JP6797600B2 - スプレー用毛髪組成物 - Google Patents
スプレー用毛髪組成物 Download PDFInfo
- Publication number
- JP6797600B2 JP6797600B2 JP2016160027A JP2016160027A JP6797600B2 JP 6797600 B2 JP6797600 B2 JP 6797600B2 JP 2016160027 A JP2016160027 A JP 2016160027A JP 2016160027 A JP2016160027 A JP 2016160027A JP 6797600 B2 JP6797600 B2 JP 6797600B2
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- Prior art keywords
- composition
- acrylate
- hair
- spray
- copolymer
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- BARWIPMJPCRCTP-CLFAGFIQSA-N oleyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC BARWIPMJPCRCTP-CLFAGFIQSA-N 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- NEOZOXKVMDBOSG-UHFFFAOYSA-N propan-2-yl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OC(C)C NEOZOXKVMDBOSG-UHFFFAOYSA-N 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 239000008165 rice bran oil Substances 0.000 description 1
- 239000010667 rosehip oil Substances 0.000 description 1
- 229940057910 shea butter Drugs 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Landscapes
- Cosmetics (AREA)
Description
項1.
(A):(アクリレーツ/アクリル酸アルキル/アルキルアクリルアミド)コポリマー又はその塩、
(B):(アクリレーツ/オクチルアクリルアミド)コポリマー又はその塩、及び
(C):エタノール
を含み、含有される(A)と(B)の重量比が1:0.3〜1である、(好ましくは1:0.4〜0.9、より好ましくは1:0.4〜0.8、さらに好ましくは1:0.5〜0.7)
スプレー用毛髪組成物。
項2.
さらに噴霧ガスを含む、項1に記載のスプレー用毛髪組成物。
項3.
(A)が(アクリレーツ/アクリル酸アルキル(C1−18)/アルキル(C1−8)アクリルアミド)コポリマーAMPであり、(B)が(アクリレーツ/オクチルアクリルアミド)コポリマーである、項1又は2に記載のスプレー用毛髪組成物。
項4.
(A):(アクリレーツ/アクリル酸アルキル/アルキルアクリルアミド)コポリマー又はその塩、
(B):(アクリレーツ/オクチルアクリルアミド)コポリマー又はその塩、及び
(C):エタノール
を含み、(且つ好ましくは噴霧ガスを含まず、)含有される(A)と(B)の重量比が1:0.3〜1である、(好ましくは1:0.4〜0.9、より好ましくは1:0.4〜0.8、さらに好ましくは1:0.5〜0.7)
整髪液組成物(好ましくはスプレー用毛髪組成物調製用整髪液組成物であり、より好ましくは項1〜4のいずれかに記載のスプレー用毛髪組成物の調製用の整髪液組成物である。)。
項5.
項4に記載の整髪液組成物と噴霧ガスとを混合する工程を含む、スプレー用毛髪組成物の製造方法。
項6.
以下の(i)〜(iii)の構成を備えたエアゾールスプレー缶用である、項1〜3のいずれかに記載のスプレー用毛髪組成物。
(i)ハウジングにベーパータップ(VT)孔を有さない
(ii)ディップチューブの内径が0.8〜1.5mm
(iii)ステムの孔径が0.2〜0.6mm
プラスサイズL−9909B、プラスサイズ−L9715、及びプラスサイズ−L9959(以上、互応化学工業)を、120:60:1(重量比)で混合して、「(アクリレーツ/アクリル酸アルキル(C1−18)/アルキル(C1−8)アクリルアミド)コポリマーAMP液」として用いた。
表1に記載の組成に従って、各成分を混合し、ヘアスプレー用組成物(整髪液組成物)を調製した。なお、表1に記載の成分量を示す数値の単位はg(グラム)であり、各例の組成物を100gずつ調製した。
各例の組成物を、それぞれ、エアゾールスプレー缶に入れ、以下のようにして、噴霧後の乾きの早さ、及びカールリテンション(毛髪を一定の形のままキープする力の指標)を評価した。なお、各例の組成物には同重量のLPGガスを混合し(すなわち、組成物とLPGガスを重量比50:50で混合し)、ヘアスプレー用毛髪組成物を調製して、これをエアゾールスプレー缶に封入した。また、当該組成物に加えて、噴射剤としてLPGガス0.15Mpaをエアゾールスプレー缶に封入した。
剛体振り子物性試験器RPT−3000W((株)エー・アンド・デイ製)を用い、毛髪に噴霧した各組成物の乾きの早さを測定した。剛体振り子物性試験機RPT−3000Wは、粘着性、粘弾性、乾燥性等の表面物性変化を摩擦の増減の面から評価するための装置である。具体的には、アルミ板(5cm×2cm)に均一に毛髪を貼り付けたものを試料とし、試料上に丸棒型シリンダーエッジを載せた後、各組成物入りのエアゾールスプレーを3秒間、均一に噴射し、振り子を振動させ、その振動の対数減衰率を測定した。ヘアスプレーのようなスタイリング剤を毛髪に塗布した場合、塗布した薬剤が乾き始めると対数減衰率が急上昇する挙動を示す。この変化点が表れるまでにかかる時間を薬剤の乾きの早さとして測定した。詳細な評価条件は次の通りである。フレーム種類:FRB−100、 測定部形状:丸棒型シリンダーエッジ RBP−020、 試料温度:21℃ (一定)。
水に濡らした毛髪束(長さ(L):17.5cm、重さ:2g)をロッドに巻き、完全に乾燥させた。上記エアゾール製品を3秒間、均一に噴射し、自然乾燥させ、ロッドから外した毛髪を一定の条件下(温度:25℃、湿度:95%)の恒温恒湿器に吊り下げ、3時間静置した。このとき(噴霧後自然乾燥させたとき)の長さをL1、3時間放置後の長さをL3とし、下記の式にてカールリテンション(カール保持率)を算出した。なお、カールリテンションが60%以上である場合、髪型キープ力が優良であると考えられる。
実施例1の整髪液組成物に、これと同重量のLPGガスを混合し、ヘアスプレー用毛髪組成物を調製して、これをエアゾールスプレー缶に封入した。そして、噴霧した際の、霧の粒子径及び勢い(風速)を測定した。
Claims (5)
- (A):(アクリレーツ/アクリル酸アルキル/アルキルアクリルアミド)コポリマーの塩、
(B):(アクリレーツ/オクチルアクリルアミド)コポリマー、及び
(C):エタノール
を含み、含有される(A)と(B)の重量比が1:0.4〜0.8である、
スプレー用の毛髪に適用するための組成物。 - さらに噴霧ガスを含む、請求項1に記載の組成物。
- (A)が(アクリレーツ/アクリル酸アルキル(C1−18)/アルキル(C1−8)アクリルアミド)コポリマーAMPであり、(B)が(アクリレーツ/オクチルアクリルアミド)コポリマーである、請求項1又は2に記載の組成物。
- (A):(アクリレーツ/アクリル酸アルキル/アルキルアクリルアミド)コポリマーの塩、
(B):(アクリレーツ/オクチルアクリルアミド)コポリマー、及び
(C):エタノール
を含み、含有される(A)と(B)の重量比が1:0.4〜0.8である、
整髪液組成物。 - 請求項4に記載の整髪液組成物と噴霧ガスとを混合する工程を含む、スプレー用の毛髪に適用するための組成物の製造方法。
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