JP7499478B2 - 化粧料インク、これを含むインクジェット用インク、およびインクカートリッジ、ならびに化粧用シートの製造方法 - Google Patents
化粧料インク、これを含むインクジェット用インク、およびインクカートリッジ、ならびに化粧用シートの製造方法 Download PDFInfo
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- JP7499478B2 JP7499478B2 JP2023017121A JP2023017121A JP7499478B2 JP 7499478 B2 JP7499478 B2 JP 7499478B2 JP 2023017121 A JP2023017121 A JP 2023017121A JP 2023017121 A JP2023017121 A JP 2023017121A JP 7499478 B2 JP7499478 B2 JP 7499478B2
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- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 1
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- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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Description
本開示の化粧料インクは、化粧用シートを作製するためのインクである。当該インクを用いて作製される化粧用シートは、例えば肌に貼着して用いられ、肌の彩色や、美化等に用いられる。ただし、当該化粧料インクは、メイクアップ等の化粧用途のみならず、日焼け止め等のスキンケア用途、医療用途、さらにはプラスチックフィルムの加飾等の工業的な用途にも利用可能である。
化粧料インクに含まれる(A)色材は、上述の分光反射率を実現することが可能であれば特に制限されない。通常、複数種類の色材が組み合わせて用いられる。例えば、白色系色材、赤色系色材、および黄色系色材を少なくとも組み合わせることで、上述の分光反射率が実現されやすくなる。より具体的には、白色系色材は、(A)色材の総量100質量部に対して60~99.8質量部含まれることが好ましい。また、(A)色材の総量100質量部に対して、赤色系色材は0.1~30質量部含まれることが好ましい。また、(A)色材の総量100質量部に対して、黄色系色材は0.1~30質量部含まれることが好ましい。
本開示の化粧料インクに含まれる高級アルコールは、炭素数が3以上であり、(C)精製水と相溶する高級アルコールであれば特に制限されない。(B)高級アルコールは化粧料インクの溶媒としての機能を果たす。なお、(B)高級アルコールは、化粧料インクを被印刷体に印刷した後、被印刷体に吸収されたり、揮発したりする。
本開示の化粧料インクには、(C)精製水が含まれる。(C)精製水も化粧料インクの溶媒としての機能を果たし、(C)精製水は、化粧料インクを被印刷体に印刷した後、被印刷体に吸収されたり、揮発したりする。
本開示の化粧料インクには、(D)バインダが含まれる。(D)バインダは、上述の(A)色材等を、被印刷体に結着するための化合物である。本開示の化粧料インクでは、「バインダ」が、(B)高級アルコールおよび(C)精製水に不溶の粒子状の樹脂であることが好ましい。化粧料インクには、(D)バインダが一種のみ含まれていてもよく、二種以上含まれていてもよい。
本開示の化粧料インクには、上述のように、必要に応じて皮膜形成剤や各種添加剤等がさらに含まれていてもよい。
上述の化粧料インクは、(A)色材、(B)高級アルコール、および(C)精製水と、(D)バインダを含むスラリーもしくは分散液と、必要に応じて他の成分とを分散機で混合すること等により得られる。各成分の混合は、公知のボールミル、サンドミル、ロールミル、ホモミキサー、アトライターなど分散機等で行うことができる。
上述の化粧料インクは、コーンプレート型粘度計にて、速度1000(1/s)で測定したときの25℃における粘度が、50mPa・s以下であることが好ましく、1~20mPa・sであることがより好ましく、3.5~8mPa・sであることがさらに好ましい。化粧料インクの粘度が上記範囲であると、化粧料インクを、各種印刷装置を用いて印刷しやすくなる。また特に、粘度が上記範囲であると、インクジェット装置からから安定して吐出しやすくなる。
上述の化粧料インクは、例えばカートリッジに充填して保存することができる。カートリッジの種類や構造は特に制限されず、化粧料インクを印刷するための印刷装置に合わせて適宜選択される。このようなインクカートリッジの一例として、化粧料インクを収容するためのインク収容部と、インクを印刷装置の記録ヘッドに供給するためのインク供給口と、を有するカートリッジが挙げられる。
2-1.上述の化粧料インクを用いた化粧用シートの製造方法
上述の化粧料インクを被印刷体に印刷する工程と、被印刷体に塗布された化粧料インクを乾燥させる工程と、を含む製造方法により、化粧シートを製造することができる。
