JP6508836B2 - 殺菌・殺カビ組成物 - Google Patents
殺菌・殺カビ組成物 Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/60—1,4-Diazines; Hydrogenated 1,4-diazines
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/74—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,3
- A01N43/78—1,3-Thiazoles; Hydrogenated 1,3-thiazoles
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/82—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with three ring hetero atoms
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
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- A61K47/12—Carboxylic acids; Salts or anhydrides thereof
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Description
Rは、水素またはメトキシであり;
Qは、
R1は、水素、ハロゲンまたはC1〜C6アルキルであり;
R2は、水素、ハロゲン、C1〜C6アルキル、C2〜C6アルケニル、C3〜C6アルキニル、C3〜C6シクロアルキル−C3〜C6アルキニル、ハロフェノキシ、ハロフェニル−C3〜C6アルキニル、C(C1〜C4アルキル)=NO−C1〜C4アルキル、C1〜C6ハロアルキル、C1〜C6ハロアルコキシ、C2〜C6ハロアルケニルまたはC2〜C6ハロアルケニルオキシであり;
R3は、水素、ハロゲン、C1〜C6アルキルであり;
R4、R5およびR6は、相互に独立して、水素、ハロゲンまたは−≡−R7であり;ただし、R4、R5およびR6の少なくとも1つは水素ではなく;
R7は、水素、C1〜C6アルキル、C1〜C6ハロアルキルまたはC1〜C4アルコキシアルキルである)
であり;ならびに
R8は、水素またはメトキシである)
および、農芸化学的に許容可能な塩、立体異性体、ジアステレオ異性体、エナンチオマーならびにこれらの化合物の互変異性体であり;
ならびに、コンポーネント(B)は、
(B1)式(II)の化合物
(B2)フェンピラザミン;
(B3)イソフェタミド;
(B4)オキサチアピプロリン;
(B5)トルプロカルブ;
(B6)フルフェノキシストロビン;
(B7)BLAD;
(B8)UK−2Aプロシド、すなわち、以下の構造
(B9)式(III)の化合物
(B10)クモキシストロビン;
(B11)マンデストロビン;
(B12)テブフロキン;
(B13)トリクロピリカルブ;
(B14)式IVの化合物
(B15)式Vの化合物
(B16)マンジプロパミド;
からなる群から選択される化合物、または、これらの農芸化学的に許容可能な塩である。
ppm=1リットルの噴霧混合物当たりの活性処方成分(=a.i.)のミリグラム量
X=p ppmの活性処方成分を用いた場合の活性処方成分(A)による作用の割合
Y=q ppmの活性処方成分を用いた場合の活性処方成分(B)による作用の割合。
式(II)の化合物
式(II)の化合物
式(II)の化合物
式(II)の化合物
フェンピラザミン+TX;
イソフェタミド+TX;
オキサチアピプロリン+TX;
トルプロカルブ+TX;
フルフェノキシストロビン+TX;
BLAD+TX;
UK−2Aプロシド+TX;
式(III)の化合物
クモキシストロビン+TX;
マンデストロビン+TX;
テブフロキン+TX;
(B13)トリクロピリカルブ+TX;
(B14)式(IV)の化合物
(B15)式(V)の化合物
(B16)マンジプロパミド+TX。
1.Syngenta Seeds SAS,Chemin de l’Hobit 27,F−31 790 St.Sauveur,France製Bt11トウモロコシ、登録番号C/FR/96/05/10。切断型CryIA(b)トキシンのトランスジェニック発現により、アワノメイガ(ヨーロッパアワノメイガ(Ostrinia nubilalis)およびセサミアノナグリオイデス(Sesamia nonagrioides))に対する耐性が付与された遺伝子操作されたトウモロコシ(Zea mays)。Bt11トウモロコシはまた、酵素PATをトランスジェニック発現して除草剤グルホシネートアンモニウムに対する耐容性が達成されている。
