JP6373530B1 - C重油組成物 - Google Patents
C重油組成物 Download PDFInfo
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- JP6373530B1 JP6373530B1 JP2018513681A JP2018513681A JP6373530B1 JP 6373530 B1 JP6373530 B1 JP 6373530B1 JP 2018513681 A JP2018513681 A JP 2018513681A JP 2018513681 A JP2018513681 A JP 2018513681A JP 6373530 B1 JP6373530 B1 JP 6373530B1
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- heavy oil
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- sulfur content
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- 239000000295 fuel oil Substances 0.000 title claims abstract description 54
- 239000000203 mixture Substances 0.000 title claims abstract description 49
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 38
- 239000011593 sulfur Substances 0.000 claims abstract description 38
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 36
- IYYZUPMFVPLQIF-UHFFFAOYSA-N dibenzothiophene Chemical compound C1=CC=C2C3=CC=CC=C3SC2=C1 IYYZUPMFVPLQIF-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000009835 boiling Methods 0.000 claims abstract description 16
- 150000003464 sulfur compounds Chemical class 0.000 claims abstract description 12
- 239000003921 oil Substances 0.000 claims description 21
- 125000003118 aryl group Chemical group 0.000 claims description 10
- 238000006477 desulfuration reaction Methods 0.000 claims description 10
- 230000023556 desulfurization Effects 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000000446 fuel Substances 0.000 abstract description 17
- 230000020169 heat generation Effects 0.000 abstract description 4
- 238000012360 testing method Methods 0.000 description 16
- 238000010998 test method Methods 0.000 description 10
- 239000010779 crude oil Substances 0.000 description 9
- 239000007789 gas Substances 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 7
- 239000010959 steel Substances 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 239000003208 petroleum Substances 0.000 description 6
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical group C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 5
- 238000004821 distillation Methods 0.000 description 5
- 238000004364 calculation method Methods 0.000 description 4
- 229920001971 elastomer Polymers 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 229930195734 saturated hydrocarbon Natural products 0.000 description 4
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000002283 diesel fuel Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 231100000241 scar Toxicity 0.000 description 3
- HTIRHQRTDBPHNZ-UHFFFAOYSA-N Dibutyl sulfide Chemical compound CCCCSCCCC HTIRHQRTDBPHNZ-UHFFFAOYSA-N 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 230000000740 bleeding effect Effects 0.000 description 2
- 238000011088 calibration curve Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- TXKMVPPZCYKFAC-UHFFFAOYSA-N disulfur monoxide Inorganic materials O=S=S TXKMVPPZCYKFAC-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000013618 particulate matter Substances 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 239000003209 petroleum derivative Substances 0.000 description 2
- YNPNZTXNASCQKK-UHFFFAOYSA-N phenanthrene Chemical compound C1=CC=C2C3=CC=CC=C3C=CC2=C1 YNPNZTXNASCQKK-UHFFFAOYSA-N 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052815 sulfur oxide Inorganic materials 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- DGUACJDPTAAFMP-UHFFFAOYSA-N 1,9-dimethyldibenzo[2,1-b:1',2'-d]thiophene Natural products S1C2=CC=CC(C)=C2C2=C1C=CC=C2C DGUACJDPTAAFMP-UHFFFAOYSA-N 0.000 description 1
- MYAQZIAVOLKEGW-UHFFFAOYSA-N 4,6-dimethyldibenzothiophene Chemical compound S1C2=C(C)C=CC=C2C2=C1C(C)=CC=C2 MYAQZIAVOLKEGW-UHFFFAOYSA-N 0.000 description 1
- NICUQYHIOMMFGV-UHFFFAOYSA-N 4-Methyldibenzothiophene Chemical compound S1C2=CC=CC=C2C2=C1C(C)=CC=C2 NICUQYHIOMMFGV-UHFFFAOYSA-N 0.000 description 1
