JP6687843B2 - 五フッ化ヨウ素の製造方法 - Google Patents

五フッ化ヨウ素の製造方法 Download PDF

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Publication number: JP6687843B2
Authority: JP; Japan
Prior art keywords: iodine; pentafluoride; heptafluoride; gas; producing
Prior art date: 2015-07-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Active

Application number

JP2016076936A

Other languages

English (en)

Japanese (ja)

Other versions

JP2017024971A (ja

Inventor

真聖長友

晋也池田

茂朗柴山

柴山　　茂朗

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Central Glass Co Ltd

Original Assignee

Central Glass Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2015-07-23

Filing date

2016-04-07

Publication date

2020-04-28

2016-04-07 Application filed by Central Glass Co Ltd filed Critical Central Glass Co Ltd

2016-04-21 Priority to CN201680037046.8A priority Critical patent/CN107709229B/zh

2016-04-21 Priority to KR1020177035930A priority patent/KR102014907B1/ko

2016-04-21 Priority to PCT/JP2016/062607 priority patent/WO2017013916A1/ja

2016-06-15 Priority to TW108117971A priority patent/TWI695813B/zh

2016-06-15 Priority to TW105118823A priority patent/TWI683790B/zh

2017-02-02 Publication of JP2017024971A publication Critical patent/JP2017024971A/ja

2020-04-28 Application granted granted Critical

2020-04-28 Publication of JP6687843B2 publication Critical patent/JP6687843B2/ja

Status Active legal-status Critical Current

2036-04-07 Anticipated expiration legal-status Critical

Links

CEBDXRXVGUQZJK-UHFFFAOYSA-N 2-methyl-1-benzofuran-7-carboxylic acid Chemical compound C1=CC(C(O)=O)=C2OC(C)=CC2=C1 CEBDXRXVGUQZJK-UHFFFAOYSA-N 0.000 title claims description 171
238000004519 manufacturing process Methods 0.000 title claims description 66
XRURPHMPXJDCOO-UHFFFAOYSA-N iodine heptafluoride Chemical compound FI(F)(F)(F)(F)(F)F XRURPHMPXJDCOO-UHFFFAOYSA-N 0.000 claims description 126
238000006243 chemical reaction Methods 0.000 claims description 109
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 99
239000011630 iodine Substances 0.000 claims description 98
229910052740 iodine Inorganic materials 0.000 claims description 98
239000007791 liquid phase Substances 0.000 claims description 69
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 61
239000011737 fluorine Substances 0.000 claims description 61
229910052731 fluorine Inorganic materials 0.000 claims description 61
239000007787 solid Substances 0.000 claims description 19
239000007788 liquid Substances 0.000 claims description 17
PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 14
229910001512 metal fluoride Inorganic materials 0.000 claims description 13
239000000945 filler Substances 0.000 claims description 11
238000003756 stirring Methods 0.000 claims description 11
PDJAZCSYYQODQF-UHFFFAOYSA-N iodine monofluoride Chemical compound IF PDJAZCSYYQODQF-UHFFFAOYSA-N 0.000 claims description 10
150000001875 compounds Chemical class 0.000 claims description 3
239000007789 gas Substances 0.000 description 122
235000019000 fluorine Nutrition 0.000 description 59
239000012071 phase Substances 0.000 description 27
239000011261 inert gas Substances 0.000 description 13
238000000034 method Methods 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
238000001816 cooling Methods 0.000 description 7
230000007423 decrease Effects 0.000 description 7
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
230000000052 comparative effect Effects 0.000 description 6
229910001873 dinitrogen Inorganic materials 0.000 description 5
238000000137 annealing Methods 0.000 description 4
239000000203 mixture Substances 0.000 description 4
206010024769 Local reaction Diseases 0.000 description 3
229910052786 argon Inorganic materials 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
239000002184 metal Substances 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
239000008188 pellet Substances 0.000 description 3
229910001220 stainless steel Inorganic materials 0.000 description 3
239000010935 stainless steel Substances 0.000 description 3
238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
238000007664 blowing Methods 0.000 description 2
230000020169 heat generation Effects 0.000 description 2
239000001307 helium Substances 0.000 description 2
229910052734 helium Inorganic materials 0.000 description 2
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
DBJLJFTWODWSOF-UHFFFAOYSA-L nickel(ii) fluoride Chemical compound F[Ni]F DBJLJFTWODWSOF-UHFFFAOYSA-L 0.000 description 2
239000000126 substance Substances 0.000 description 2
229910004261 CaF 2 Inorganic materials 0.000 description 1
238000004497 NIR spectroscopy Methods 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000005265 energy consumption Methods 0.000 description 1
239000012025 fluorinating agent Substances 0.000 description 1
238000003682 fluorination reaction Methods 0.000 description 1
125000001153 fluoro group Chemical group F* 0.000 description 1
239000000463 material Substances 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
238000000465 moulding Methods 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
239000003507 refrigerant Substances 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
238000004611 spectroscopical analysis Methods 0.000 description 1
231100000331 toxic Toxicity 0.000 description 1
230000002588 toxic effect Effects 0.000 description 1
229910021561 transition metal fluoride Inorganic materials 0.000 description 1
JOHWNGGYGAVMGU-UHFFFAOYSA-N trifluorochlorine Chemical compound FCl(F)F JOHWNGGYGAVMGU-UHFFFAOYSA-N 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