果実および野菜におけるアルテルナリア属(Alternaria)種、
しゅく穀作物におけるアスコキタ属(Ascochyta)種、
イチゴ、トマト、ヒマワリ、しゅく穀作物、野菜およびブドウにおけるボトリチス シネレア(Botrytis cinerea)、
ピーナッツにおけるセルコスポラ アラキディコーラ(Cercospora arachidicola)、
穀類におけるコクリオボルスサチブス(Cochliobolus sativus)、
しゅく穀作物におけるコレトトリカム(Colletotrichum)種、
穀類におけるエリシフェ属(Erysiphe)種、
ウリ科植物におけるエリシフェシコラセアラム(Erysiphe cichoracearum)およびスファエロテカフリギネア(Sphaerotheca fuliginea)、
穀類およびトウモロコシにおけるフザリウム属(Fusarium)種、
穀類および芝生におけるゲーウマノミセスグラミニス(Gaeumannomyces graminis)、
トウモロコシ、イネおよびジャガイモにおけるヘルミントスポリウム属(Helminthosporium)種、
コーヒーにおけるヘミレイア バスタトリクス(Hemileia vastatrix)、
コムギおよびライ麦におけるマイクロドキウム属(Microdochium)種、
ダイズにおけるファコプソラ属(Phakopsora)種、
穀類、広葉作物および多年生植物におけるプッシニア属(Puccinia)種、
穀類におけるシュードセルコスポレラ属(Pseudocercosporella)種、
バラにおけるファラグミジウムムクロナツム(Phragmidium mucronatum)、
果実におけるポドスファエラ属(Podosphaera)種、
オオムギにおけるピレノフォラ属(Pyrenophora)種、
イネにおけるイモチ病菌(Pyricularia oryzae)、
オオムギにおけるラムラリアコロシグニ(Ramularia collo−cygni)、
綿、ダイズ、穀類、トウモロコシ、ジャガイモ、イネおよび芝生におけるリゾクトニア属(Rhizoctonia)種、
オオムギおよびライ麦におけるリンコスポリウムセカリス(Rhynchosporium secalis)種、
芝生、レタス、野菜および油種子セイヨウアブラナにおけるスクレロティニア属(Sclerotinia)種、
穀類、ダイズおよび野菜におけるセプトリア属(Septoria)種、
トウモロコシにおけるスファセロテカレイリアナ(Sphacelotheca reilliana)、
穀類におけるティレチア属(Tilletia)種、
ブドウにおける、ウンシヌラ ネカトル(Uncinula necator)、ガイグナルディア ビドウェリイ(Guignardia bidwellii)およびホモプシス ビティコーラ(Phomopsis viticola)、
ライ麦におけるウロシスティスオクルタ(Urocystis occulta)、
穀類およびトウモロコシにおけるウスチラゴ属(Ustilago)種、
果実におけるベンチュリア属(Venturia)種、
果実におけるモニリニア属(Monilinia)種、
柑橘類およびリンゴにおけるアオカビ属(Penicillium)種。
ダニ目(Acarina)から、例えば、
アシブトコナダニ(Acarus siro)、アケリアシェルドニ(Aceria sheldoni)、リンゴサビダニ(Aculus schlechtendali)、アンブリオンマ属の一種(Amblyomma spp.)、ナガヒメダニ属の一種(Argas spp.)、オウシマダニ属の一種(Boophilus spp.)、ブレビパルプス属の一種(Brevipalpus spp.)、クローバーハダニ(Bryobia praetiosa)、カリピトリメルス属の一種(Calipitrimerus spp.)、ショクヒヒゼンダニ属の一種(Chorioptes spp.)、ワクモ(Dermanyssus gallinae)、エオテトラニクスカッピニ(Eotetranychus carpini)、エリオフィエス属の一種(Eriophyes spp.)、イボマダニ属の一種(Hyalomma spp.)、マダニ属の一種(Ixodes spp.)、オリゴニクスプラテンシス(Olygonychus pratensis)、カズキダニ属の一種(Ornithodoros spp.)、パノニクス属の一種(Panonychus spp.)、ミカンサビダニ(Phyllocoptruta oleivora)、チャノホコリダニ(Polyphagotarsonemus latus)、キュウセンヒゼンダニ属の一種(Psoroptes spp.)、コイタマダニ属の一種(Rhipicephalus spp.)、リゾグリフス属の一種(Rhizoglyphus spp.)、サルコプテス属の一種(Sarcoptes spp.)、ホコリダニ属の一種(Tarsonemus spp.)およびテトラニクス属の一種(Tetranychus spp.)であり;
