JP7448134B2 - 混合システム及び材料供給装置 - Google Patents
混合システム及び材料供給装置 Download PDFInfo
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- JP7448134B2 JP7448134B2 JP2019086938A JP2019086938A JP7448134B2 JP 7448134 B2 JP7448134 B2 JP 7448134B2 JP 2019086938 A JP2019086938 A JP 2019086938A JP 2019086938 A JP2019086938 A JP 2019086938A JP 7448134 B2 JP7448134 B2 JP 7448134B2
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- OBNCKNCVKJNDBV-UHFFFAOYSA-N ethyl butyrate Chemical group CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 1
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- 229910052733 gallium Inorganic materials 0.000 description 1
- PHXATPHONSXBIL-JTQLQIEISA-N gamma-Undecalactone Natural products CCCCCCC[C@H]1CCC(=O)O1 PHXATPHONSXBIL-JTQLQIEISA-N 0.000 description 1
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- 229940020436 gamma-undecalactone Drugs 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000003349 gelling agent Substances 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
- 229910021389 graphene Inorganic materials 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
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- 150000004820 halides Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- LLEVMYXEJUDBTA-UHFFFAOYSA-N heptanedinitrile Chemical compound N#CCCCCCC#N LLEVMYXEJUDBTA-UHFFFAOYSA-N 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-M hexanoate Chemical compound CCCCCC([O-])=O FUZZWVXGSFPDMH-UHFFFAOYSA-M 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- CPSYWNLKRDURMG-UHFFFAOYSA-L hydron;manganese(2+);phosphate Chemical compound [Mn+2].OP([O-])([O-])=O CPSYWNLKRDURMG-UHFFFAOYSA-L 0.000 description 1
- MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 description 1
- 150000004693 imidazolium salts Chemical class 0.000 description 1
- KHLVKKOJDHCJMG-QDBORUFSSA-L indigo carmine Chemical compound [Na+].[Na+].N/1C2=CC=C(S([O-])(=O)=O)C=C2C(=O)C\1=C1/NC2=CC=C(S(=O)(=O)[O-])C=C2C1=O KHLVKKOJDHCJMG-QDBORUFSSA-L 0.000 description 1
- 229960003988 indigo carmine Drugs 0.000 description 1
- 235000012738 indigotine Nutrition 0.000 description 1
- 239000004179 indigotine Substances 0.000 description 1
- 229910001410 inorganic ion Inorganic materials 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- 239000010416 ion conductor Substances 0.000 description 1
- 229910000398 iron phosphate Inorganic materials 0.000 description 1
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 1
- LRDFRRGEGBBSRN-UHFFFAOYSA-N isobutyronitrile Chemical compound CC(C)C#N LRDFRRGEGBBSRN-UHFFFAOYSA-N 0.000 description 1
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 1
- 229940011051 isopropyl acetate Drugs 0.000 description 1
- GWYFCOCPABKNJV-UHFFFAOYSA-M isovalerate Chemical compound CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
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- 239000004922 lacquer Substances 0.000 description 1
- 239000006233 lamp black Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
