JP7104873B1 - 有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 - Google Patents
有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 Download PDFInfo
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- JP7104873B1 JP7104873B1 JP2022012483A JP2022012483A JP7104873B1 JP 7104873 B1 JP7104873 B1 JP 7104873B1 JP 2022012483 A JP2022012483 A JP 2022012483A JP 2022012483 A JP2022012483 A JP 2022012483A JP 7104873 B1 JP7104873 B1 JP 7104873B1
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- 239000003480 eluent Substances 0.000 title claims abstract description 72
- 238000000746 purification Methods 0.000 title claims abstract description 62
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 239000000460 chlorine Substances 0.000 title claims abstract description 34
- 229910052801 chlorine Inorganic materials 0.000 title claims abstract description 34
- 239000002689 soil Substances 0.000 title claims abstract description 20
- 238000011084 recovery Methods 0.000 title claims abstract description 19
- 238000001914 filtration Methods 0.000 claims abstract description 19
- 239000003993 organochlorine pesticide Substances 0.000 claims abstract description 16
- 239000007787 solid Substances 0.000 claims abstract description 16
- 239000002245 particle Substances 0.000 claims abstract description 10
- 238000005067 remediation Methods 0.000 claims abstract description 8
- 238000001556 precipitation Methods 0.000 claims abstract 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 54
- 239000008213 purified water Substances 0.000 claims description 45
- 238000012856 packing Methods 0.000 claims description 44
- 238000004062 sedimentation Methods 0.000 claims description 22
- 238000004140 cleaning Methods 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 13
- 239000007790 solid phase Substances 0.000 claims description 12
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 9
- 239000000741 silica gel Substances 0.000 claims description 9
- 229910002027 silica gel Inorganic materials 0.000 claims description 9
- 238000001514 detection method Methods 0.000 claims description 6
- 239000002351 wastewater Substances 0.000 claims description 6
- 239000006004 Quartz sand Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000000575 pesticide Substances 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000003905 agrochemical Substances 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 238000010828 elution Methods 0.000 abstract description 13
- 230000006866 deterioration Effects 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract description 2
- 238000002414 normal-phase solid-phase extraction Methods 0.000 description 34
- 238000000605 extraction Methods 0.000 description 11
- 238000001179 sorption measurement Methods 0.000 description 10
- GXGAKHNRMVGRPK-UHFFFAOYSA-N dimagnesium;dioxido-bis[[oxido(oxo)silyl]oxy]silane Chemical compound [Mg+2].[Mg+2].[O-][Si](=O)O[Si]([O-])([O-])O[Si]([O-])=O GXGAKHNRMVGRPK-UHFFFAOYSA-N 0.000 description 8
- 239000000391 magnesium silicate Substances 0.000 description 8
- 229940099273 magnesium trisilicate Drugs 0.000 description 8
- 229910000386 magnesium trisilicate Inorganic materials 0.000 description 8
- 235000019793 magnesium trisilicate Nutrition 0.000 description 8
- 230000035485 pulse pressure Effects 0.000 description 8
- 239000000356 contaminant Substances 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 238000010586 diagram Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000004128 high performance liquid chromatography Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000011049 filling Methods 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 239000004094 surface-active agent Substances 0.000 description 4
- UCNVFOCBFJOQAL-UHFFFAOYSA-N DDE Chemical compound C=1C=C(Cl)C=CC=1C(=C(Cl)Cl)C1=CC=C(Cl)C=C1 UCNVFOCBFJOQAL-UHFFFAOYSA-N 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000004904 shortening Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- JLYXXMFPNIAWKQ-CDRYSYESSA-N beta-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@H](Cl)[C@@H](Cl)[C@@H]1Cl JLYXXMFPNIAWKQ-CDRYSYESSA-N 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- JLYXXMFPNIAWKQ-GNIYUCBRSA-N gamma-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@@H](Cl)[C@H](Cl)[C@H]1Cl JLYXXMFPNIAWKQ-GNIYUCBRSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229960002809 lindane Drugs 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 231100000219 mutagenic Toxicity 0.000 description 1
- 230000003505 mutagenic effect Effects 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 239000002957 persistent organic pollutant Substances 0.000 description 1
- 238000001782 photodegradation Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 231100000378 teratogenic Toxicity 0.000 description 1
- 230000003390 teratogenic effect Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/30—Treatment of water, waste water, or sewage by irradiation