また化粧シートは、白色インク、赤色インク、黄色インク、青色インク、および黒色インクからなる群から選ばれる3色以上のインクの液滴をずらした位置に塗布して塗膜を形成する塗膜形成工程と、被印刷体に塗布された化粧料インクを乾燥させる乾燥工程と、を含む製造方法により、製造することもできる。なお、乾燥工程については、上述の化粧料インクを用いた化粧用シートの製造方法における乾燥工程と同様とすることができるため、以下、塗膜形成工程についてのみ説明する。
1-1.材料
各実施例および比較例に用いた材料は、以下の通りである。なお、各粒子の平均粒子径は、レーザ回折法で測定される粒度分布の積算値の中央値(D50)の値である。
(A)色材
赤色系色材:無機赤色系顔料(平均粒子径:150nm)
黄色系色材:無機黄色系顔料(平均粒子径:150nm)
青色系色材:無機青色系顔料(平均粒子径:150nm)
黒色系色材:無機黒色系顔料(平均粒子径:150nm)
白色系色材:無機白色系顔料(平均粒子径:120nm)
(B)高級アルコール
グリセリン
1,3-プロパンジオール
(C)精製水
(D)バインダ
アクリル系ポリマー粒子(平均粒子径:50nm)
下記表1および表2に示す成分比で、各材料を混合し、化粧料インクを調製した。なお、表1には、(A)色材に含まれる各色色材の量の質量比も併せて示す。
上記化粧料インクの物性について、以下の方法で評価を行った。結果を表1および表2に示す。また、図1および図2に、各化粧料インクの分光反射率曲線、肌模型の分光反射率曲線、人の肌(頬および腕の内側)の分光反射率曲線を示す。
化粧料インクの粘度は、コーンプレート型粘度計にて、25℃、せん断速度1000(1/s)にて測定した。化粧料インクのpHは、pHメータ(LAQUAtwin HORIBA社製)により測定した。化粧料インクの表面張力は、接触角計(DropMaster DM-501、協和界面化学社製)で測定した。
分光反射率および明度(L*値)は、化粧料インクから得られる塗膜について、波長400nm~700nmの範囲、分光測色計(例えば、コニカミノルタ社製 CM-700d)により、主光源:D50、測定モード:SCEで測定した値である。
上記化粧料インクA-1、A-3、A-12、および上記A-2とA-10とを1:1で混合した化粧料インクA-20を、パナソニックプレシジョンデバイス株式会社製LB3インクジェットヘッドを備えるインクジェット装置のインクタンクに充填した。なお、化粧料インクA-20について、上述と同様に、塗膜の分光反射率曲線を確認したところ、分光反射率曲線が、波長550nm以上波長610nm以下の領域に第1の変曲点が存在し、波長550nm未満の領域に第2の変曲点が存在していた。また、これらの化粧料インクでは、第1の変曲点における分光反射率が、第2の変曲点における分光反射率より高かった。さらに、これらの化粧料インクでは、波長580nm超の領域における分光反射率がいずれも、波長580nmにおける分光反射率以上であった。
また、色差ΔE*abについて、以下の基準で評価した。なお、評価C以上が実用上問題ないレベルである。
AA:色差ΔE*abが0.8以上1.6未満
A:色差ΔE*abが1.6以上3.2未満
B:色差ΔE*abが3.2以上6.5未満
C:色差ΔE*abが6.5以上13.0未満
D:色差ΔE*abが13.0以上25.0未満
◎:官能的に肌模型と完全に同じ色
○:官能的には肌模型と同じ色であるが、凝視すると極めて類似する異なる色味
2-1.材料
各実施例および比較例に用いた材料は、以下の通りである。
(A)色材
赤色系色材:無機赤色系顔料(平均粒子径:150nm)
黄色系色材:無機黄色系顔料(平均粒子径:150nm)
青色系色材:無機青色系顔料(平均粒子径:150nm)
黒色系色材:無機黒色系顔料(平均粒子径:150nm)
白色系色材:無機白色系顔料(平均粒子径:120nm)
(B)高級アルコール
グリセリン
1,3-プロパンジオール
(C)精製水
(D)バインダ
アクリル系ポリマー粒子(平均粒子径:50nm)
色材をそれぞれ1種ずつ含めた以外は、実施例1の化粧料インクと同様に、白色、赤色、黄色、青色、および黒色の化粧料用インクをそれぞれ調製した。色材の量は、各化粧料インクを塗布した際の濃さが略均一となるように、それぞれ調整した。
白色インク、赤色インク、黄色インク、青色インク、および黒色インクをそれぞれ、パナソニックプレシジョンデバイス株式会社製LB3インクジェットヘッドを備えるインクジェット装置のインクタンクに充填した。一方、厚みが200nmのポリ乳酸シートを、ろ紙からなる支持体に貼り付けた被印刷体を準備した。そして、上記化粧料インクを、ポリ乳酸シート上に塗布し、半径30mmの円形状のパターン(塗りつぶしパターン)を形成した。このとき、一色塗布するごとに、ポリ乳酸シートを適当な角度回転させて、各色インクの液滴が完全に重ならないように印刷した。またこのとき、各インクの塗布量は、各インク中に含まれる色材の量がそれぞれ、上述の実施例1の化粧料インクの顔料比率と略同等になるように調整した。印刷後のシートを50℃の環境下で乾燥させて、化粧用シートB-1(実施例)を得た。
Claims (16)