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000008264 cloud Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000003009 desulfurizing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 238000004231 fluid catalytic cracking Methods 0.000 description 1
- 239000002828 fuel tank Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
- C10L1/08—Liquid carbonaceous fuels essentially based on blends of hydrocarbons for compression ignition
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2200/00—Components of fuel compositions
- C10L2200/04—Organic compounds
- C10L2200/0407—Specifically defined hydrocarbon fractions as obtained from, e.g. a distillation column
- C10L2200/0438—Middle or heavy distillates, heating oil, gasoil, marine fuels, residua
- C10L2200/0446—Diesel
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2270/00—Specifically adapted fuels
- C10L2270/02—Specifically adapted fuels for internal combustion engines
- C10L2270/026—Specifically adapted fuels for internal combustion engines for diesel engines, e.g. automobiles, stationary, marine
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
Description
表1に記載の基材を表2に記載の容量比で混合して、実施例1〜4及び比較例1〜2に係るC重油組成物を得た。表1〜3に記載されている性状等は、下記のように測定した。
JIS K 2249「原油及び石油製品−密度試験方法及び密度・質量・容量換算表」に従って測定した。
引火点(℃):
JIS K 2265−3「引火点の求め方−第3部:ペンスキーマルテンス密閉法」に従って測定した。
JIS K 2270「原油及び石油製品−残留炭素分試験方法」に従って測定した。
動粘度(30℃)、動粘度(50℃):
JIS K 2283「原油及び石油製品−動粘度試験方法及び粘度指数算出方法」に従って測定した。
芳香族含有量と着火性との関連に着目した指標であり、芳香族性を簡便的に重油の密度、動粘度を用いて次式で算出される。
CCAI=D−140.7log{log(V+0.85)}−80.6
ここで、Dは密度(kg/m3@15℃)、Vは動粘度(mm2/s@50℃)を示す。
流動点(℃):
JIS K 2269「原油及び石油製品の流動点並びに石油製品曇り点試験方法」に従って測定した。
JPI−5S−70法「TLC/FID法による組成分析試験方法」に従って測定した。
窒素分:
JIS K 2609「原油及び石油製品‐窒素分試験方法」化学発光法に従って測定した。
硫黄分:
JIS K 2541−4「原油及び石油製品−硫黄分試験方法 第4部:放射線式励起法」に従って測定した。
硫黄化学発光検出器を備えたAgilent製ガスクロマトグラフ装置を用いてガスクロマトグラフ法で測定した。カラムはJ&WのDB−Sulfur SCDを用いた。ジベンゾチオフェンをヘキサンに溶解したものを測定し、ピークの位置をリテンションタイムとして求めた。またジブチルスルフィドを標準物質とし検量線を作製した。次に試料を測定し、ジベンゾチオフェンのピークを含むジベンゾチオフェンのリテンションタイム以降の位置にあるピークの総面積をジブチルスルフィドの検量線で定量してジベンゾチオフェンの沸点以上の沸点を有する硫黄化合物のC重油組成物中の硫黄含有量を求めた。ガスクロマトグラフの測定条件は、35℃で3分保持したのち、5℃/分で150℃まで昇温し、その後10℃/分で270℃まで昇温し、22分保持した。
ISO12156−1 軽油−潤滑性試験方法に定められた方法のうち、荷重のみを1000gfとしてHFRR試験を行い、固定鋼球の摩耗痕径を潤滑性能評価の指標とした。
<試験条件>
試験球 : 軸受鋼(SUJ−2)
荷重(P) : 1000gf
振動数 : 50Hz
ストローク : 1000μm
試験時間 : 75分
温度 : 60℃
測定方法 : 試験試料を試験浴に入れ、試料の温度を60℃に保持した。試験鋼球を鉛直方向に取付けた試験鋼球固定台に固定し、水平方向にセットした試験ディスクに荷重(1.96mN)をかけて押し付けた。試料浴内で完全に試料に浸漬した状態で、試験ディスクと接触しながら試験鋼球を50Hzの周波数で往復運動(振動)させた。試験終了後に固定鋼球の摩耗痕径(μm)を測定した。
JIS K 2279 「原油及び石油製品−発熱量試験方法及び計算による推定方法」により算出した。計算に必要な灰分および水分は測定の結果微量であったので、0質量%として計算した。
JIS K 6258に従って測定した。ゴム材はNBRを用い、温度は70℃、期間は1週間とした。
Claims (4)
- 硫黄分が0.100質量%以下、及びジベンゾチオフェンの沸点以上の沸点を有する硫黄化合物の硫黄含有量が5〜400質量ppmであって、
密度(15℃)が0.8700〜0.9400g/cm3、動粘度(50℃)が3.500〜25.000mm2/s、流動点が25.0℃以下、引火点が70.0℃以上、HFRRが500μm以下、及び総発熱量が39000J/L以上であることを特徴とするC重油組成物。 - 芳香族分が25.0〜70.0質量%である請求項1記載のC重油組成物。
- 硫黄分が0.100質量%以下、密度(15℃)が0.8700〜0.9100g/cm3、動粘度(50℃)が10.000〜25.000mm2/s、及び残留炭素分が0.1質量%以下である間接脱硫残油を10容量%以上含む請求項1又は2記載のC重油組成物。
- 前記間接脱硫残油を30〜95容量%、硫黄分が0.100質量%以下の分解軽油を5〜70容量%含む請求項3記載のC重油組成物。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016234525 | 2016-12-01 | ||
JP2016234525 | 2016-12-01 | ||
PCT/JP2017/042560 WO2018101244A1 (ja) | 2016-12-01 | 2017-11-28 | C重油組成物 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP6373530B1 true JP6373530B1 (ja) | 2018-08-15 |
JPWO2018101244A1 JPWO2018101244A1 (ja) | 2018-12-06 |
Family
ID=62242122
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2018513681A Active JP6373530B1 (ja) | 2016-12-01 | 2017-11-28 | C重油組成物 |
Country Status (4)
Country | Link |
---|---|
US (1) | US10760020B2 (ja) |
EP (1) | EP3549999A4 (ja) |
JP (1) | JP6373530B1 (ja) |
WO (1) | WO2018101244A1 (ja) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10604709B2 (en) | 2017-02-12 | 2020-03-31 | Magēmā Technology LLC | Multi-stage device and process for production of a low sulfur heavy marine fuel oil from distressed heavy fuel oil materials |
