JP7520001B2 - アクリレート系共重合体、該共重合体の製造方法、該共重合体からなる摩擦抑制剤及び該摩擦抑制剤を含有する潤滑油組成物 - Google Patents
アクリレート系共重合体、該共重合体の製造方法、該共重合体からなる摩擦抑制剤及び該摩擦抑制剤を含有する潤滑油組成物 Download PDFInfo
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- JP7520001B2 JP7520001B2 JP2021524844A JP2021524844A JP7520001B2 JP 7520001 B2 JP7520001 B2 JP 7520001B2 JP 2021524844 A JP2021524844 A JP 2021524844A JP 2021524844 A JP2021524844 A JP 2021524844A JP 7520001 B2 JP7520001 B2 JP 7520001B2
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- 229920001577 copolymer Polymers 0.000 title claims description 127
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- 125000004432 carbon atom Chemical group C* 0.000 claims description 51
- 125000000217 alkyl group Chemical group 0.000 claims description 45
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- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 1
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- 125000005040 tridecenyl group Chemical group C(=CCCCCCCCCCCC)* 0.000 description 1
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- QOQNJVLFFRMJTQ-UHFFFAOYSA-N trioctyl phosphite Chemical compound CCCCCCCCOP(OCCCCCCCC)OCCCCCCCC QOQNJVLFFRMJTQ-UHFFFAOYSA-N 0.000 description 1
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Classifications
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Description
これらの中でも、ポリ-α-オレフィン、ポリイソブチレン(ポリブテン)、ジエステル及びポリオールエステル等の化学合成基油を含む基油が好ましく、ポリ-α-オレフィン等の炭化水素油を含む基油がより好ましく、これらの基油の高度精製基油を用いることがさらに好ましい。
・重合性単量体(a)
(a-i):一般式(1)において、R1が炭素数12のアルキル基であり、A1が水素原子である重合性単量体
・重合性単量体(b)
(b-i):一般式(2)において、R2がエチレン基であり、R3がメチル基であり、A2が水素原子であり、nが11~15(平均値は13)である重合性単量体
・重合性単量体(c-1)
(c-1-i):一般式(4)において、R5がメチレン基であり、A4が水素原子である重合性単量体
・重合性単量体(c-2)
(c-2-i):一般式(3)において、R4がエチル基であり、A3が水素原子である重合性単量体
・その他の重合性単量体(d)
(d-i):一般式(5)において、R6がエチレン基であり、A5が水素原子である重合性単量体
(d-ii): ラウリルメタクリレート
(d-iii): エチルメタクリレート
反応容器中に、溶媒として1,4-ジオキサン108g、高度精製鉱物油(100℃動粘度3.12mm2/s、粘度指数112)108gを投入し、85℃に昇温した。そこに、重合性単量体として重合性単量体(a-i)25.0g、重合性単量体(b-i)62.8g、重合性単量体(c-1-i)20.5g、2,2-アゾビスイソブチロニトリル0.19g及び1,1-アゾビスシクロヘキサン-1-カルボニトリル0.51gを滴下し、4時間攪拌することで重合反応を行い、アクリレート系共重合体を製造した。その後、115~125℃に昇温しながら減圧(0.2~1.0kPa)することで1,4-ジオキサンを除去し、アクリレート系共重合体溶液を調製した。得られたアクリレート系共重合体中の各重合性単量体の構成比率を表1に示す。
実施例1で製造したアクリレート系共重合体(アクリレート系共重合体1)を摩擦抑制剤として用い、摩擦特性評価を行った。具体的には、基油1としてのエンジンオイル(100℃動粘度7.2mm2/s、粘度指数167)と、アクリレート系共重合体1とを、アクリレート系共重合体の含有量が潤滑油組成物全量に対して0.25質量%となるよう添加し、潤滑油組成物1を調製した。得られた潤滑油組成物1についてPCS Instruments社製MTM試験機を用い、下記試験条件により摩擦係数を測定した。摩擦係数は、試験終了前の5分間の摩擦係数の平均値を用いた。測定結果を表1に示す。