シラミ目(Anoplura)から、例えば、
ブタジラミ属の一種(Haematopinus spp.)、ケモノホソジラミ属の一種(Linognathus spp.)、ペディクルス属の一種(Pediculus spp.)、ペムフィグス属の一種(Pemphigus spp.)およびフィロキセラ属の一種(Phylloxera spp.)であり;
鞘翅目(Coleoptera)から、例えば、
アグリオテス属の一種(Agriotes spp.)、アントノムス属の一種(Anthonomus spp.)、アトマリアリネアリス(aria linearis)、カエトクネマチビアリス(Chaetocnema tibialis)、コスモポリテス属の一種(Cosmopolites spp.)、クルクリオ属の一種(Curculio spp.)、デルメステス属の一種(Dermestes spp.)、ディアブロティカ属の一種(Diabrotica spp.)、エピラクナ属の一種(Epilachna spp.)、エレムヌス属の一種(Eremnus spp.)、コロラドハムシ(Leptinotarsa decemlineata)、リッソルホプトルス属の一種(Lissorhoptrus spp.)、メロロンタ属の一種(Melolontha spp.)、オリジャエフィルス属の一種(Orycaephilus spp.)、オチオリンクス属の一種(Otiorhynchus spp.)、フリクチヌス属の一種(Phlyctinus spp.)、ポピリア属の一種(Popillia spp.)、プシリオデス属の一種(Psylliodes spp.)、リゾペルタ属の一種(Rhizopertha spp.)、コガネムシ類、シトフィルス属の一種(Sitophilus spp.)、シトトルガ属の一種(Sitotroga spp.)、ゴミムシダマシ属の一種(Tenebrio spp.)、トリボリウム属の一種(Tribolium spp.)およびトロゴデルマ属の一種(Trogoderma spp.)であり;
双翅目(Diptera)から、例えば、
ヤブカ属の一種(Aedes spp.)、アンテリゴナソカタ(Antherigona soccata)、ビビオホルツラヌス(Bibio hortulanus)、カリホラエリスロセファラ(Calliphora erythrocephala)、セラチチス属の一種(Ceratitis spp.)、オビキンバエ属の一種(Chrysomyia spp.)、イエカ属の一種(Culex spp.)、クテレブラ属の一種(Cuterebra spp.)、ダクス属の一種(Dacus spp.)、キイロショウジョウバエ(Drosophila melanogaster)、ヒメイエバエ属の一種(Fannia spp.)、ガストロフィラス属の一種(Gastrophilus spp.)、ツェツェバエ属の一種(Glossina spp.)、ヒフバエ属の一種(Hypoderma spp.)、ヒッポボスカ属の一種(Hyppobosca spp.)、リリオミザ属の一種(Liriomyza spp.)、ギンバエ属の一種(Lucilia spp.)、メラナグロミザ属の一種(Melanagromyza spp.)、イエバエ属の一種(Musca spp.)、ヒツジバエ属の一種(Oestrus spp.)、オルセオリア属の一種(Orseolia spp.)、オシネラフリット(Oscinella frit)、アカザモグリハナバエ(Pegomyia hyoscyami)、ホルビア属の一種(Phorbia spp.)、リンゴミバエ(Rhagoletis pomonella)、キノコバエ属の一種(Sciara spp.)、サシバエ属の一種(Stomoxys spp.)、アブ属の一種(Tabanus spp.)、タニア属の一種(Tannia spp.)およびガガンボ属の一種(Tipula spp.)であり;
カメムシ亜目(Heteroptera)から、例えば、
