により取り出され、洗浄部2に搬送される。
When the semiconductor wafer 11 is washed and dried, when the wafer storage jig 10a containing one or more semiconductor wafers 11 is set in the loader section 1 by the transfer mechanism, the semiconductor wafer 11 is removed from the wafer storage jig 10a. Only the carrier is taken out by the transfer mechanism and transferred to the cleaning unit 2.

【0025】洗浄部2では、半導体ウエハ11は超純水
5をオーバーフローさせた洗浄槽6で洗浄され、表面が
清浄化される。洗浄済の半導体ウエハ11は搬送機構に
より乾燥部3に搬送される。
In the cleaning unit 2, the semiconductor wafer 11 is cleaned in the cleaning tank 6 in which the ultrapure water 5 has overflowed to clean the surface. The cleaned semiconductor wafer 11 is transferred to the drying unit 3 by the transfer mechanism.

【0026】乾燥部3では、乾燥チャンバ3aに洗浄済
の半導体ウエハ11が収納され、蓋9で密閉される。半
導体ウエハ11に付着した水滴13は、液化不活性ガス
供給部7から供給される不活性ガス12によって急冷却
され、氷14となる。
In the drying section 3, the cleaned semiconductor wafer 11 is housed in the drying chamber 3a and sealed with the lid 9. The water droplets 13 attached to the semiconductor wafer 11 are rapidly cooled by the inert gas 12 supplied from the liquefied inert gas supply unit 7 to become ice 14.

【0027】その後、半導体ウエハ11の雰囲気は真空
ポンプ8によって真空状態にされ、半導体ウエハ11に
付着した氷14は昇華され、半導体ウエハ1は乾燥さ
れ、搬送機構によりアンローダ部4に搬送される。
After that, the atmosphere of the semiconductor wafer 11 is evacuated by the vacuum pump 8, the ice 14 adhering to the semiconductor wafer 11 is sublimated, the semiconductor wafer 1 is dried, and the semiconductor wafer 1 is transferred to the unloader section 4 by the transfer mechanism.

【0028】アンローダ部4では、乾燥を終了した高清
浄な半導体ウエハ11は搬送機構により高清浄なウエハ
収納治具10bに収納され、洗浄乾燥処理を終了する。
In the unloader section 4, the highly clean semiconductor wafer 11 that has been dried is stored in the highly clean wafer storage jig 10b by the transfer mechanism, and the cleaning / drying process is completed.

【0029】このように、半導体ウエハ11を清浄に保
った状態で半導体ウエハ11に付着した水滴13を急冷
却して氷14とし、半導体ウエハ11の雰囲気を真空状
態にして半導体ウエハ11に付着した氷14を昇華させ
ることにより、半導体ウエハ11の表面にウォーターマ
ークと呼ばれるシミ等を残さずに半導体ウエハ11を高
清浄に乾燥することができる。
As described above, while the semiconductor wafer 11 is kept clean, the water droplets 13 attached to the semiconductor wafer 11 are rapidly cooled to form ice 14, and the atmosphere of the semiconductor wafer 11 is vacuumed to be attached to the semiconductor wafer 11. By sublimating the ice 14, the semiconductor wafer 11 can be highly cleanly dried without leaving a stain called a watermark on the surface of the semiconductor wafer 11.

【0030】したがって、従来、問題となっていた乾燥
の際の異物の付着をなくし、可燃性のイソプロピルアル
コールの使用を不要にし、安全性を向上させることがで
きる。
Therefore, it is possible to improve the safety by eliminating the adhesion of foreign matter during the drying, which has been a problem in the past, and by eliminating the use of flammable isopropyl alcohol.

【0031】以上本発明者によってなされた発明を実施
例に基づき具体的に説明したが、本発明は前記実施例に
限定されるものではなく、その要旨を逸脱しない範囲で
種々変更可能であることはいうまでもない。
Although the invention made by the present inventor has been specifically described based on the embodiments, the present invention is not limited to the embodiments and various modifications can be made without departing from the scope of the invention. Needless to say.