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- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 1
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- 239000011344 liquid material Substances 0.000 description 1
- DEUISMFZZMAAOJ-UHFFFAOYSA-N lithium dihydrogen borate oxalic acid Chemical compound B([O-])(O)O.C(C(=O)O)(=O)O.C(C(=O)O)(=O)O.[Li+] DEUISMFZZMAAOJ-UHFFFAOYSA-N 0.000 description 1
- PAZHGORSDKKUPI-UHFFFAOYSA-N lithium metasilicate Chemical compound [Li+].[Li+].[O-][Si]([O-])=O PAZHGORSDKKUPI-UHFFFAOYSA-N 0.000 description 1
- MHCFAGZWMAWTNR-UHFFFAOYSA-M lithium perchlorate Chemical compound [Li+].[O-]Cl(=O)(=O)=O MHCFAGZWMAWTNR-UHFFFAOYSA-M 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 229910052912 lithium silicate Inorganic materials 0.000 description 1
- 229910001496 lithium tetrafluoroborate Inorganic materials 0.000 description 1
- MCVFFRWZNYZUIJ-UHFFFAOYSA-M lithium;trifluoromethanesulfonate Chemical compound [Li+].[O-]S(=O)(=O)C(F)(F)F MCVFFRWZNYZUIJ-UHFFFAOYSA-M 0.000 description 1
- GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 description 1
- 239000004137 magnesium phosphate Substances 0.000 description 1
- 229910000157 magnesium phosphate Inorganic materials 0.000 description 1
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- 235000010994 magnesium phosphates Nutrition 0.000 description 1
- CUONGYYJJVDODC-UHFFFAOYSA-N malononitrile Chemical compound N#CCC#N CUONGYYJJVDODC-UHFFFAOYSA-N 0.000 description 1
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- 230000008018 melting Effects 0.000 description 1
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- 239000000113 methacrylic resin Substances 0.000 description 1
- RJBYSQHLLIHSLT-UHFFFAOYSA-N methyl 2-fluoroacetate Chemical compound COC(=O)CF RJBYSQHLLIHSLT-UHFFFAOYSA-N 0.000 description 1
- CZXGXYBOQYQXQD-UHFFFAOYSA-N methyl benzenesulfonate Chemical compound COS(=O)(=O)C1=CC=CC=C1 CZXGXYBOQYQXQD-UHFFFAOYSA-N 0.000 description 1
- ANGDWNBGPBMQHW-UHFFFAOYSA-N methyl cyanoacetate Chemical compound COC(=O)CC#N ANGDWNBGPBMQHW-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
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- OIRDBPQYVWXNSJ-UHFFFAOYSA-N methyl trifluoromethansulfonate Chemical compound COS(=O)(=O)C(F)(F)F OIRDBPQYVWXNSJ-UHFFFAOYSA-N 0.000 description 1
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- JOUIQRNQJGXQDC-AXTSPUMRSA-N namn Chemical compound O1[C@@H](COP(O)([O-])=O)[C@H](O)[C@@H](O)[C@@H]1[N+]1=CC=CC(C(O)=O)=C1 JOUIQRNQJGXQDC-AXTSPUMRSA-N 0.000 description 1
- 239000002121 nanofiber Substances 0.000 description 1
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- 150000002825 nitriles Chemical class 0.000 description 1
- 229920001220 nitrocellulos Polymers 0.000 description 1
- LYGJENNIWJXYER-UHFFFAOYSA-N nitromethane Chemical compound C[N+]([O-])=O LYGJENNIWJXYER-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- BTNXBLUGMAMSSH-UHFFFAOYSA-N octanedinitrile Chemical compound N#CCCCCCCC#N BTNXBLUGMAMSSH-UHFFFAOYSA-N 0.000 description 1