トコジラミ属の一種(Cimex spp.)、ジスタンチエラテオブロマ(Distantiella theobroma)、ジスデルクス属の一種(Dysdercus spp.)、オイキスツス属の一種(Euchistus spp.)、エウリガステル属の一種(Eurygaster spp.)、レプトコリサ属の一種(Leptocorisa spp.)、ネザラ属の一種(Nezara spp.)、ピエスマ属の一種(Piesma spp.)、ロドニウス属の一種(Rhodnius spp.)、サールベルゲラシングラリス(Sahlbergella singularis)、スコチノファラ属の一種(Scotinophara spp.)およびサシガメ属の一種(Triatoma spp.)であり;
同翅目(Homoptera)から、例えば、
アレウロトリキスフロッコスス(Aleurothrixus floccosus)、アレイロデスブラシカエ(Aleyrodes brassicae)、アオニジエラ属の一種(Aonidiella spp.)、アリマキ科(Aphididae)、ワタアブラムシ属の一種(Aphis spp.)、アスピジオツス属の一種(Aspidiotus spp.)、タバココナジラミ(Bemisia tabaci)、セロプラスタ属の一種(Ceroplaster spp.)、クリソムファルスアオニジウム(Chrysomphalus aonidium)、オンシツマルカイガラムシ(Chrysomphalus dictyospermi)、ヒラタカタカイガラムシ(Coccus hesperidum)、カキノヒメヨコバイ属の一種(エムポアスカ属の一種(Empoasca spp.))、リンゴワタムシ(Eriosoma larigerum)、エリスロネウラ属の一種(Erythroneura spp.)、カスカルジア属の一種(Gascardia spp.)、ラオデルファクス属の一種(Laodelphax spp.)、ミズキカタカイガラムシ(Lecanium corni)、レピドサフェス属の一種(Lepidosaphes spp.)、マクロシフス属の一種(Macrosiphus spp.)、ミズス属の一種(Myzus spp.)、ツマグロヨコバイ属の一種(Nephotettix spp.)、ニラパルバタ属の一種(Nilaparvata spp.)、パルラトリア属の一種(Parlatoria spp.)、ペムフィグス属の一種(Pemphigus spp.)、プラノコッカス属の一種(Planococcus spp.)、プセウダウラカスピス属の一種(Pseudaulacaspis spp.)、シュードコッカス属の一種(Pseudococcus spp.)、プシラ属の一種(Psylla spp.)、プルビナリアエチオピカ(Pulvinaria aethiopica)、クアドラズピジオツス属の一種(Quadraspidiotus spp.)、ロパロシフム属の一種(Rhopalosiphum spp.)、サイセチア属の一種(Saissetia spp.)、スカホイデウス属の一種(Scaphoideus spp.)、スチザフィス属の一種(Schizaphis spp.)、シトビオン属の一種(Sitobion spp.)、オンシツコナジラミ(Trialeurodes vaporariorum)、ミカントガリキジラミ(Trioza erytreae)およびニセヤノネカイガラムシ(Unaspis citri)であり;
膜翅目(Hymenoptera)から、例えば、
ヒメハキリアリ属(Acromyrmex)、アッタ属の一種(Atta spp.)、セフス属の一種(Cephus spp.)、ジプリオン属の一種(Diprion spp.)、マツハバチ科(Diprionidae)、シマトウヒハバチ(Gilpinia polytoma)、ホプロカンパ属の一種(Hoplocampa spp.)、ケアリ属の一種(Lasius spp.)、イエヒメアリ(Monomorium pharaonis)、ネオジプリオン属の一種(Neodiprion spp.)、ソレノプシス属の一種(Solenopsis spp.)およびベスパ属の一種(Vespa spp.)であり;
等翅目(Isoptera)から、例えば、
ヤマトシロアリ属の一種(Reticulitermes spp.)であり;
鱗翅目(Lepidoptera)から、例えば、
