JP6267297B1 - 焼結体、スパッタリングターゲット及びその製造方法 - Google Patents
焼結体、スパッタリングターゲット及びその製造方法 Download PDFInfo
- Publication number
- JP6267297B1 JP6267297B1 JP2016167135A JP2016167135A JP6267297B1 JP 6267297 B1 JP6267297 B1 JP 6267297B1 JP 2016167135 A JP2016167135 A JP 2016167135A JP 2016167135 A JP2016167135 A JP 2016167135A JP 6267297 B1 JP6267297 B1 JP 6267297B1
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- JP
- Japan
- Prior art keywords
- sputtering target
- sintered body
- bulk resistivity
- thickness direction
- depth position
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000005477 sputtering target Methods 0.000 title claims abstract description 61
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 21
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 14
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 14
- 229910052738 indium Inorganic materials 0.000 claims abstract description 12
- 239000011701 zinc Substances 0.000 claims description 35
- 238000005245 sintering Methods 0.000 claims description 19
- 239000012298 atmosphere Substances 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 12
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000001301 oxygen Substances 0.000 claims description 11
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 8
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 6
- 229910003437 indium oxide Inorganic materials 0.000 claims description 5
- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000012300 argon atmosphere Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims description 2
- 239000010408 film Substances 0.000 description 24
- 238000000227 grinding Methods 0.000 description 21
- 239000013078 crystal Substances 0.000 description 11
- 230000007423 decrease Effects 0.000 description 10
- 238000005498 polishing Methods 0.000 description 8
- 238000004544 sputter deposition Methods 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 6
- 206010021143 Hypoxia Diseases 0.000 description 5
- 238000001816 cooling Methods 0.000 description 5
- 230000003247 decreasing effect Effects 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 238000007088 Archimedes method Methods 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000005401 electroluminescence Methods 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 238000001878 scanning electron micrograph Methods 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- 240000004282 Grewia occidentalis Species 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 229910007570 Zn-Al Inorganic materials 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- -1 but IZO (InZO Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- AMGQUBHHOARCQH-UHFFFAOYSA-N indium;oxotin Chemical compound [In].[Sn]=O AMGQUBHHOARCQH-UHFFFAOYSA-N 0.000 description 1
- 229940110676 inzo Drugs 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 239000002905 metal composite material Substances 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- YVTHLONGBIQYBO-UHFFFAOYSA-N zinc indium(3+) oxygen(2-) Chemical compound [O--].[Zn++].[In+3] YVTHLONGBIQYBO-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/08—Oxides
- C23C14/086—Oxides of zinc, germanium, cadmium, indium, tin, thallium or bismuth
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/453—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zinc, tin, or bismuth oxides or solid solutions thereof with other oxides, e.g. zincates, stannates or bismuthates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
- C23C14/3414—Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3284—Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3286—Gallium oxides, gallates, indium oxides, indates, thallium oxides, thallates or oxide forming salts thereof, e.g. zinc gallate