US11788017B2 (en) | 2017-02-12 | 2023-10-17 | Magëmã Technology LLC | Multi-stage process and device for reducing environmental contaminants in heavy marine fuel oil |
US12025435B2 (en) | 2017-02-12 | 2024-07-02 | Magēmã Technology LLC | Multi-stage device and process for production of a low sulfur heavy marine fuel oil |
US20180230389A1 (en) | 2017-02-12 | 2018-08-16 | Magēmā Technology, LLC | Multi-Stage Process and Device for Reducing Environmental Contaminates in Heavy Marine Fuel Oil |
KR20210106454A (ko) | 2018-12-28 | 2021-08-30 | 이데미쓰 고산 가부시키가이샤 | 연료유 조성물 |
JP7227787B2 (ja) * | 2019-02-22 | 2023-02-22 | コスモ石油株式会社 | 重油組成物および重油組成物の製造方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2009096855A (ja) * | 2007-10-16 | 2009-05-07 | Japan Energy Corp | 高発熱量燃料油組成物 |
JP2011046892A (ja) * | 2009-08-28 | 2011-03-10 | Jx Nippon Oil & Energy Corp | 外燃用燃料組成物及びその製造方法 |
US20120246999A1 (en) * | 2011-03-28 | 2012-10-04 | Exxonmobil Research And Engineering Company | Novel fuel compositions and methods for making same |
JP2015189891A (ja) * | 2014-03-28 | 2015-11-02 | 鹿島石油株式会社 | C重油の製造方法 |
Family Cites Families (12)
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US4526586A (en) * | 1982-09-24 | 1985-07-02 | The United States Of America As Represented By The Secretary Of Agriculture | Microemulsions from vegetable oil and aqueous alcohol with 1-butanol surfactant as alternative fuel for diesel engines |
US4557734A (en) * | 1984-08-08 | 1985-12-10 | The United States Of America As Represented By The Secretary Of Agriculture | Microemulsions from vegetable oil and lower alcohol with octanol surfactant as alternative fuel for diesel engines |
US7459597B2 (en) * | 2005-12-13 | 2008-12-02 | Neste Oil Oyj | Process for the manufacture of hydrocarbons |
EP2130895A1 (en) * | 2007-03-28 | 2009-12-09 | Nippon Oil Corporation | Gas oil composition |
JP5340230B2 (ja) * | 2010-06-30 | 2013-11-13 | Jx日鉱日石エネルギー株式会社 | C重油組成物 |
US20120167451A1 (en) * | 2010-07-06 | 2012-07-05 | New Generation Biofuels Holdings, Inc. | Pyrolysis oil based fuel and method of production |
JP5639532B2 (ja) * | 2011-05-26 | 2014-12-10 | Jx日鉱日石エネルギー株式会社 | C重油組成物およびその製造方法 |
US20130144098A1 (en) * | 2011-12-06 | 2013-06-06 | Phillips 66 Company | Direct conversion of biomass oxygenates to hydrocarbons |
JP5841422B2 (ja) * | 2011-12-19 | 2016-01-13 | Jx日鉱日石エネルギー株式会社 | C重油組成物およびその製造方法 |
AP2014007952A0 (en) * | 2012-03-05 | 2014-09-30 | Sasol Tech Pty Ltd | Heavy synthetic fuel |
JP5847673B2 (ja) | 2012-09-07 | 2016-01-27 | Jx日鉱日石エネルギー株式会社 | C重油組成物 |
MX2016014623A (es) * | 2014-05-22 | 2017-03-06 | Shell Int Research | Composiciones de combustible. |
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2017
- 2017-11-28 US US16/465,695 patent/US10760020B2/en active Active
- 2017-11-28 WO PCT/JP2017/042560 patent/WO2018101244A1/ja unknown
- 2017-11-28 JP JP2018513681A patent/JP6373530B1/ja active Active
- 2017-11-28 EP EP17875685.4A patent/EP3549999A4/en not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2009096855A (ja) * | 2007-10-16 | 2009-05-07 | Japan Energy Corp | 高発熱量燃料油組成物 |
JP2011046892A (ja) * | 2009-08-28 | 2011-03-10 | Jx Nippon Oil & Energy Corp | 外燃用燃料組成物及びその製造方法 |
US20120246999A1 (en) * | 2011-03-28 | 2012-10-04 | Exxonmobil Research And Engineering Company | Novel fuel compositions and methods for making same |
JP2015189891A (ja) * | 2014-03-28 | 2015-11-02 | 鹿島石油株式会社 | C重油の製造方法 |
Also Published As
Publication number | Publication date |
---|---|
EP3549999A4 (en) | 2020-08-05 |
WO2018101244A1 (ja) | 2018-06-07 |
EP3549999A1 (en) | 2019-10-09 |
JPWO2018101244A1 (ja) | 2018-12-06 |
US10760020B2 (en) | 2020-09-01 |
US20190300806A1 (en) | 2019-10-03 |
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