アクレリス属の一種(Acleris spp.)、アドキソフィエス属の一種(Adoxophyes spp.)、アエゲリア属の一種(Aegeria spp.)、アグロティス属の一種(Agrotis spp.)、アラバマアルギラセア(Alabama argillaceae)、アミロイス属の一種(Amylois spp.)、アンチカルシアゲマタリス(Anticarsia gemmatalis)、アルチップス属の一種(Archips spp.)、アルギロタエニア属の一種(Argyrotaenia spp.)、アウトグラファ属の一種(Autographa spp.)、アフリカズイム(Busseola fusca)、スジマダラメイガ(Cadra cautella)、モモシンクイガ(Carposina nipponensis)、キロ属の一種(Chilo spp.)、コリストネウラ属の一種(Choristoneura spp.)、クリシアアンビグエラ(Clysia ambiguella)、クナファロクロシス属の一種(Cnaphalocrocis spp.)、クネファシア属の一種(Cnephasia spp.)、コチリス属の一種(Cochylis spp.)、コレオフォラ属の一種(Coleophora spp.)、ケブカノメイガ(Crocidolomia binotalis)、クリプトフレビアロイコトレタ(Cryptophlebia leucotreta)、シジア属の一種(Cydia spp.)、ジアトラエア属の一種(Diatraea spp.)、ジパロプシスカスタネア(Diparopsis castanea)、エアリアス属の一種(Earias spp.)、エフェスチア属の一種(Ephestia spp.)、オイコスマ属の一種(Eucosma spp.)、ブドウホソハマキ(Eupoecilia ambiguella)、ユープロクチス属の一種(Euproctis spp.)、エウクソア属の一種(Euxoa spp.)、グラホリタ属の一種(Grapholita spp.)、ヘディアヌビフェラナ(Hedya nubiferana)、ヘリオティス属の一種(Heliothis spp.)、ハイマダラノメイガ(Hellula undalis)、アメリカシロヒトリ(Hyphantria cunea)、ケイフェリアリコペルシセラ(Keiferia lycopersicella)、レウコプテラシテラ(Leucoptera scitella)、リトコレチス属の一種(Lithocollethis spp.)、ホソバヒメハマキ(Lobesia botrana)、リマントリア属の一種(Lymantria spp.)、リオネチア属の一種(Lyonetia spp.)、マラコソマ属の一種(Malacosoma spp.)、ヨトウガ(Mamestra brassicae)、タバコスズメガ(Manduca sexta)、オペロフテラ属の一種(Operophtera spp.)、ヨーロッパアワノメイガ(Ostrinia nubilalis)、パメネ属の一種(Pammene spp.)、パンデミス属の一種(Pandemis spp.)、マツキリガ(Panolis flammea)、ワタアカミムシ(Pectinophora gossypiela)、ジャガイモガ(Phthorimaea operculella)、モンシロチョウ(Pieris rapae)、ピエリス属の一種(Pieris spp.)、コナガ(Plutella xylostella)、プレイス属の一種(Prays spp.)、シルポファガ属の一種(Scirpophaga spp.)、セサミア属の一種(Sesamia spp.)、スパルガノチス属の一種(Sparganothis spp.)、スポドプテラ属の一種(Spodoptera spp.)、シナンテドン属の一種(Synanthedon spp.)、タウメトポエア属の一種(Thaumetopoea spp.)、トルトリックス属の一種(Tortrix spp.)、イラクサギンウワバ(Trichoplusia ni)およびスガ属の一種(Yponomeuta spp.)であり;
食毛目(Mallophaga)から、例えば、
ダマリネア属の一種(Damalinea spp.)およびケモノハジラミ属の一種(Trichodectes spp.)であり;
直翅目(Orthoptera)から、例えば、
ゴキブリ属の一種(Blatta spp.)、チャバネゴキブリ属の一種(Blattella spp.)、ケラ属の一種(Gryllotalpa spp.)、マデイラゴキブリ(Leucophaea maderae)、トノサマバッタ属の一種(Locusta spp.)、ワモンゴキブリ属の一種(Periplaneta spp.)およびコオロギ属の一種(Schistocerca spp.)であり;
チャタテムシ目(Psocoptera)から、例えば、
リポセリス属の一種(Liposcelis spp.)であり;
ノミ目(Siphonaptera)から、例えば、
ナガノミ属の一種(Ceratophyllus spp.)、イヌノミ属の一種(Ctenocephalides spp.)およびケオプスネズミノミ(Xenopsylla cheopis)であり;
総翅目(Thysanoptera)から、例えば、