【0032】たとえば、前記実施例では、洗浄部に超純
水をオーバーフローさせる洗浄槽を設けた場合について
説明したが、これに限らず、純水を蒸気化させ、半導体
ウエハを蒸気洗浄する蒸気洗浄ユニットを設けることも
できる。
For example, in the above-described embodiment, the case where the cleaning section is provided with a cleaning tank for overflowing ultrapure water has been described, but the invention is not limited to this, and steam cleaning in which pure water is vaporized and semiconductor wafers are vapor-cleaned Units can also be provided.

【0033】また、真空ポンプとして、荒引きポンプと
ターボ分子ポンプなどのドライポンプとの組み合わせた
ものを使用し、オイルミストの混入を防止することもで
きる。
Further, as the vacuum pump, a combination of a roughing pump and a dry pump such as a turbo molecular pump can be used to prevent mixing of oil mist.

【0034】また、半導体ウエハとウエハ収納治具とを
一緒に洗浄乾燥しても良い。
The semiconductor wafer and the wafer storage jig may be washed and dried together.

【0035】また、ローダ部と洗浄部との間に無機薬品
や有機溶剤による薬品洗浄部を設け、半導体ウエハの洗
浄乾燥を一貫処理することもできる。
Further, a chemical cleaning section using an inorganic chemical or an organic solvent may be provided between the loader section and the cleaning section so that cleaning and drying of the semiconductor wafer can be carried out consistently.

【0036】以上の説明では、主として本発明者によっ
てなされた発明をその背景となった利用分野である、半
導体ウエハの真空乾燥方法および装置で説明したが、他
の電子部品の真空乾燥方法および装置にも適用できる。
In the above description, the invention made by the present inventor was mainly described in the background of the field of application, which is the method and apparatus for vacuum drying semiconductor wafers. However, the method and apparatus for vacuum drying other electronic components are described. Can also be applied to.

【0037】[0037]

【発明の効果】本願において開示される発明のうち、代
表的なものによって得られる効果を簡単に説明すれば、
以下のとおりである。
The effects obtained by the typical ones of the inventions disclosed in the present application will be briefly described as follows.
It is as follows.

【0038】(1).ワークに付着した水滴もしくは水分を
急冷却して氷化させ、ワークの雰囲気を真空状態にして
氷化した氷を昇華させてワークを乾燥する真空乾燥方法
および装置としたので、ワークの表面にウォーターマー
クと呼ばれるシミ等を残さずにワークを高清浄に乾燥す
ることができる。
(1). A vacuum drying method and apparatus for rapidly cooling water droplets or water adhering to a work to be iced, bringing the atmosphere of the work into a vacuum state and sublimating the iced ice to dry the work. Therefore, the work can be highly cleanly dried without leaving a stain called a watermark on the surface of the work.

【0039】(2).前記(1) の効果により、従来、問題と
なっていた乾燥の際の異物の付着をなくし、可燃性のイ
ソプロピルアルコールの使用を不要にし、安全性を向上
させることができる。
(2) Due to the effect of the above (1), it is possible to eliminate the adhesion of foreign matter during drying, which has been a problem in the past, and to eliminate the use of flammable isopropyl alcohol, thereby improving safety. it can.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施例である乾燥装置を備えた洗浄
乾燥システムを示す断面図である。
FIG. 1 is a cross-sectional view showing a cleaning / drying system including a drying device according to an embodiment of the present invention.