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Structural Engineering (AREA)
- Physical Vapour Deposition (AREA)
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016167135A JP6267297B1 (ja) | 2016-08-29 | 2016-08-29 | 焼結体、スパッタリングターゲット及びその製造方法 |
CN201710734442.2A CN107779821B (zh) | 2016-08-29 | 2017-08-24 | 烧结体、溅射靶及其制造方法 |
KR1020170107874A KR101921827B1 (ko) | 2016-08-29 | 2017-08-25 | 소결체, 스퍼터링 타깃 및 그 제조 방법 |
TW106129196A TWI649293B (zh) | 2016-08-29 | 2017-08-28 | Sintered body, sputtering target and manufacturing method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016167135A JP6267297B1 (ja) | 2016-08-29 | 2016-08-29 | 焼結体、スパッタリングターゲット及びその製造方法 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2017245322A Division JP6453990B2 (ja) | 2017-12-21 | 2017-12-21 | 焼結体、スパッタリングターゲット及びその製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP6267297B1 true JP6267297B1 (ja) | 2018-01-24 |
JP2018035013A JP2018035013A (ja) | 2018-03-08 |
Family
ID=61020963
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2016167135A Active JP6267297B1 (ja) | 2016-08-29 | 2016-08-29 | 焼結体、スパッタリングターゲット及びその製造方法 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP6267297B1 (zh) |
KR (1) | KR101921827B1 (zh) |
CN (1) | CN107779821B (zh) |
TW (1) | TWI649293B (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109072417B (zh) * | 2017-03-31 | 2020-06-16 | Jx金属株式会社 | 溅镀靶及其制造方法 |
JP6724057B2 (ja) * | 2018-03-30 | 2020-07-15 | Jx金属株式会社 | スパッタリングターゲット部材 |
JP2020143359A (ja) * | 2019-03-08 | 2020-09-10 | Jx金属株式会社 | スパッタリングターゲット部材の製造方法及びスパッタリングターゲット部材 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH10297962A (ja) * | 1997-04-28 | 1998-11-10 | Sumitomo Metal Mining Co Ltd | スパッタリングターゲット用ZnO−Ga2O3系焼結体およびその製造方法 |
JPH11302835A (ja) * | 1998-04-21 | 1999-11-02 | Sumitomo Metal Mining Co Ltd | ZnO系焼結体の製造方法 |
WO2008078486A1 (ja) * | 2006-12-25 | 2008-07-03 | Idemitsu Kosan Co., Ltd. | 透明導電膜の製造方法 |
WO2010125801A1 (ja) * | 2009-05-01 | 2010-11-04 | 株式会社アルバック | ZnO-Ga2O3系スパッタリングターゲット用焼結体及びその製造方法 |
JP2011068993A (ja) * | 1999-11-25 | 2011-04-07 | Idemitsu Kosan Co Ltd | スパッタリングターゲット、透明導電性酸化物、およびスパッタリングターゲットの製造方法 |
JP2015021165A (ja) * | 2013-07-19 | 2015-02-02 | 三菱マテリアル株式会社 | スパッタリングターゲット及びその製造方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100603128B1 (ko) * | 1999-05-10 | 2006-07-20 | 닛코킨조쿠 가부시키가이샤 | 스퍼터링 타겟트 |
JP5096250B2 (ja) * | 2008-07-18 | 2012-12-12 | 出光興産株式会社 | 酸化物焼結体の製造方法、酸化物焼結体、スパッタリングタ−ゲット、酸化物薄膜、薄膜トランジスタの製造方法及び半導体装置 |
WO2014112368A1 (ja) * | 2013-01-15 | 2014-07-24 | 出光興産株式会社 | スパッタリングターゲット、酸化物半導体薄膜及びそれらの製造方法 |
-
2016
- 2016-08-29 JP JP2016167135A patent/JP6267297B1/ja active Active
-
2017
- 2017-08-24 CN CN201710734442.2A patent/CN107779821B/zh active Active
- 2017-08-25 KR KR1020170107874A patent/KR101921827B1/ko active IP Right Grant
- 2017-08-28 TW TW106129196A patent/TWI649293B/zh active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH10297962A (ja) * | 1997-04-28 | 1998-11-10 | Sumitomo Metal Mining Co Ltd | スパッタリングターゲット用ZnO−Ga2O3系焼結体およびその製造方法 |
JPH11302835A (ja) * | 1998-04-21 | 1999-11-02 | Sumitomo Metal Mining Co Ltd | ZnO系焼結体の製造方法 |
JP2011068993A (ja) * | 1999-11-25 | 2011-04-07 | Idemitsu Kosan Co Ltd | スパッタリングターゲット、透明導電性酸化物、およびスパッタリングターゲットの製造方法 |
WO2008078486A1 (ja) * | 2006-12-25 | 2008-07-03 | Idemitsu Kosan Co., Ltd. | 透明導電膜の製造方法 |
WO2010125801A1 (ja) * | 2009-05-01 | 2010-11-04 | 株式会社アルバック | ZnO-Ga2O3系スパッタリングターゲット用焼結体及びその製造方法 |
JP2015021165A (ja) * | 2013-07-19 | 2015-02-02 | 三菱マテリアル株式会社 | スパッタリングターゲット及びその製造方法 |
Also Published As
Publication number | Publication date |
---|---|
CN107779821B (zh) | 2020-12-18 |
TWI649293B (zh) | 2019-02-01 |
KR101921827B1 (ko) | 2019-02-13 |
JP2018035013A (ja) | 2018-03-08 |
TW201806909A (zh) | 2018-03-01 |
CN107779821A (zh) | 2018-03-09 |
KR20180025225A (ko) | 2018-03-08 |
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