荷重:36N
転がり速度:50mm/s
すべり率:50%
試験温度:100℃
試験時間:120分
実施例2~7及び比較例1~3としてそれぞれ、実施例1において、用いる重合性単量体の種類及び使用量を変更した以外は同様の方法により、表1の重合性単量体構成比であるアクリレート系共重合体を製造した。実施例2~7及び比較例1~3で製造したアクリレート系共重合体(アクリレート系共重合体2~10)について、それぞれ実施例1と同様の方法により摩擦係数を測定した。結果をそれぞれ表1に示す。また、比較例4として、アクリレート系共重合体を含まず、基油1のみからなる潤滑油組成物についても実施例1と同様の方法により摩擦係数を測定した。結果を表1に示す。
本発明のアクリレート系共重合体と、下記の基油、摩擦低減剤、摩耗防止剤、清浄剤、無灰分散剤を用いて調製される燃料油組成物の配合例を表2~8に示す。なお、モリブデンジチオカルバメートの配合量はMo元素換算量、ジチオリン酸亜鉛の配合量はP元素換算量、カルシウム系清浄剤の配合量はCa元素換算量、マグネシウム系清浄剤の配合量はMg元素換算量で表す。
基油3:高度精製鉱物油(100℃動粘度10.4mm2/s、粘度指数112)
基油4:αオレフィン系合成油(100℃動粘度1.7mm2/s、粘度指数91)
基油5:高度精製鉱物油(100℃動粘度4.2mm2/s、粘度指数134)
基油6:高度精製鉱物油(100℃動粘度3.1mm2/s、粘度指数105)
基油7:αオレフィン系合成油(100℃動粘度4.1mm2/s、粘度指数126)
摩擦低減剤1:一般式(6)において、R7、R8が炭素数8のアルキル基であり、R9、R10が炭素数13のアルキル基であり、X1及びX2が硫黄原子でありX3及びX4が酸素原子であるモリブデンジチオカルバメート
摩擦低減剤2:一般式(6)において、R7~R10が炭素数13のアルキル基でありX1及びX2が硫黄原子でありX3及びX4が酸素原子であるモリブデンジチオカルバメート
摩耗防止剤1:一般式(7)において、R11~R14が炭素数4のアルキル基であるジチオリン酸亜鉛
摩耗防止剤2:一般式(7)において、R11~R14が炭素数8のアルキル基であるジチオリン酸亜鉛
摩耗防止剤3:一般式(7)において、R11~R14が炭素数4又は6のアルキル基であるジチオリン酸亜鉛
清浄剤1:108mgKOH/gのカルシウムサリシレート
清浄剤2:220mgKOH/gのカルシウムサリシレート
清浄剤3:341mgKOH/gのカルシウムサリシレート
清浄剤4:201mgKOH/gのカルシウムスルホネート
清浄剤5:142mgKOH/gのマグネシウムサリシレート
清浄剤6:185mgKOH/gのマグネシウムスルホネート
清浄剤7:321mgKOH/gのマグネシウムスルホネート
無灰分散剤1:窒素含有量2.0重量%の非ホウ素化アルケニルコハク酸イミド
無灰分散剤2:窒素含有量1.1重量%、ホウ素原子含有量0.9重量%のホウ素化アルケニルコハク酸イミド
無灰分散剤3:窒素含有量2.7重量%、ホウ素原子含有量2.0重量%のホウ素化アルケニルコハク酸イミド
Claims (10)
- 下記の一般式(1)で表されるアルキルアクリレート系単量体からなる重合性単量体(a)を構成単量体の全モル数に対して10~95モル%、下記の一般式(2)で表されるアルキレングリコールアクリレート系単量体からなる重合性単量体(b)を構成単量体の全モル数に対して5~50モル%、並びに芳香族ビニル系単量体(c-1)及び下記の一般式(3)で表される短鎖アルキルアクリレート系単量体(c-2)からなる群から選ばれる少なくとも1種の重合性単量体(c)を構成単量体の全モル数に対して0~60モル%で含む構成単量体を重合して得られるアクリレート系共重合体からなる摩擦抑制剤。
- 重合性単量体(b)として、一般式(2)において、R3が水素原子又は炭素数1~6のアルキル基であり、nが6~20であるアルキレングリコールアクリレート系単量体を含む、請求項1又は2に記載の摩擦抑制剤。
- 芳香族ビニル系単量体(c-1)の構成比率が前記構成単量体の全モル数に対して5~60モル%である、請求項1~3のいずれか1項に記載の摩擦抑制剤。
- 前記構成単量体中の、アルキレングリコールアクリレート系単量体(b)と芳香族ビニル系単量体(c-1)との構成比率の比が、モル比で10:90~100:0である、請求項1~4のいずれか1項に記載の摩擦抑制剤。
- 請求項1~7のいずれか1項に記載の摩擦抑制剤と、基油とを含有する潤滑油組成物。
- 下記の一般式(1)で表されるアルキルアクリレート系単量体からなる重合性単量体(a)を構成単量体の全モル数に対して10~95モル%、下記の一般式(2)で表されるアルキレングリコールアクリレート系単量体からなる重合性単量体(b)を構成単量体の全モル数に対して5~50モル%、並びに芳香族ビニル系単量体(c-1)及び下記の一般式(3)で表される短鎖アルキルアクリレート系単量体(c-2)からなる群から選ばれる少なくとも1種の重合性単量体(c)を構成単量体の全モル数に対して0~60モル%で含む構成単量体を重合することを含む、アクリレート系共重合体からなる摩擦抑制剤の製造方法。
- 基油に請求項1~7のいずれか1項に記載の摩擦抑制剤を添加することを含む、基油の摩擦を抑制する方法。
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