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- MHYFEEDKONKGEB-UHFFFAOYSA-N oxathiane 2,2-dioxide Chemical compound O=S1(=O)CCCCO1 MHYFEEDKONKGEB-UHFFFAOYSA-N 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
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- 230000010287 polarization Effects 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
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- 229920001083 polybutene Polymers 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229940050271 potassium alum Drugs 0.000 description 1
- GNHOJBNSNUXZQA-UHFFFAOYSA-J potassium aluminium sulfate dodecahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.O.O.[Al+3].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GNHOJBNSNUXZQA-UHFFFAOYSA-J 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 229910001487 potassium perchlorate Inorganic materials 0.000 description 1
- 229920005614 potassium polyacrylate Polymers 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 229910052913 potassium silicate Inorganic materials 0.000 description 1
- GLGXXYFYZWQGEL-UHFFFAOYSA-M potassium;trifluoromethanesulfonate Chemical compound [K+].[O-]S(=O)(=O)C(F)(F)F GLGXXYFYZWQGEL-UHFFFAOYSA-M 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
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- FVSKHRXBFJPNKK-UHFFFAOYSA-N propionitrile Chemical compound CCC#N FVSKHRXBFJPNKK-UHFFFAOYSA-N 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- HUAZGNHGCJGYNP-UHFFFAOYSA-N propyl butyrate Chemical compound CCCOC(=O)CCC HUAZGNHGCJGYNP-UHFFFAOYSA-N 0.000 description 1
- JUJWROOIHBZHMG-UHFFFAOYSA-O pyridinium Chemical compound C1=CC=[NH+]C=C1 JUJWROOIHBZHMG-UHFFFAOYSA-O 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 229910000275 saponite Inorganic materials 0.000 description 1
- 229910052706 scandium Inorganic materials 0.000 description 1
- 235000019355 sepiolite Nutrition 0.000 description 1
- 229910052624 sepiolite Inorganic materials 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 235000011127 sodium aluminium sulphate Nutrition 0.000 description 1
- BAZAXWOYCMUHIX-UHFFFAOYSA-M sodium perchlorate Chemical compound [Na+].[O-]Cl(=O)(=O)=O BAZAXWOYCMUHIX-UHFFFAOYSA-M 0.000 description 1
- 229910001488 sodium perchlorate Inorganic materials 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 229910001495 sodium tetrafluoroborate Inorganic materials 0.000 description 1
- YLKTWKVVQDCJFL-UHFFFAOYSA-N sodium;bis(trifluoromethylsulfonyl)azanide Chemical compound [Na+].FC(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F YLKTWKVVQDCJFL-UHFFFAOYSA-N 0.000 description 1
- XGPOMXSYOKFBHS-UHFFFAOYSA-M sodium;trifluoromethanesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C(F)(F)F XGPOMXSYOKFBHS-UHFFFAOYSA-M 0.000 description 1