ハナアザミウマ属の一種(Frankliniella spp.)、ヘルシノトリプス属の一種(Hercinothrips spp.)、シルトトリプスアウランチィ(Scirtothrips aurantii)、タエニオトリプス属の一種(Taeniothrips spp.)、ミナミキイロアザミウマ(Thrips palmi)およびネギアザミウマ(Thrips tabaci)であり;
シミ目(Thysanura)から、例えば、
セイヨウシミ(Lepisma saccharina)であり;
例えば根こぶ線虫、ステムイールワーム(stem eelworm)およびハガレセンチュウといった線虫;
特に、例えばテンサイシストセンチュウ(Heterodera schachtii)、ヘテロドラアベネ(Heterodora avenae)およびヘテロドラトリフォリイ(Heterodora trifolii)といったシストセンチュウ属の一種(Heterodera spp.);例えばグロボデラロストキエンシス(Globodera rostochiensis)といったグロボデラ属の一種(Globodera spp.);例えばメロイドギネインコギニタ(Meloidogyne incoginita)およびメロイドギネジャバニカ(Meloidogynejavanica)といったネコブセンチュウ属の一種(Meloidogyne spp.);例えばネモグリセンチュウ属の一種(Radopholus similis)といったネモグリセンチュウ属の一種(Radopholus spp.);例えばプラチレンクスネグレクタンス(Pratylenchus neglectans)およびプラチレンクスペネトランス(Pratylenchus penetrans)といったネグサレセンチュウ属の一種(Pratylenchus);例えばミカンネセンチュウ(Tylenchulus semipenetrans)といったチレンクルス属の一種(Tylenchulus);ロンギドルス属(Longidorus)、トリコドルス属(Trichodorus)、キシフィネマ属(Xiphinema)、ジチレンクス属(Ditylenchus)、アフェレンコイデス属(Aphelenchoides)およびアングイナ属(Anguina);
十字花科植物ノミハムシ(フィロトレタ属の一種(Phyllotreta spp.));
根喰い虫(デリア属の一種(Delia spp.))ならびに
キャベツシードポッドゾウムシ(cabbage seedpod weevil)(シュートリンクス属の一種(Ceutorhynchus spp.))である。
式Iの化合物と、コンポーネント(B)または個別のこれらの化合物の各々との組み合わせ28部を、2部の芳香族溶剤および7部のトルエンジイソシアネート/ポリメチレン−ポリフェニルイソシアネート−混合物(8:1)と混合する。この混合物を、1.2部のポリビニルアルコール、0.05部の脱泡剤および51.6部の水の混合物中で、所望の粒径が達成されるまで乳化させる。このエマルジョンに、2.8部の1,6−ジアミノヘキサンの5.3部の水中の混合物を添加する。この混合物を重合反応が完了するまで撹拌する。
ウェルプレートにおける液体培養テスト:
真菌の液体培養から新たに調製した、または、極低温保管していた真菌の菌糸体断片または分生子懸濁液を栄養液体培地に直接混合した。テスト化合物のDMSO溶液(最大10mg/ml)を0.025% Tween20で50倍に希釈し、この溶液10μlをマイクロタイタープレート(96ウェル型)にピペットで入れた。次いで、真菌胞子を含有する栄養液体培地/菌糸体断片を加えて、被テスト化合物を最終濃度とした。テストプレートを暗中に24℃および96%rhでインキュベートした。真菌の成長の阻害を病原体応答系に応じて2〜4日間後に分光光学的に、および、視認により判定し、未処理の基準に対する抗真菌活性割合を算出した。
極低温保管していた真菌の分生子を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から2〜3日間後に分光光学的に、および、視認により判定した。
極低温保管していた真菌の分生子を、栄養液体培地(アカパンカビ用最少液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から3日間後に分光光学的に、および、視認により判定した。
極低温保管していた真菌の分生子を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から3日間後に分光光学的に、および、視認により判定した。
極低温保管していた真菌の菌糸体断片を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から3〜4日間後に分光光学的に、および、視認により判定した。
