JPH0211577B2 - - Google Patents

Info

Publication number: JPH0211577B2
Authority: JP; Japan
Prior art keywords: liquid; thin film; reaction; ester; heater
Prior art date: 1985-06-07
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

JP60123988A

Other languages

English (en)

Japanese (ja)

Other versions

JPS61282340A (ja

Inventor

Sadao Kobayashi

Ryoji Nakatsu

Hiroo Okada

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Kao Corp

Original Assignee

Kao Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-06-07

Filing date

1985-06-07

Publication date

1990-03-14

1985-06-07 Application filed by Kao Corp filed Critical Kao Corp

1985-06-07 Priority to JP12398885A priority Critical patent/JPS61282340A/ja

1986-12-12 Publication of JPS61282340A publication Critical patent/JPS61282340A/ja

1990-03-14 Publication of JPH0211577B2 publication Critical patent/JPH0211577B2/ja

Status Granted legal-status Critical Current

Links

239000007788 liquid Substances 0.000 claims description 64
150000002148 esters Chemical class 0.000 claims description 50
239000010409 thin film Substances 0.000 claims description 44
238000006243 chemical reaction Methods 0.000 claims description 36
239000012295 chemical reaction liquid Substances 0.000 claims description 22
238000004519 manufacturing process Methods 0.000 claims description 12
150000005846 sugar alcohols Polymers 0.000 claims description 10
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
239000002253 acid Substances 0.000 claims description 8
238000003756 stirring Methods 0.000 claims description 7
238000005809 transesterification reaction Methods 0.000 claims description 7
238000010438 heat treatment Methods 0.000 claims description 3
239000002994 raw material Substances 0.000 description 10
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
230000000052 comparative effect Effects 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
230000000694 effects Effects 0.000 description 5
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 4
KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 4
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 4
239000005642 Oleic acid Substances 0.000 description 4
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 4
238000001816 cooling Methods 0.000 description 4
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 4
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 4
230000035484 reaction time Effects 0.000 description 4
238000005886 esterification reaction Methods 0.000 description 3
235000011187 glycerol Nutrition 0.000 description 3
238000000034 method Methods 0.000 description 3
LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 2
241001550224 Apha Species 0.000 description 2
235000021355 Stearic acid Nutrition 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
238000007796 conventional method Methods 0.000 description 2
239000000284 extract Substances 0.000 description 2
150000002763 monocarboxylic acids Chemical class 0.000 description 2
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
239000007858 starting material Substances 0.000 description 2
239000008117 stearic acid Substances 0.000 description 2
UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 2
FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
238000004040 coloring Methods 0.000 description 1
230000032050 esterification Effects 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000000376 reactant Substances 0.000 description 1
238000013341 scale-up Methods 0.000 description 1
238000004904 shortening Methods 0.000 description 1
239000000600 sorbitol Substances 0.000 description 1
150000003626 triacylglycerols Chemical class 0.000 description 1
238000009834 vaporization Methods 0.000 description 1
230000008016 vaporization Effects 0.000 description 1
238000003809 water extraction Methods 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/2425—Tubular reactors in parallel
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Physical Or Chemical Processes And Apparatus (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Fats And Perfumes (AREA)

JP12398885A 1985-06-07 1985-06-07 エステルの製造装置 Granted JPS61282340A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP12398885A JPS61282340A (ja)	1985-06-07	1985-06-07	エステルの製造装置

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP12398885A JPS61282340A (ja)	1985-06-07	1985-06-07	エステルの製造装置

Publications (2)

Publication Number	Publication Date
JPS61282340A JPS61282340A (ja)	1986-12-12
JPH0211577B2 true JPH0211577B2 (fr)	1990-03-14

Family

ID=14874260

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP12398885A Granted JPS61282340A (ja)	1985-06-07	1985-06-07	エステルの製造装置

Country Status (1)

Country	Link
JP (1)	JPS61282340A (fr)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR1534622A (fr) *	1967-08-24	1968-07-26	Hydrierwerk Rodleben Veb	Procédé pour l'estérification
DE2015174A1 (de) *	1969-04-01	1970-10-08	Allied Chemical Corp., New York, N.Y. (V.St.A.)	Verfahren zur Herstellung linearer Polyester

1985
- 1985-06-07 JP JP12398885A patent/JPS61282340A/ja active Granted

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR1534622A (fr) *	1967-08-24	1968-07-26	Hydrierwerk Rodleben Veb	Procédé pour l'estérification
DE2015174A1 (de) *	1969-04-01	1970-10-08	Allied Chemical Corp., New York, N.Y. (V.St.A.)	Verfahren zur Herstellung linearer Polyester

Also Published As

Publication number	Publication date
JPS61282340A (ja)	1986-12-12

Legal Events

Date	Code	Title	Description
2004-02-24	R250	Receipt of annual fees	Free format text: JAPANESE INTERMEDIATE CODE: R250
2005-03-14	LAPS	Cancellation because of no payment of annual fees

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