【符号の説明】[Explanation of symbols]

1 ローダ部 2 洗浄部 3 乾燥部 3a 乾燥チャンバ 4 アンローダ部 5 超純水 6 洗浄槽 7 液化不活性ガス供給部 8 真空ポンプ 9 蓋 10a ウエハ収納治具 10b ウエハ収納治具 11 半導体ウエハ 12 不活性ガス 13 水滴 14 氷 15 配管 16 アッパフロア 17 ロアフロア C ケーシング DESCRIPTION OF SYMBOLS 1 loader section 2 cleaning section 3 drying section 3a drying chamber 4 unloader section 5 ultrapure water 6 cleaning tank 7 liquefied inert gas supply section 8 vacuum pump 9 lid 10a wafer storage jig 10b wafer storage jig 11 semiconductor wafer 12 inert Gas 13 Water drops 14 Ice 15 Piping 16 Upper floor 17 Lower floor C Casing

───────────────────────────────────────────────────── フロントページの続き (72)発明者 野口 雄二 東京都小平市上水本町5丁目20番1号 株 式会社日立製作所武蔵工場内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Inventor Yuji Noguchi 5-20-1 Kamimizuhonmachi, Kodaira-shi, Tokyo Hitachi, Ltd. Musashi Factory

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 ワークに付着した水滴もしくは水分を急
冷却して氷化させ、ワークの雰囲気を真空状態にして氷
化した氷を昇華させてワークを乾燥することを特徴とす
る真空乾燥方法。
1. A vacuum drying method, characterized in that water droplets or water attached to a work is rapidly cooled to be iced, the atmosphere of the work is brought to a vacuum state to sublimate the iced ice, and the work is dried.
【請求項2】 ワークに付着した水滴もしくは水分を急
冷却して氷化させる冷却手段と、前記氷化したワークの
雰囲気を真空状態にする真空手段とを備えたことを特徴
とする真空乾燥装置。
2. A vacuum drying apparatus comprising: a cooling means for rapidly cooling water droplets or water attached to a work to be frozen, and a vacuum means for bringing an atmosphere of the frozen work into a vacuum state. ..
【請求項3】 前記冷却手段に液化不活性ガスを用いた
ことを特徴とする請求項2の真空乾燥装置。
3. The vacuum drying apparatus according to claim 2, wherein a liquefied inert gas is used for the cooling means.
JP6173892A 1992-03-18 1992-03-18 Method and apparatus for vacuum drying Pending JPH05267269A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP6173892A JPH05267269A (en) 1992-03-18 1992-03-18 Method and apparatus for vacuum drying

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6173892A JPH05267269A (en) 1992-03-18 1992-03-18 Method and apparatus for vacuum drying

Publications (1)

Publication Number Publication Date
JPH05267269A true JPH05267269A (en) 1993-10-15

Family

ID=13179837

Family Applications (1)

Application Number Title Priority Date Filing Date
JP6173892A Pending JPH05267269A (en) 1992-03-18 1992-03-18 Method and apparatus for vacuum drying

Country Status (1)

Country Link
JP (1) JPH05267269A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007111269A1 (en) * 2006-03-24 2007-10-04 Central Research Institute Of Electric Power Industry Method of removing ice from ice-containing material with use of liquefied substance
JP2012015450A (en) * 2010-07-05 2012-01-19 Three M Innovative Properties Co Method for drying surface structure
JP2012074564A (en) * 2010-09-29 2012-04-12 Dainippon Screen Mfg Co Ltd Substrate processing apparatus and substrate processing method
JP2013201302A (en) * 2012-03-26 2013-10-03 Dainippon Screen Mfg Co Ltd Substrate processing apparatus and substrate processing method

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007111269A1 (en) * 2006-03-24 2007-10-04 Central Research Institute Of Electric Power Industry Method of removing ice from ice-containing material with use of liquefied substance
JP4734406B2 (en) * 2006-03-24 2011-07-27 財団法人電力中央研究所 Method for removing ice from ice-containing material using liquefied material
JP2012015450A (en) * 2010-07-05 2012-01-19 Three M Innovative Properties Co Method for drying surface structure
JP2012074564A (en) * 2010-09-29 2012-04-12 Dainippon Screen Mfg Co Ltd Substrate processing apparatus and substrate processing method
US9922848B2 (en) 2010-09-29 2018-03-20 SCREEN Holdings Co., Ltd. Apparatus for and method of processing substrate
JP2013201302A (en) * 2012-03-26 2013-10-03 Dainippon Screen Mfg Co Ltd Substrate processing apparatus and substrate processing method

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