極低温保管していた真菌の分生子を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から3〜4日間後に分光光学的に、および、視認により判定した。
極低温保管していた真菌の分生子を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌胞子を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から4日間後に分光光学的に、および、視認により判定した。
真菌の新しく成長させた液体培養の菌糸体断片および卵胞子を、栄養液体培地(PDBジャガイモブドウ糖液体培地)に直接混合した。テスト化合物の(DMSO)溶液をマイクロタイタープレート(96ウェル型)に入れた後、真菌菌糸/胞子混合物を含有する栄養液体培地を加えた。テストプレートを24℃でインキュベートし、成長の阻害を、適用から2〜3日間後に、視認により判定した。
上記に概要を記載したテストの結果の代表例を以下の表3〜38に示す。これらのデータによって、上記に概要が記載されているとおり1種または複数種の真菌に対するテストにおいて、以下の、式(I)の化合物および(B1)式(II)の化合物、式(I)の化合物および(B2)フェンピラジン、式(I)の化合物および(B4)オキサチアピプロリン、式(I)の化合物および(B5)トルプロカルブ、式(I)の化合物および(B6)フルフェノキシストロビン、式(I)の化合物および(B9)式(III)の化合物、式(I)の化合物および(B10)クモキシストロビン、式(I)の化合物および(B11)マンデストロビン、式(I)の化合物およびB12)テブフロキン、式(I)の化合物および(B13)トリクロピリカルブ、式(I)の化合物および(B14)式(IV)の化合物の組み合わせの各々について、相乗的な殺菌・殺カビ活性が観察されることが示されている。各事例において、テストした式(I)の化合物は、化合物1.001(すなわち3−(ジフルオロメチル)−N−メトキシ−1−メチル−N−[1−メチル−2−(2,4,6−トリクロロフェニル)エチル]ピラゾール−4−カルボキサミド)であった。
本発明のまた別の態様は、以下のとおりであってもよい。
〔1〕 コンポーネント(A)として、式(I)の化合物
(式中、
Rは、水素またはメトキシであり;
Qは、
(式中、
R 1 は、水素、ハロゲンまたはC 1 〜C 6 アルキルであり;
R 2 は、水素、ハロゲン、C 1 〜C 6 アルキル、C 2 〜C 6 アルケニル、C 3 〜C 6 アルキニル、C 3 〜C 6 シクロアルキル−C 3 〜C 6 アルキニル、ハロフェノキシ、ハロフェニル−C 3 〜C 6 アルキニル、C(C 1 〜C 4 アルキル)=NO−C 1 〜C 4 アルキル、C 1 〜C 6 ハロアルキル、C 1 〜C 6 ハロアルコキシ、C 2 〜C 6 ハロアルケニルまたはC 2 〜C 6 ハロアルケニルオキシであり;
R 3 は、水素、ハロゲンまたはC 1 〜C 6 アルキルであり;ただし、R 1 、R 2 およびR 3 の少なくとも1つは水素ではなく;
R 4 、R 5 およびR 6 は、相互に独立して、水素、ハロゲンまたは−≡−R 7 であり;ただし、R 4 、R 5 およびR 6 の少なくとも1つは水素ではなく;
R 7 は、水素、C 1 〜C 6 アルキル、C 1 〜C 6 ハロアルキルまたはC 1 〜C 4 アルコキシアルキルである)
であり;ならびに
R 8 は、水素またはメトキシである)
および、農芸化学的に許容可能な塩、立体異性体、ジアステレオ異性体、エナンチオマーならびにこれらの化合物の互変異性体を含み;
ならびに、コンポーネント(B)として、
(B1)式(II)の化合物
(式中、両方のR 9 は等しく、メチル、エチル、n−プロピルまたはイソプロピルを表す);
(B2)フェンピラザミン;
(B3)イソフェタミド;
(B4)オキサチアピプロリン;
(B5)トルプロカルブ;
(B6)フルフェノキシストロビン;
(B7)BLAD;
(B8)UK−2Aプロシド;
(B9)式(III)の化合物
;
(B10)クモキシストロビン;
(B11)マンデストロビン;
(B12)テブフロキン;
(B13)トリクロピリカルブ;
(B14)式(IV)の化合物
;
(B15)式Vの化合物
;および
(B16)マンジプロパミド;
からなる群から選択される化合物、または、これらの農芸化学的に許容可能な塩を含む、植物病原体によって引き起こされる病害の防除に好適な組成物。
〔2〕 コンポーネント(A)が、化合物3−(ジフルオロメチル)−N−メトキシ−1−メチル−N−[1−メチル−2−(2,4,6−トリクロロフェニル)エチル]ピラゾール−4−カルボキサミドである、前記〔1〕に記載の組成物。
