JP7104873B1 - 有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 - Google Patents

有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 Download PDF

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Publication number: JP7104873B1
Authority: JP; Japan
Prior art keywords: purification; eluent; purified water; organic chlorine; unit
Prior art date: 2021-03-05
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Active

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JP2022012483A

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English (en)

Japanese (ja)

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JP2022135940A (ja

Inventor

▲とう▼紹坡

周艶

孔令雅

丁達

李旭偉

Original Assignee

生態環境部南京環境科学研究所

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2021-03-05

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2022-01-29

Publication date

2022-07-22

2022-01-29 Application filed by 生態環境部南京環境科学研究所 filed Critical 生態環境部南京環境科学研究所

2022-07-22 Application granted granted Critical

2022-07-22 Publication of JP7104873B1 publication Critical patent/JP7104873B1/ja

2022-09-15 Publication of JP2022135940A publication Critical patent/JP2022135940A/ja

Status Active legal-status Critical Current

2042-01-29 Anticipated expiration legal-status Critical

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239000003480 eluent Substances 0.000 title claims abstract description 72
238000000746 purification Methods 0.000 title claims abstract description 62
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims abstract description 34
239000000460 chlorine Substances 0.000 title claims abstract description 34
229910052801 chlorine Inorganic materials 0.000 title claims abstract description 34
239000002689 soil Substances 0.000 title claims abstract description 20
238000011084 recovery Methods 0.000 title claims abstract description 19
238000001914 filtration Methods 0.000 claims abstract description 19
239000003993 organochlorine pesticide Substances 0.000 claims abstract description 16
239000007787 solid Substances 0.000 claims abstract description 16
239000002245 particle Substances 0.000 claims abstract description 10
238000005067 remediation Methods 0.000 claims abstract description 8
238000001556 precipitation Methods 0.000 claims abstract 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 54
239000008213 purified water Substances 0.000 claims description 45
238000012856 packing Methods 0.000 claims description 44
238000004062 sedimentation Methods 0.000 claims description 22
238000004140 cleaning Methods 0.000 claims description 21
239000007788 liquid Substances 0.000 claims description 15
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 13
239000007790 solid phase Substances 0.000 claims description 12
125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 9
239000000741 silica gel Substances 0.000 claims description 9
229910002027 silica gel Inorganic materials 0.000 claims description 9
238000001514 detection method Methods 0.000 claims description 6
239000002351 wastewater Substances 0.000 claims description 6
239000006004 Quartz sand Substances 0.000 claims description 5
238000010438 heat treatment Methods 0.000 claims description 5
239000000575 pesticide Substances 0.000 claims description 4
150000001875 compounds Chemical class 0.000 claims description 3
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
239000002253 acid Substances 0.000 claims 1
239000003905 agrochemical Substances 0.000 claims 1
239000011777 magnesium Substances 0.000 claims 1
229910052749 magnesium Inorganic materials 0.000 claims 1
238000010828 elution Methods 0.000 abstract description 13
230000006866 deterioration Effects 0.000 abstract description 2
238000004064 recycling Methods 0.000 abstract description 2
238000002414 normal-phase solid-phase extraction Methods 0.000 description 34
238000000605 extraction Methods 0.000 description 11
238000001179 sorption measurement Methods 0.000 description 10
GXGAKHNRMVGRPK-UHFFFAOYSA-N dimagnesium;dioxido-bis[[oxido(oxo)silyl]oxy]silane Chemical compound [Mg+2].[Mg+2].[O-][Si](=O)O[Si]([O-])([O-])O[Si]([O-])=O GXGAKHNRMVGRPK-UHFFFAOYSA-N 0.000 description 8
239000000391 magnesium silicate Substances 0.000 description 8
229940099273 magnesium trisilicate Drugs 0.000 description 8
229910000386 magnesium trisilicate Inorganic materials 0.000 description 8
235000019793 magnesium trisilicate Nutrition 0.000 description 8
230000035485 pulse pressure Effects 0.000 description 8
239000000356 contaminant Substances 0.000 description 7
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
238000010586 diagram Methods 0.000 description 5
230000000694 effects Effects 0.000 description 5
238000004128 high performance liquid chromatography Methods 0.000 description 5
238000000034 method Methods 0.000 description 5
238000005406 washing Methods 0.000 description 5
238000011049 filling Methods 0.000 description 4
239000012071 phase Substances 0.000 description 4
238000003860 storage Methods 0.000 description 4
239000004094 surface-active agent Substances 0.000 description 4
UCNVFOCBFJOQAL-UHFFFAOYSA-N DDE Chemical compound C=1C=C(Cl)C=CC=1C(=C(Cl)Cl)C1=CC=C(Cl)C=C1 UCNVFOCBFJOQAL-UHFFFAOYSA-N 0.000 description 2
230000000903 blocking effect Effects 0.000 description 2
239000002131 composite material Substances 0.000 description 2
CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 description 2
239000011148 porous material Substances 0.000 description 2
238000004904 shortening Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
230000009286 beneficial effect Effects 0.000 description 1
JLYXXMFPNIAWKQ-CDRYSYESSA-N beta-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@H](Cl)[C@@H](Cl)[C@@H]1Cl JLYXXMFPNIAWKQ-CDRYSYESSA-N 0.000 description 1
230000000711 cancerogenic effect Effects 0.000 description 1
231100000315 carcinogenic Toxicity 0.000 description 1
230000008859 change Effects 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
JLYXXMFPNIAWKQ-GNIYUCBRSA-N gamma-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@@H](Cl)[C@H](Cl)[C@H]1Cl JLYXXMFPNIAWKQ-GNIYUCBRSA-N 0.000 description 1
230000036541 health Effects 0.000 description 1
238000009434 installation Methods 0.000 description 1
230000001678 irradiating effect Effects 0.000 description 1
238000002386 leaching Methods 0.000 description 1
229960002809 lindane Drugs 0.000 description 1
238000012423 maintenance Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
231100000219 mutagenic Toxicity 0.000 description 1
230000003505 mutagenic effect Effects 0.000 description 1
230000002085 persistent effect Effects 0.000 description 1
239000002957 persistent organic pollutant Substances 0.000 description 1
238000001782 photodegradation Methods 0.000 description 1
230000001376 precipitating effect Effects 0.000 description 1
230000008569 process Effects 0.000 description 1
230000008439 repair process Effects 0.000 description 1
230000004044 response Effects 0.000 description 1
238000007789 sealing Methods 0.000 description 1
239000010865 sewage Substances 0.000 description 1
231100000378 teratogenic Toxicity 0.000 description 1
230000003390 teratogenic effect Effects 0.000 description 1

