JP6309953B2 - ホログラムによって視覚的に変化可能な窓を含む機密書類および/または貴重書類 - Google Patents
ホログラムによって視覚的に変化可能な窓を含む機密書類および/または貴重書類 Download PDFInfo
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- JP6309953B2 JP6309953B2 JP2015527865A JP2015527865A JP6309953B2 JP 6309953 B2 JP6309953 B2 JP 6309953B2 JP 2015527865 A JP2015527865 A JP 2015527865A JP 2015527865 A JP2015527865 A JP 2015527865A JP 6309953 B2 JP6309953 B2 JP 6309953B2
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Landscapes
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Description
−少なくとも1つの感光性樹脂を含むとともに少なくとも1つのホログラム(H)を組み込む、少なくとも1つの層(P)と、
−熱または照射によって不透明になる少なくとも1つの透明の光学的に切替え可能な層(O)と、を有することを特徴とする、機密書類および/または貴重書類を提供する。
b)ポリエステルジオールおよび/またはポリエーテルジオール、好ましくはポリエーテルジオール、ならびに、
c)随意に鎖伸張剤。
Rは、ヘテロ原子(エーテル酸素等)によって置換され得るもしくは中断され得るアルキルもしくはアリールラジカル、または水素であり、Yは、元のスタータ(parent starter)である。
ここで、nが1以上、nが4以下、R1およびR2が互いに独立して水素、線状、分岐状、環状または複素環状の未置換型であり、またはヘテロ原子置換型の有機ラジカルであってもよい。R2が水素もしくはメチルであり、および/またはR1が線状、分岐状、環状もしくは複素環状の未置換型であり、またはヘテロ原子置換型の有機ラジカルであってもよいことが特に好ましい。
mが1以上であり、mが8以下であり、R3、R4およびR5が、互いに独立して水素であり、または、置換されておらず、またはヘテロ原子によって置換されていてもよい、線状、分岐状、環状もしくは複素環状の有機ラジカルであり、好ましくはラジカルR3、R4およびR5の少なくとも1つが少なくとも1つのフッ素原子によって置換され、より好ましくは、R3が、少なくとも1つのフッ素原子を有する有機ラジカルである。特に好みに応じて、R4は、置換されておらず、または例えばフッ素等のヘテロ原子によって置換されていてもよい、線状、分岐状、環状または複素環状の有機ラジカルである。
ここで、mfが水飽和後の染料の質量であり、mtが乾燥染料の質量である。mtは、例えば真空中で温度を上昇させて、特定量の染料を一定質量まで乾燥させることによって確認される。mfは、所定の湿度の空気中で特定量の染料を一定重量まで放置することによって決定される。
a)機密書類および/または貴重書類のための単一または多層の基体に凹部が組み込まれ、
b)凹部に適合するようにトリムされるとともに、
・少なくとも1つの感光性樹脂を含むとともに少なくとも1つのホログラム(H)を組み込む、少なくとも1つの層(P)と、
・熱または照射によって不透明になる少なくとも1つの透明の光学的に切替え可能な層(O)と、
を備える多層アセンブリが凹部に組み込まれ、
c)b)によって得られた構成が、少なくとも1つの熱可塑性物質を含む少なくとも2つの透明フィルムの間に置かれ、前記フィルムが、b)によって得られた構成と二次元的に少なくとも同じサイズであり、
d)c)によって得られた構成が積層される、
ことを特徴とする、本発明の機密書類および/または貴重書類を製造するための方法がさらに提供される。
・感光性樹脂配合物によって、層(S)を形成する基材フィルムに層(P)を適用し、層(S)が好ましくはポリカーボネートからなり、および/またはカード本体と同じ材料からなり、
・この層(P)にホログラム(H)を組み込み、
・層(O)を製造するために、その後に層(P)の上に樹脂フィルムを置き、
・更なる透明層を製造するために、層(O)を製造するために樹脂フィルムの上に更なる透明樹脂フィルムを置いてもよく、
・得られたフィルムスタックを積層して多層アセンブリを形成し、
・その後に、積層体から凹部に適合する部分を打ち抜くまたは切り抜くこと、
によって製造される。
2 計測デバイス
3 真空脱気デバイス
4 フィルタ
5 静的ミキサ
6 被覆デバイス
7 強制空気式ドライヤ
8 キャリア基材
9 ライナ層
ラインの機能は、「フィルム被覆ラインにおけるホログラフィック媒体の製造」の項に記述されている。図2は、露光波長633nm(赤)用の感光性樹脂フィルムにおいてホログラムを発生させるための装置を示している。装置の機能は、「感光性樹脂における反射ホログラムの製造」の項に記述されている。
使用されるフィルム:
フィルム1(D):Makrofol(登録商標)ID6−2、透明ポリカーボネートフィルム、一側−艶消し(6)、一側繊細な艶消し(第2の側)、厚さ300μm(Bayer MaterialScience AG製)。