- 229910021384 soft carbon Inorganic materials 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- IAHFWCOBPZCAEA-UHFFFAOYSA-N succinonitrile Chemical compound N#CCCC#N IAHFWCOBPZCAEA-UHFFFAOYSA-N 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- PCCVSPMFGIFTHU-UHFFFAOYSA-N tetracyanoquinodimethane Chemical compound N#CC(C#N)=C1C=CC(=C(C#N)C#N)C=C1 PCCVSPMFGIFTHU-UHFFFAOYSA-N 0.000 description 1
- ZUHZGEOKBKGPSW-UHFFFAOYSA-N tetraglyme Chemical compound COCCOCCOCCOCCOC ZUHZGEOKBKGPSW-UHFFFAOYSA-N 0.000 description 1
- 239000006234 thermal black Substances 0.000 description 1
- GINSRDSEEGBTJO-UHFFFAOYSA-N thietane 1-oxide Chemical compound O=S1CCC1 GINSRDSEEGBTJO-UHFFFAOYSA-N 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 229930192474 thiophene Natural products 0.000 description 1
- QUBMWJKTLKIJNN-UHFFFAOYSA-B tin(4+);tetraphosphate Chemical compound [Sn+4].[Sn+4].[Sn+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QUBMWJKTLKIJNN-UHFFFAOYSA-B 0.000 description 1
- JUWGUJSXVOBPHP-UHFFFAOYSA-B titanium(4+);tetraphosphate Chemical compound [Ti+4].[Ti+4].[Ti+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O JUWGUJSXVOBPHP-UHFFFAOYSA-B 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 150000008648 triflates Chemical class 0.000 description 1
- YFNKIDBQEZZDLK-UHFFFAOYSA-N triglyme Chemical compound COCCOCCOCCOC YFNKIDBQEZZDLK-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- RXPQRKFMDQNODS-UHFFFAOYSA-N tripropyl phosphate Chemical compound CCCOP(=O)(OCCC)OCCC RXPQRKFMDQNODS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
- 229910000165 zinc phosphate Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Landscapes
- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
- Accessories For Mixers (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Secondary Cells (AREA)
- Battery Electrode And Active Subsutance (AREA)
Description
図1Aは、本実施形態に係る混合システムの概略を示すブロック図である。図1Bは、ホッパーの概略を示す図である。図1Aに示すように、本実施形態に係る混合システム100は、材料供給装置110と、混合装置120とを備える。材料供給装置110はホッパー111を有し、ホッパー111と、混合装置120を構成する混合機構121とが、バタフライバルブ130を介して外気と隔絶された状態で接続されている。
次に、本発明の材料供給装置を含む混合システムを、スラリーを製造するスラリー製造装置に適用した例について説明する。以下は、粉体である第1材料と、液体である第2材料とを混合するスラリー製造装置の一例である。
図3に示すように、材料供給装置Xは、フィーダ220より材料調整部31Aに投入された粉体Pを、注ぎ口部31Bを通過して、下部開口部31Cから排出させるホッパー31を備える。ホッパー31の注ぎ口部31B内には、粉体Pを攪拌する攪拌機構32を備える。また、材料供給装置Xは、下部開口部31Cの下流側に接続された吸引ポンプ機構部80の吸引により、下部開口部31Cから排出された粉体Pを定量供給するための容積式の定量供給部40を備える。
(溶媒供給部)
図2及び図3に示すように、タンク260は、タンク260内の液体Rを設定流量で混合装置Yの供給口11に連続的に供給するように構成されている。よって、タンク260は、液体Rを混合装置Yに供給する溶媒供給源として機能する。また、タンク260には、再循環機構部70から排出路22を介してスラリーFが供給される。よって、タンク260は、スラリーFを回収するスラリー回収源として機能する。
図3、図6~図9に基づいて、吸引ポンプ機構部80について説明を加える。図6に示すように、吸引ポンプ機構部80は、両端開口が前壁部2と後壁部3とで閉じられた円筒状の外周壁部4を備えた本体ケーシング1を備え、その本体ケーシング1の内部に同心状で回転駆動自在に設けられたロータ5と、その本体ケーシング1の内部に同心状で前壁部2に固定配設された円筒状のステータ7と、ロータ5を回転駆動するポンプ駆動モータM3等を備えて構成されている。
再循環機構部(分離部の一例)70は、円筒状容器71内において比重によって溶解液を分離するように構成され、図3に示すように、吸引ポンプ機構部80の吐出部12から吐出路18を通して供給されるスラリーFから、完全に溶解していない粉体Pを含む可能性がある状態の未溶解スラリーFrを循環路16に、粉体Pが略完全に溶解した状態のスラリーFを排出路22にそれぞれ分離するように構成されている。吐出路18及び循環路16は、夫々、円筒状容器71の下部に接続され、排出路22は、円筒状容器71の上部とスラリーFの供給先であるタンク260とに接続される。