Images

Classifications

- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/30—Treatment of water, waste water, or sewage by irradiation
- C02F1/32—Treatment of water, waste water, or sewage by irradiation with ultraviolet light
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F2001/007—Processes including a sedimentation step
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/36—Organic compounds containing halogen
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/32—Details relating to UV-irradiation devices
- C02F2201/322—Lamp arrangement
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/32—Details relating to UV-irradiation devices
- C02F2201/322—Lamp arrangement
- C02F2201/3227—Units with two or more lamps
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2301/00—General aspects of water treatment
- C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions

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Life Sciences & Earth Sciences (AREA)
Hydrology & Water Resources (AREA)
Engineering & Computer Science (AREA)
Environmental & Geological Engineering (AREA)
Water Supply & Treatment (AREA)
Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Processing Of Solid Wastes (AREA)
Water Treatment By Sorption (AREA)

JP2022012483A 2021-03-05 2022-01-29 有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置 Active JP7104873B1 (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
CN202110244453.9A CN112979043B (zh)	2021-03-05	2021-03-05	有机氯农药污染土壤修复用增效洗脱液的净化回收装置
CN202110244453.9		2021-03-05

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Publication Number	Publication Date
JP7104873B1 true JP7104873B1 (ja)	2022-07-22
JP2022135940A JP2022135940A (ja)	2022-09-15

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JP2022012483A Active JP7104873B1 (ja)	2021-03-05	2022-01-29	有機塩素系農薬汚染土壤修復用の高性能溶離液の浄化回収装置

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JP (1)	JP7104873B1 (zh)
CN (1)	CN112979043B (zh)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN115448437A (zh) *	2022-10-10	2022-12-09	福建南平三元循环技术有限公司	一种硅胶生产用废水循环回用装置及其处理方法
CN117427519A (zh) *	2023-12-22	2024-01-23	山东上远环保科技有限公司	一种污水药剂净化处理装置