〔3〕 コンポーネント(B)が:
(B1)式(II)の化合物
(式中、両方のR 9 は等しく、メチル、エチル、n−プロピルまたはイソプロピルを表す);
(B2)フェンピラザミン;
(B4)オキサチアピプロリン;
(B5)トルプロカルブ;
(B6)フルフェノキシストロビン;
(B9)式(III)の化合物
;
(B10)クモキシストロビン;
(B11)マンデストロビン;
(B12)テブフロキン;
(B13)トリクロピリカルブ;または
(B14)式(IV)の化合物
である、前記〔1〕または前記〔2〕に記載の組成物。
〔4〕 コンポーネント(A)および(B)が相乗的に有効な量で存在する、前記〔1〕〜〔3〕のいずれか一項に記載の組成物。
〔5〕 (A)対(B)の重量比が1000:1〜1:1000である、前記〔1〕〜〔4〕のいずれか一項に記載の組成物。
〔6〕 農学的に許容可能な補助剤および/またはキャリアをさらに含む、前記〔1〕〜〔5〕のいずれか一項に記載の組成物。
〔7〕 植物病原体によって引き起こされる有用な植物またはその繁殖体における病害を防除する方法であって、前記有用な植物、その生息地またはその繁殖体に、前記〔1〕〜〔6〕のいずれか一項に記載の組成物を適用するステップを含む方法。
〔8〕 自然のライフサイクルから得られた植物および/もしくは動物由来の天然物質ならびに/またはその加工形態を保護する方法であって、植物および/もしくは動物由来の前記天然物質またはその加工形態に、前記〔1〕〜〔6〕のいずれか一項に記載のコンポーネント(A)および(B)の組み合わせを適用するステップを含む方法。
Claims (6)
- コンポーネント(A)として、化合物3−(ジフルオロメチル)−N−メトキシ−1−メチル−N−[1−メチル−2−(2,4,6−トリクロロフェニル)エチル]ピラゾール−4−カルボキサミド、前記化合物の農芸化学的に許容可能な塩、立体異性体、ジアステレオ異性体、エナンチオマーまたは互変異性体を含み;
ならびに、コンポーネント(B)として、
(B1)式(II)の化合物
(式中、両方のR9は等しく、メチル、エチル、n−プロピルまたはイソプロピルを表す);
(B2)フェンピラザミン;
(B4)オキサチアピプロリン;
(B5)トルプロカルブ;
(B6)フルフェノキシストロビン;
(B9)式(III)の化合物
;
(B10)クモキシストロビン;
(B11)マンデストロビン;
(B12)テブフロキン;
(B13)トリクロピリカルブ;および
(B14)式(IV)の化合物
からなる群から選択される化合物を含む、植物病原体によって引き起こされる病害の防除用組成物。 - コンポーネント(A)および(B)が相乗的に有効な量で存在する、請求項1に記載の組成物。
- (A)対(B)の重量比が1000:1〜1:1000である、請求項1〜2のいずれか一項に記載の組成物。
- 農学的に許容可能な補助剤および/またはキャリアをさらに含む、請求項1〜3のいずれか一項に記載の組成物。
- 植物病原体によって引き起こされる有用な植物またはその繁殖体における病害を防除する方法であって、前記有用な植物、その生息地またはその繁殖体に、請求項1〜4のいずれか一項に記載の組成物を適用するステップを含む方法。
- 自然のライフサイクルから得られた植物および/もしくは動物由来の天然物質ならびに/またはその加工形態を保護する方法であって、植物および/もしくは動物由来の前記天然物質またはその加工形態に、請求項1に記載のコンポーネント(A)および(B)を適用するステップを含む方法。
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CN106538572A (zh) * | 2015-09-18 | 2017-03-29 | 南京华洲药业有限公司 | 一种含氰烯菌酯和代森锰锌的杀菌组合物及其应用 |
CN106538581A (zh) * | 2015-09-18 | 2017-03-29 | 南京华洲药业有限公司 | 一种含氰烯菌酯和咪鲜胺锰盐的杀菌组合物及其应用 |
JP6810062B2 (ja) | 2016-02-01 | 2021-01-06 | 住友化学株式会社 | 有害生物防除組成物及び有害生物防除方法 |
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CN108605961A (zh) * | 2018-05-23 | 2018-10-02 | 深圳诺普信农化股份有限公司 | 一种含有氟唑菌酰羟胺的杀菌组合物及其应用 |
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