特に制御部Cは、ロータ5(回転翼6)の回転数を制御可能に構成され、ステータ7の供給室側透孔7a及び導入室側透孔7b(絞り透孔)の出口領域の圧力が当該出口領域の全周に亘って液体Rの飽和蒸気圧(25℃の水の場合、3.169kPa)以下となるように回転翼6の回転数を設定し、当該設定された回転数で回転翼6を回転することで、少なくともステータ7の供給室側透孔7a及び導入室側透孔7bを通過した直後の翼室8内の領域を、翼室8内の全周に亘って連続して、液体Rの微細気泡(マイクロバブル)が多数発生した微細気泡領域として形成させることができるように構成されている。
次に、このスラリー製造装置200の動作について説明する。まず、ドライボックス230及び240を運転して露点温度を低下させ、冷却装置250も運転する。また、除湿ユニット233の調整により、ホッパー31内の気圧を陽圧(外気圧より2~3Pa程度高い状態)とし、ドライボックス230の気圧を陰圧(外気圧より2~3Pa程度低い状態)とする。
上記実施形態の構成に加えて、ホッパー31に投入される粉体Pの量を監視する構成を追加してもよい。例えば、ホッパー31の最下端から所定位置の下部に粉体Pを検出可能なセンサAを設ける。センサAにより、ホッパー31の最下端から所定位置まで粉体Pがホッパー31に投入されていることが検出できる。センサAが粉体Pを検出した場合には、図示しない制御部がフィーダ220からホッパー31への粉体Pの供給速度を遅くする。これにより、ホッパー31に過度に粉体Pが供給されるのを抑制し、ホッパー31での粉体Pの詰まり等を抑制できる。
110:材料供給装置
111:ホッパー
111A:材料調整部
111B:注ぎ口部
111C:仕切り板
111D:開口
111E:シャッター
111F:グローブ
112:ドライガス供給部
112a:ボンベ
112b:静電気除去装置
113:炭酸ガス供給部
114:真空ポンプ
115:圧力計
116:除湿機
117:前室
118:開閉機構
119:開閉機構
120:混合装置
130:バタフライバルブ
1:本体ケーシング
2:前壁部
3:後壁部
4:外周壁部
5:ロータ
5a:取付部
6:回転翼
7:ステータ
7a:供給室側透孔
7b:導入室側透孔
8:翼室
9:掻出翼
9B:基端部
9M:中間部
9T:先端部
9a;背面
9f:掻き出し面
9i:内向き側面
9m:放散面
9o:外向き側面
9t:先端面
10:環状溝
11:供給ロ
12:吐出部
13:供給室
14:導入室
14a:絞り部
15:区画板
15a:筒状摺接部
15b:漏斗状部
15c:環状平板部
16:循環路
17:導入口
18:吐出路
19:駆動軸
20:間隔保持部材
21:攪拌羽根
22:排出路
31:ホッパー
31A:材料調整部
31B:注ぎ口部
31C:下部開口部
31D:グローブ
32:攪拌機構
32A:攪拌羽根
40:定量供給部
41:導入部
42:開口閉鎖部材
43:ケーシング
43a:供給ロ
43b:排出口
44:計量回転体
44a:板状隔壁
44b:粉体収容室
45:粉体排出管
46:シャックバルブ
47:膨張室
48:駆動軸
49:円盤部材
52:溶媒供給管
60:ミキシング機構
61:ミキシング部材
62:筒状部
63:スリット
64:環状流路
65:環状流路形成部
70:再循環機構部
71:円筒状容器
80:吸引ポンプ機構部
200:スラリー製造装置
210:フィーダホッパー
211:エア抜きロ
220:フィーダ
221:粉体排出口
230:粉体用ドライボックス
231:外側ボックス
232:内側ボックス
233:除湿ユニット
240:本体用ドライボックス
250:冷却装置
260:タンク
261:ポンプ
270:圧力抜き部
271:フィルタ
280:架台
C:制御部
F:スラリー
Fp:予備混合物
Fr:未溶解スラリー
M2:計量回転体駆動モータ
M3:ポンプ駆動モータ
M4:タンク攪拌モータ
P:粉体
R:液体
V:概略
X:材料供給装置
Y:混合装置
Claims (9)
- 複数の材料を混合する混合システムであり、複数の材料を混合する混合機構と、前記混合機構に粉体または液体である第1材料を供給する材料供給装置と、を備え、
前記材料供給装置は、材料を調整する材料調整部と、第1材料を前記混合機構に供給する注ぎ口部とを具備するホッパーと、前記ホッパーに設けられ外気から遮断された状態で前記ホッパー内で作業可能なグローブと、前記ホッパー内にドライガスを供給するドライガス供給部と、を有し、
前記材料供給装置と前記混合機構が、前記注ぎ口部の出口部に取り付けられたバルブを介して外気と隔絶された状態で接続され、前記ドライガス供給部から供給されるドライガスにより、前記ホッパー内の露点温度がマイナス100℃以上マイナス20℃以下、内部圧力(絶対圧)が0.01MPa以上10MPa以下のドライガス環境とすることを特徴とし、
前記ホッパーは、前記材料調整部と前記注ぎ口部との間に仕切り部を備え、前記仕切り部により、前記材料調整部と前記注ぎ口部とが区画されており、前記仕切り部は前記第1材料が通過可能な開口と、材料が注ぎ口部へ流入することを防止するための前記開口をふさぐ蓋、または、前記開口を開閉可能な開閉機構とを有し、
前記材料調整部は前室を備え、前記材料調整部と前記前室には、材料を出し入れできる開閉可能な第1開閉機構が介在し、前記材料調整部と前記前室との内空間が前記第1開閉機構を介して連通し、前記前室の内空間と大気が第2開閉機構を介して連通し、前記前室にはガス置換するための真空ポンプおよびドライガス供給部が接続され、前記前室が前記材料調整部よりも体積が小さいことを特徴とする、混合システム。 - 前記材料供給装置は、前記第1材料が前記ホッパーの注ぎ口部を通過するより前に、該第1材料を乾燥する乾燥機構をさらに有する、
請求項1に記載の混合システム。 - 前記乾燥機構は、前記第1材料をドライガス環境に曝して、材料中の揮発成分を除去するものであり、
前記材料供給装置は、除去した揮発成分を外気に排気するための排出機構をさらに有する、
請求項2に記載の混合システム。 - 前記乾燥機構は、前記第1材料に流動性を与えて、該第1材料に含まれる揮発成分を除去するものである、
請求項2または3に記載の混合システム。 - 前記乾燥機構は、前記第1材料を加熱して、該第1材料に含まれる揮発成分を除去するものである、
請求項2乃至請求項4のいずれかに記載の混合システム。 - 前記材料供給装置は、前記ホッパー内または前記ドライガス供給部もしくはこれらの間に、静電気除去装置をさらに備える、
請求項1乃至請求項5のいずれかに記載の混合システム。 - 前記混合機構により複数の材料が混合されて吐き出された混合材料を排出するための排出口をさらに備え、
前記排出口が外気と隔絶された状態である、
請求項1乃至請求項6のいずれかに記載の混合システム。 - 非水電解質蓄電デバイスの製造工程に用いられる混合システムである、
請求項1乃至請求項7のいずれかに記載の混合システム。 - 請求項1乃至請求項8のいずれかに記載の混合システムの前記混合機構に接続して用いられる、材料供給装置。
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