成分D:Fascat4102 0.07%、ウレタン化触媒、ブチルスズトリ(2−エチルヘキサン酸)、Arkema GmbH(デュッセルドルフ、独国)の製品。
I.ホログラフィック感光性樹脂フィルムに使用される更なる物質の調製手順
ポリオール成分Bの調製:
1lのフラスコがスズオクトアート0.18g、ε−カプロラクトン374.8gおよび二官能性ポリテトラヒドロフランポリエーテルポリオール(500g/モル等価重量のOH)374.8gによって充填され、この初期充填物が120℃に加熱され、固形分(非揮発成分の画分)が99.5重量%以上であるまでその温度に維持された。それは、次いで冷却されて、ワックス状固形物としての生成物を与えた。
500mlの丸底フラスコに、2,6−ジ−tert−ブチル−4−メチルフェノール0.1g、ジブチルスズジラウレート(Desmorapid(登録商標)Z、Bayer MaterialScience AG(レヴァークーゼン、独国))0.05gおよび、酢酸エチル中の溶液濃度27%のトリ(p−イソシアネートフェニル)チオリン酸塩(Desmodur(登録商標)RFE、Bayer MaterialScience AG(レヴァークーゼン、独国)の製品)213.07gが導入され、60℃に加熱された。次いで、2−ヒドロキシエチルアクリレート42.37gが滴下され、イソシアネート含量が0.1%未満に低下するまで混合物が60℃でさらに維持された。これに、冷却が続き、減圧下での酢酸エチルの完全な除去が続いた。生成物は、部分的に結晶化した固体の形で得られた。
100mlの丸底フラスコに、2,6−ジ−tert−ブチル−4−メチルフェノール0.02g、Desmorapid(登録商標)Z0.01gおよび3−(メチルチオ)フェニルイソシアネート11.7gが導入され、60℃に加熱された。次いで、2−ヒドロキシエチルアクリレート8.2gが滴下され、イソシアネート含量が0.1%未満に低下するまで混合物が60℃でさらに維持された。これに、冷却が続いた。生成物は、淡黄色の液体の形で得られた。
2000mlの丸底フラスコに、Desmorapid(登録商標)Z0.02gおよび2,4,4−トリメチルヘキサン1,6−ジイソシアネート(TMDI)3.60gが導入され、70℃に加熱された。次いで、2,2,3,3,4,4,5,5,6,6,7,7−ドデカフルオロヘプタン−1−オール11.39gが滴下され、イソシアネート含量が0.1%に低下するまで混合物が70℃でさらに維持された。これに、冷却が続いた。生成物は、無色オイルの形で得られた。
以下には、図1のラインにおける感光性樹脂配合物からのフィルムの形のホログラフィック媒体の連続製造について記述する。
IIのホログラフィック媒体内への露光によってホログラムを導入するために、図2の計測装備が使用された。これらのホログラムは、レーザ波長633nmの単色ホログラムであった。それらを製造するために、フィルムの断片が暗がりで切り離され、ライニングフィルムが除去され、フィルムは、感光性樹脂側を下向きにして、50×75mm、厚さ1mmのサイズのガラスの上に気泡なしで積層された。使用されたガラスは、Schott AG(マインツ、独国)製のコーニングガラスであった。
a)製造された機密書類は、図4に示されており、以下のように製造された。以下のフィルムシートは、GMP Laminart製の470LSIロールラミネータを使用して積層された。選ばれた積層温度:120℃、積層速度2.4m/分:
フィルム2(O)
フィルム2と接触する感光性樹脂被覆を有するフィルム3(P+S)。
Claims (13)
- 多層アセンブリから形成される少なくとも1つの窓を備える機密書類および/または貴重書類において、前記多層アセンブリが、
少なくとも1つの感光性樹脂を含むとともに少なくとも1つのホログラム(H)を組み込む、少なくとも1つの層(P)と、
熱または照射によって不透明になる少なくとも1つの透明の光学的に切替え可能な層(O)と、
を有し、
前記透明の光学的に切替え可能な層(O)が、少なくとも1つの光変色性または熱変色性の材料または組成物を含む少なくとも1つの透明の熱可塑性ポリウレタンの層であり、
前記層(P)の前記感光性樹脂が、ポリオール成分、ポリイソシアネート成分、描画モノマーおよび光開始剤を含む感光性樹脂配合物から調製された感光性樹脂であることを特徴とする、機密書類および/または貴重書類。 - 前記ホログラム(H)が、体積ホログラムであり、好ましくは反射ホログラムであることを特徴とする、請求項1に記載の機密書類および/または貴重書類。
- 前記透明の光学的に切替え可能な層(O)が、少なくとも1つの光変色性色素または少なくとも1つの光変色性染料を含む少なくとも1つの透明の熱可塑性ポリウレタンの層であることを特徴とする、請求項1または2に記載の機密書類および/または貴重書類。
- 前記感光性樹脂配合物の前記描画モノマーが少なくとも1つの単官能性および/または1つの多官能性のウレタン(メタ)アクリレートを含むことを特徴とする、請求項1乃至4のいずれか1項に記載の機密書類および/または貴重書類。
- 確認書類、好ましくはIDカードであることを特徴とする、請求項1乃至5のいずれか1項に記載の機密書類および/または貴重書類。
- 前記機密書類および/または前記貴重書類の残りの内側部分および前記窓が、少なくとも1つの熱可塑性物質を含むとともに二次元的にそれぞれ前記文書の全体を覆う、少なくとも2つの透明外側層の間に位置するように、前記窓が前記書類に組み込まれることを特徴とする、請求項1乃至6のいずれか1項に記載の機密書類および/または貴重書類。