- 白色インク、赤色インク、黄色インク、青色インク、および黒色インクからなる群から選ばれる3色以上のインクの液滴をずらした位置に塗布して塗膜を形成する塗膜形成手段を含み、
前記塗膜形成手段で形成される塗膜は、
波長400nm~700nmにおける分光反射率を測定して得られる分光反射率曲線の波長550nm以上波長610nm以下の領域に第1の変曲点が存在し、波長550nm未満の領域に第2の変曲点が存在し、前記第1の変曲点における分光反射率が、前記第2の変曲点における分光反射率より高く、波長610nm以上の領域における分光反射率が、前記第1の変曲点における分光反射率以上であり、かつ波長590nm~700nmの領域における分光反射率が、波長580nmの分光反射率の1倍~1.3倍の範囲に収まり、
前記白色インク、前記赤色インク、前記黄色インク、前記青色インク、および前記黒色インクが、それぞれ、(A)色材と、(B)炭素数3以上の高級アルコールと、(C)精製水と、(D)(メタ)アクリル系モノマーの単独重合体、および二種以上の(メタ)アクリル系モノマーの共重合体のうち、少なくとも一方を含み、かつ平均粒子径が30nm~150nmである(メタ)アクリル系樹脂からなる粒子と、(E)HLB値が8以上である皮膜形成剤(ただし、(D)(メタ)アクリル系樹脂からなる粒子に相当するものを除く)と、を含む、
化粧用シートの製造装置。 - 前記塗膜形成手段で形成される塗膜のL*a*b*表色系におけるL*値が、48以上である、
請求項1に記載の化粧用シートの製造装置。 - 前記(E)皮膜形成剤のHLB値は、8~19である、
請求項1または2に記載の化粧用シートの製造装置。 - 前記(E)皮膜形成剤は、アクリル系ポリマーを含む、
請求項1または2に記載の化粧用シートの製造装置。 - 前記(A)色材が、黒色系顔料または黒色系染料を含む、
請求項1または2に記載の化粧用シートの製造装置。 - 前記(A)色材の平均粒子径が2μm以下である、
請求項1に記載の化粧用シートの製造装置。 - 前記(D)(メタ)アクリル系樹脂からなる粒子の含有量が0.1質量%以上10質量%以下である、
請求項1に記載の化粧用シートの製造装置。 - (A)白色系色材、黄色系色材、赤色系色材、および青色系色材を含む色材と、
(B)炭素数3以上の高級アルコールと、
(D)(メタ)アクリル系モノマーの単独重合体、および二種以上の(メタ)アクリル系モノマーの共重合体のうち、少なくとも一方を含み、かつ平均粒子径が30nm~150nmである(メタ)アクリル系樹脂からなる粒子と、
(E)HLB値が8以上である皮膜形成剤(ただし、(D)(メタ)アクリル系樹脂からなる粒子に相当するものを除く)と、
を含む化粧料インクの固化物からなる塗膜であり、
波長400nm~700nmの分光反射率を測定して得られる、分光反射率曲線の波長550nm以上波長610nm以下の領域には第1の変曲点が存在し、波長550nm未満の領域には第2の変曲点が存在し、
前記第1の変曲点における分光反射率が、前記第2の変曲点における分光反射率より高く、
波長580nm超の領域における分光反射率がいずれも、波長580nmにおける分光反射率以上であり、
かつ波長590nm~700nmの領域における分光反射率が、波長580nmの分光反射率の1倍~1.3倍の範囲に収まる、
塗膜。 - L*a*b*表色系におけるL*値が、48以上である、
請求項8に記載の塗膜。 - 前記(E)皮膜形成剤のHLB値は、8~19である、
請求項8または9に記載の塗膜。 - 前記(E)皮膜形成剤は、アクリル系ポリマーを含む、
請求項8または9に記載の塗膜。 - 前記(A)色材が、黒色系顔料または黒色系染料を含む、
請求項8または9に記載の塗膜。 - 前記(A)色材の平均粒子径が2μm以下である、
請求項8に記載の塗膜。 - 前記(A)色材の量を10質量部としたとき、(D)(メタ)アクリル系樹脂からなる粒子の量が0.5質量部以上10質量部以下である、
請求項8に記載の塗膜。 - 前記化粧料インクが、白色インク、赤色インク、黄色インク、青色インク、および黒色インクからなる群から選ばれる3色以上の色インクで構成され、
前記3色以上の色インクの液滴の固化物からなる、
請求項8または9に記載の塗膜。 - 各前記3色以上の色インクの液滴の固化物が、ずらした位置に配置されている、
請求項15に記載の塗膜。
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CN111182882A (zh) | 2020-05-19 |
WO2019073743A1 (ja) | 2019-04-18 |
US11767441B2 (en) | 2023-09-26 |
EP3695828A4 (en) | 2020-09-23 |
JP2023058584A (ja) | 2023-04-25 |
JPWO2019073743A1 (ja) | 2020-11-05 |
US20200216693A1 (en) | 2020-07-09 |
EP3695828A1 (en) | 2020-08-19 |
JP7233012B2 (ja) | 2023-03-06 |
SG11202002896SA (en) | 2020-04-29 |
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