Citations (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2001129527A (ja)	1999-08-30	2001-05-15	Biogenesis Enterprises Inc	細かい粒状にされた土、粘土および沈積土から汚染物質を除去する装置および方法
JP2013186025A (ja)	2012-03-09	2013-09-19	Hitachi-Ge Nuclear Energy Ltd	除染廃液の処理装置及びその処理方法
JP2014000495A (ja)	2012-06-15	2014-01-09	Universal Engineering Co Ltd	汚水処理装置及びこれを用いた汚水処理方法
JP2016010768A (ja)	2014-06-30	2016-01-21	株式会社安藤・間	汚染土壌の浄化方法
JP2018001070A (ja)	2016-06-29	2018-01-11	株式会社竹村製作所	循環型水処理装置
CN109757715A (zh)	2018-12-17	2019-05-17	无名金葵(北京)科技发展有限公司	一种黄蜀葵生物酵素及其制备方法
JP2019181403A (ja)	2018-04-16	2019-10-24	清水建設株式会社	農薬汚染土壌の洗浄処理システム及び洗浄処理方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6511601B2 (en) *	2000-04-03	2003-01-28	Bechtel Bwxt Idaho, Llc	Method and system for extraction of chemicals from aquifer remediation effluent water
JP2002059160A (ja) *	2000-08-11	2002-02-26	Daikin Ind Ltd	含フッ素陰イオン系界面活性剤の分離方法
JP2004108838A (ja) *	2002-09-17	2004-04-08	Showa Denko Kk	固相抽出用カートリッジカラム
CA2630894A1 (fr) *	2008-05-02	2009-11-02	Northex Environnement	Methode pour decontaminer des sols d'un contaminant inorganique par lavage physico-chimique
CN102211795A (zh) *	2011-04-20	2011-10-12	华中科技大学	一种再生有机污染土壤洗脱液中洗脱剂的方法
CN106132525B (zh) *	2014-03-31	2018-02-06	旭硝子株式会社	阴离子型含氟乳化剂的回收方法
CN104524812B (zh) *	2014-12-17	2016-04-27	南京博蕴生物科技有限公司	使用固载液液萃取柱从中药材水提液中萃取有效成分的方法
CN106077061B (zh) *	2016-06-15	2019-11-08	东北林业大学	一种表面活性剂洗脱和类Fenton氧化联合修复有机氯农药污染土壤的方法
CN107364978B (zh) *	2017-08-31	2020-07-28	中国科学院合肥物质科学研究院	利用纳米铁与白腐菌吸附移除洗脱液有机氯农药的方法
CN109319871A (zh) *	2018-10-17	2019-02-12	浙江大学	一种选择性吸附再生回收有机污染土壤修复洗脱液的方法

2021
- 2021-03-05 CN CN202110244453.9A patent/CN112979043B/zh not_active Expired - Fee Related
2022
- 2022-01-29 JP JP2022012483A patent/JP7104873B1/ja active Active

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2001129527A (ja)	1999-08-30	2001-05-15	Biogenesis Enterprises Inc	細かい粒状にされた土、粘土および沈積土から汚染物質を除去する装置および方法
JP2013186025A (ja)	2012-03-09	2013-09-19	Hitachi-Ge Nuclear Energy Ltd	除染廃液の処理装置及びその処理方法
JP2014000495A (ja)	2012-06-15	2014-01-09	Universal Engineering Co Ltd	汚水処理装置及びこれを用いた汚水処理方法
JP2016010768A (ja)	2014-06-30	2016-01-21	株式会社安藤・間	汚染土壌の浄化方法
JP2018001070A (ja)	2016-06-29	2018-01-11	株式会社竹村製作所	循環型水処理装置
JP2019181403A (ja)	2018-04-16	2019-10-24	清水建設株式会社	農薬汚染土壌の洗浄処理システム及び洗浄処理方法
CN109757715A (zh)	2018-12-17	2019-05-17	无名金葵(北京)科技发展有限公司	一种黄蜀葵生物酵素及其制备方法

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN115448437A (zh) *	2022-10-10	2022-12-09	福建南平三元循环技术有限公司	一种硅胶生产用废水循环回用装置及其处理方法
CN115448437B (zh) *	2022-10-10	2023-08-08	福建南平三元循环技术有限公司	一种硅胶生产用废水循环回用装置及其处理方法
CN117427519A (zh) *	2023-12-22	2024-01-23	山东上远环保科技有限公司	一种污水药剂净化处理装置
CN117427519B (zh) *	2023-12-22	2024-03-26	山东上远环保科技有限公司	一种污水药剂净化处理装置

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JP2022135940A (ja)	2022-09-15
CN112979043B (zh)	2022-08-26

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