- C02F1/32—Treatment of water, waste water, or sewage by irradiation with ultraviolet light
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F2001/007—Processes including a sedimentation step
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/36—Organic compounds containing halogen
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/32—Details relating to UV-irradiation devices
- C02F2201/322—Lamp arrangement
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/32—Details relating to UV-irradiation devices
- C02F2201/322—Lamp arrangement
- C02F2201/3227—Units with two or more lamps
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2301/00—General aspects of water treatment
- C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Processing Of Solid Wastes (AREA)
- Water Treatment By Sorption (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110244453.9A CN112979043B (zh) | 2021-03-05 | 2021-03-05 | 有机氯农药污染土壤修复用增效洗脱液的净化回收装置 |
CN202110244453.9 | 2021-03-05 |
Publications (2)
Publication Number | Publication Date |
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JP7104873B1 true JP7104873B1 (ja) | 2022-07-22 |
JP2022135940A JP2022135940A (ja) | 2022-09-15 |
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JP2022012483A Active JP7104873B1 (ja) | 2021-03-05 | 2022-01-29 | 有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 |
Country Status (2)
Country | Link |
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JP (1) | JP7104873B1 (zh) |
CN (1) | CN112979043B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115448437A (zh) * | 2022-10-10 | 2022-12-09 | 福建南平三元循环技术有限公司 | 一种硅胶生产用废水循环回用装置及其处理方法 |
CN117427519A (zh) * | 2023-12-22 | 2024-01-23 | 山东上远环保科技有限公司 | 一种污水药剂净化处理装置 |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2001129527A (ja) | 1999-08-30 | 2001-05-15 | Biogenesis Enterprises Inc | 細かい粒状にされた土、粘土および沈積土から汚染物質を除去する装置および方法 |
JP2013186025A (ja) | 2012-03-09 | 2013-09-19 | Hitachi-Ge Nuclear Energy Ltd | 除染廃液の処理装置及びその処理方法 |
JP2014000495A (ja) | 2012-06-15 | 2014-01-09 | Universal Engineering Co Ltd | 汚水処理装置及びこれを用いた汚水処理方法 |
JP2016010768A (ja) | 2014-06-30 | 2016-01-21 | 株式会社安藤・間 | 汚染土壌の浄化方法 |
JP2018001070A (ja) | 2016-06-29 | 2018-01-11 | 株式会社竹村製作所 | 循環型水処理装置 |
CN109757715A (zh) | 2018-12-17 | 2019-05-17 | 无名金葵(北京)科技发展有限公司 | 一种黄蜀葵生物酵素及其制备方法 |
JP2019181403A (ja) | 2018-04-16 | 2019-10-24 | 清水建設株式会社 | 農薬汚染土壌の洗浄処理システム及び洗浄処理方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
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US6511601B2 (en) * | 2000-04-03 | 2003-01-28 | Bechtel Bwxt Idaho, Llc | Method and system for extraction of chemicals from aquifer remediation effluent water |
JP2002059160A (ja) * | 2000-08-11 | 2002-02-26 | Daikin Ind Ltd | 含フッ素陰イオン系界面活性剤の分離方法 |
JP2004108838A (ja) * | 2002-09-17 | 2004-04-08 | Showa Denko Kk | 固相抽出用カートリッジカラム |
CA2630894A1 (fr) * | 2008-05-02 | 2009-11-02 | Northex Environnement | Methode pour decontaminer des sols d'un contaminant inorganique par lavage physico-chimique |
CN102211795A (zh) * | 2011-04-20 | 2011-10-12 | 华中科技大学 | 一种再生有机污染土壤洗脱液中洗脱剂的方法 |
CN106132525B (zh) * | 2014-03-31 | 2018-02-06 | 旭硝子株式会社 | 阴离子型含氟乳化剂的回收方法 |
CN104524812B (zh) * | 2014-12-17 | 2016-04-27 | 南京博蕴生物科技有限公司 | 使用固载液液萃取柱从中药材水提液中萃取有效成分的方法 |
CN106077061B (zh) * | 2016-06-15 | 2019-11-08 | 东北林业大学 | 一种表面活性剂洗脱和类Fenton氧化联合修复有机氯农药污染土壤的方法 |
CN107364978B (zh) * | 2017-08-31 | 2020-07-28 | 中国科学院合肥物质科学研究院 | 利用纳米铁与白腐菌吸附移除洗脱液有机氯农药的方法 |
CN109319871A (zh) * | 2018-10-17 | 2019-02-12 | 浙江大学 | 一种选择性吸附再生回收有机污染土壤修复洗脱液的方法 |
-
2021
- 2021-03-05 CN CN202110244453.9A patent/CN112979043B/zh not_active Expired - Fee Related
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2022
- 2022-01-29 JP JP2022012483A patent/JP7104873B1/ja active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2001129527A (ja) | 1999-08-30 | 2001-05-15 | Biogenesis Enterprises Inc | 細かい粒状にされた土、粘土および沈積土から汚染物質を除去する装置および方法 |
JP2013186025A (ja) | 2012-03-09 | 2013-09-19 | Hitachi-Ge Nuclear Energy Ltd | 除染廃液の処理装置及びその処理方法 |
JP2014000495A (ja) | 2012-06-15 | 2014-01-09 | Universal Engineering Co Ltd | 汚水処理装置及びこれを用いた汚水処理方法 |
JP2016010768A (ja) | 2014-06-30 | 2016-01-21 | 株式会社安藤・間 | 汚染土壌の浄化方法 |
JP2018001070A (ja) | 2016-06-29 | 2018-01-11 | 株式会社竹村製作所 | 循環型水処理装置 |
JP2019181403A (ja) | 2018-04-16 | 2019-10-24 | 清水建設株式会社 | 農薬汚染土壌の洗浄処理システム及び洗浄処理方法 |
CN109757715A (zh) | 2018-12-17 | 2019-05-17 | 无名金葵(北京)科技发展有限公司 | 一种黄蜀葵生物酵素及其制备方法 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115448437A (zh) * | 2022-10-10 | 2022-12-09 | 福建南平三元循环技术有限公司 | 一种硅胶生产用废水循环回用装置及其处理方法 |
CN115448437B (zh) * | 2022-10-10 | 2023-08-08 | 福建南平三元循环技术有限公司 | 一种硅胶生产用废水循环回用装置及其处理方法 |
CN117427519A (zh) * | 2023-12-22 | 2024-01-23 | 山东上远环保科技有限公司 | 一种污水药剂净化处理装置 |
CN117427519B (zh) * | 2023-12-22 | 2024-03-26 | 山东上远环保科技有限公司 | 一种污水药剂净化处理装置 |
Also Published As
Publication number | Publication date |
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CN112979043A (zh) | 2021-06-18 |
JP2022135940A (ja) | 2022-09-15 |
CN112979043B (zh) | 2022-08-26 |
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