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Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/24—Inter-halogen compounds

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Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP2016076936A 2015-07-23 2016-04-07 五フッ化ヨウ素の製造方法 Active JP6687843B2 (ja)

Priority Applications (5)

Application Number	Priority Date	Filing Date	Title
CN201680037046.8A CN107709229B (zh)	2015-07-23	2016-04-21	五氟化碘的制造方法
KR1020177035930A KR102014907B1 (ko)	2015-07-23	2016-04-21	5불화 요오드의 제조 방법
PCT/JP2016/062607 WO2017013916A1 (ja)	2015-07-23	2016-04-21	五フッ化ヨウ素の製造方法
TW108117971A TWI695813B (zh)	2015-07-23	2016-06-15	五氟化碘之製造方法
TW105118823A TWI683790B (zh)	2015-07-23	2016-06-15	七氟化碘之製造方法

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
JP2015145678		2015-07-23
JP2015145678		2015-07-23

Publications (2)

Publication Number	Publication Date
JP2017024971A JP2017024971A (ja)	2017-02-02
JP6687843B2 true JP6687843B2 (ja)	2020-04-28

Family

ID=57949448

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2016076936A Active JP6687843B2 (ja)	2015-07-23	2016-04-07	五フッ化ヨウ素の製造方法

Country Status (4)

Country	Link
JP (1)	JP6687843B2 (zh)
KR (1)	KR102014907B1 (zh)
CN (1)	CN107709229B (zh)
TW (2)	TWI683790B (zh)

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4108966A (en)	1977-10-26	1978-08-22	Air Products & Chemicals, Inc.	Preparation of iodine pentafluoride by direct fluorination of molten iodine
JPS58145602A (ja)	1982-02-22	1983-08-30	Kanto Denka Kogyo Kk	五フツ化ヨウ素の製造方法
CN1241984A (zh) *	1996-12-19	2000-01-19	英国核燃料公众有限公司	用于贮存、运输和制备活性氟的装置和方法
JP2008100881A (ja)	2006-10-20	2008-05-01	Daikin Ind Ltd	五フッ化ヨウ素の製造法
CN101528593B (zh) *	2006-10-20	2013-02-27	大金工业株式会社	五氟化碘的制造方法
JP4693823B2 (ja) *	2007-06-18	2011-06-01	セントラル硝子株式会社	七フッ化ヨウ素の製造法
JP5413201B2 (ja) *	2007-12-27	2014-02-12	セントラル硝子株式会社	フッ素化気体化合物の製造方法及び装置
CN101214927B (zh) *	2008-01-17	2010-12-22	核工业理化工程研究院华核新技术开发公司	五氟化碘的制备方法
US8142549B2 (en) *	2008-03-26	2012-03-27	Matheson Tri-Gas, Inc.	Purification of fluorine containing gases and systems and materials thereof
JP5470844B2 (ja) *	2008-12-26	2014-04-16	ダイキン工業株式会社	五フッ化ヨウ素の製造方法
CN101920937B (zh) *	2010-08-23	2012-01-04	福建省邵武市永飞化工有限公司	五氟化碘的制备方法与反应设备
JP2013203571A (ja) *	2012-03-28	2013-10-07	Central Glass Co Ltd	フッ素ガスの製造方法とその装置
JP6201496B2 (ja) *	2013-08-02	2017-09-27	セントラル硝子株式会社	Ｉｆ７由来フッ化ヨウ素化合物の回収方法及び回収装置
CN103754826B (zh) *	2013-12-17	2016-02-10	福建省邵武市永晶化工有限公司	一种五氟化碘生产设备和生产方法

2016
- 2016-04-07 JP JP2016076936A patent/JP6687843B2/ja active Active
- 2016-04-21 CN CN201680037046.8A patent/CN107709229B/zh active Active
- 2016-04-21 KR KR1020177035930A patent/KR102014907B1/ko active IP Right Grant
- 2016-06-15 TW TW105118823A patent/TWI683790B/zh active
- 2016-06-15 TW TW108117971A patent/TWI695813B/zh active

Also Published As

Publication number	Publication date
TWI695813B (zh)	2020-06-11
KR102014907B1 (ko)	2019-08-27
TW201934475A (zh)	2019-09-01
JP2017024971A (ja)	2017-02-02
KR20180006439A (ko)	2018-01-17
TWI683790B (zh)	2020-02-01
TW201708098A (zh)	2017-03-01
CN107709229A (zh)	2018-02-16
CN107709229B (zh)	2020-06-23

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