- 前記窓が、少なくとも1つの熱可塑性物質を含むとともに前記層Pにおいて前記層Oから離れた側に位置する、少なくとも1つの更なる透明層を備えることを特徴とする、請求項1乃至7のいずれか1項に記載の機密書類および/または貴重書類。
- 前記窓が、少なくとも1つの熱可塑性物質を含む少なくとも2つの更なる透明層を備え、前記透明層の一方が前記層Pにおいて前記層Oから離れた側に位置し、他方が前記層Oにおいて前記層Pから離れた側に位置することを特徴とする、請求項1乃至8のいずれか1項に記載の機密書類および/または貴重書類。
- 少なくとも1つの熱可塑性物質を含む前記透明外側層が、少なくとも1つのポリカーボネートまたはコポリカーボネートを含む層であることを特徴とする、請求項7に記載の機密書類および/または貴重書類。
- 前記窓の前記多層アセンブリにおける少なくとも1つの熱可塑性物質を含む前記更なる透明層が、少なくとも1つのポリカーボネートまたはコポリカーボネートを含む層であることを特徴とする、請求項8または9に記載の機密書類および/または貴重書類。
- 請求項1乃至11のいずれか1項に記載された機密書類および/または貴重書類を製造するための方法において、
a)機密書類および/または貴重書類のための単一または多層の基体に凹部が組み込まれ、
b)前記凹部に適合するようにトリムされるとともに、
少なくとも1つの感光性樹脂を含むとともに少なくとも1つのホログラム(H)を組み込む、少なくとも1つの層(P)と、
熱または照射によって不透明になる少なくとも1つの透明の光学的に切替え可能な層(O)と、
を含む多層アセンブリが前記凹部に組み込まれ、
c)b)によって得られた構成が、二次元的に少なくとも等しいサイズであるとともに少なくとも1つの熱可塑性物質を含む、少なくとも2つの透明フィルムの間に置かれ、
d)c)によって得られた構成が積層されることを特徴とする、方法。 - b)で前記凹部に組み込まれる前記多層アセンブリが、少なくとも1つの熱可塑性物質を含む少なくとも1つの更なる透明層(S)をさらに備えるとともに、
感光性樹脂配合物によって、前記層(S)を形成する基材フィルムに前記層(P)を適用し、
この層(P)に前記ホログラム(H)を組み込み、
前記層(O)を製造するために、その後に前記層(P)の上にポリマーフィルムを置き、
更なる透明層を製造するために、前記層(O)を製造するために前記ポリマーフィルムの上に更なる透明ポリマーフィルムを置いてもよく、
得られたフィルムスタックを積層して多層アセンブリを形成し、
その後に、前記積層体から、前記凹部に適合する部分を打ち抜くまたは切り抜くこと、
によって製造されることを特徴とする、請求項12に記載の方法。
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EP2613319A1 (de) * | 2012-01-05 | 2013-07-10 | Bayer MaterialScience AG | Schichtverbund aus einem Photopolymerfilm und einer Klebstoffschicht |
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2013
- 2013-08-15 JP JP2015527865A patent/JP6309953B2/ja not_active Expired - Fee Related
- 2013-08-15 RU RU2015109872A patent/RU2015109872A/ru unknown
- 2013-08-15 EP EP13750059.1A patent/EP2888116B1/de active Active
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- 2013-08-15 CN CN201380044418.6A patent/CN104540685B/zh active Active
- 2013-08-15 US US14/422,768 patent/US9658595B2/en active Active
- 2013-08-15 WO PCT/EP2013/067075 patent/WO2014029686A1/de active Application Filing
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KR102089118B1 (ko) | 2020-03-13 |
RU2015109872A (ru) | 2016-10-10 |
US20150220057A1 (en) | 2015-08-06 |
EP2888116A1 (de) | 2015-07-01 |
KR20150047487A (ko) | 2015-05-04 |
WO2014029686A1 (de) | 2014-02-27 |
CN104540685B (zh) | 2017-09-26 |
TW201427841A (zh) | 2014-07-16 |
EP2888116B1 (de) | 2016-09-21 |
JP2015531705A (ja) | 2015-11-05 |
CN104540685A (zh) | 2015-04-22 |
US9658595B2 (en) | 2017-05-23 |
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