JP6208470B2 - 染毛剤組成物 - Google Patents
染毛剤組成物 Download PDFInfo
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- JP6208470B2 JP6208470B2 JP2013123197A JP2013123197A JP6208470B2 JP 6208470 B2 JP6208470 B2 JP 6208470B2 JP 2013123197 A JP2013123197 A JP 2013123197A JP 2013123197 A JP2013123197 A JP 2013123197A JP 6208470 B2 JP6208470 B2 JP 6208470B2
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Landscapes
- Cosmetics (AREA)
Description
(A)ローズヒップ油
(B)多価アルコール
(C)酸化染料又は直接染料
(D)サンザシエキス及び/又はセイヨウサンザシエキス
を含有する染毛剤組成物を提供するものである。
表1に示す染毛剤組成物の第一剤と表2に示す染毛剤組成物の第二剤とを第一剤:第二剤=1:1にて混合し染毛剤組成物を調製した。これを100%中国人白髪毛(ビューラックス社製)の毛束約2.0gに対して毛束と等量の染毛剤組成物をハケで均一に行きわたらせた後、毛束を室温に15分間放置した。放置後、約40℃の流水で染毛剤組成物を洗い流し、表3に示した試験用シャンプー約0.5gを塗布し、手で約30秒もみ洗いし、約40℃の流水で30秒間すすいだ。その後ドライヤーで乾燥させた。染着性を肉眼で評価した。それぞれ2本の毛束を染めた。
均一にしっかり染まっている(5点)、均一に染まっている(4点)、染まっている(3点)、ややムラがあり、あまり染まっていない(2点)、ムラがあり、ほとんど染まっていない(1点)の5段階で評価した。各パネラーの採点結果について平均点を算出し、平均値が4.6以上を「均一にしっかり染まっている:5」、3.6点以上4.5点以下を「均一に染まっている:4」、2.6点以上3.5点以下を「染まっている:3」、1.6以上2.5以下を「ややムラがあり、あまり染まっていない:2」、1点以上1.5点以下を「ムラがあり、ほとんど染まっていない:1」とし、又、「全員の評価が5点:6」として評価結果とした。
染毛工程で得た染色毛束2本のうち1本を表3に示した試験用シャンプー約0.5gを塗布し、手で約30秒もみ洗いし、約40℃の流水で30秒間すすいだ。その後ドライヤーで乾燥させた。この操作を10回繰り返した。そして色落ち具合(洗髪堅牢性試験)を肉眼で評価した。その場合、上記の染毛工程で得た残りの染色毛束(基準染色毛束)と比較し、評価した。
基準染色毛束と変わらない(5点)、基準染色毛束に比べて殆ど変わらない(4点)、基準染色毛束に比べて少し色落ちがある(3点)、染色毛束に比べて色落ちが目立つ(2点)、色落ちが激しい(色が殆ど残っていない)(1点)の5段階で評価した。各パネラーの採点結果について平均点を算出し、平均値が4.6以上を「基準染色毛束と変わらない:5」、3.6点以上4.5点以下を「基準染色毛束に比べて殆ど変わらない:4」、2.6点以上3.5点以下を「基準染色毛束に比べて少し色落ちがある:3」、1.6以上2.5以下を「染色毛束に比べて色落ちが目立つ:2」、1点以上1.5点以下を「色落ちが激しい(色が殆ど残っていない):1」とし、又、「全員の評価が5点:6」として評価結果とした。
実施例1〜7、比較例1〜5に示した染毛剤組成物を調製した。それぞれの染着性、洗髪堅牢性について評価し、その結果を表1に示した。
下記組成の第一剤がクリーム状、第二剤が液状で、第一剤:第二剤=1:2の比率で混合して乳液状となる染毛剤組成物を調製して評価を行った。
(第一剤)
成分 配合量(重量%)
1) パラフェニレンジアミン 1.00
2) レゾルシン 0.30
3) パラアミノフェノール 0.20
4) 5−アミノオルトクレゾール 0.10
5) セチルアルコール 4.00
6) 流動イソパラフィン 10.00
7) 流動パラフィン 5.00
8) ジメチルポリシロキサン 5.00
9) ポリオキシエチレンステアリルエーテル 5.00
10) 塩化ステアリルトリメチルアンモニウム(70%) 1.50
11) ステアリン酸 0.50
12) ローズヒップ油 0.50
13) 香料 0.50
14) ポリ塩化ジメチルメチレンピペリジニウム液 1.00
15) グリセリン 3.00
16) L−アスコルビン酸 0.30
17) エデト酸四ナトリウム四水塩 0.50
18) サンザシエキス(※3) 0.007
19) 1,3−ブチレングリコール 1.00
20) 大豆たん白加水分解物 0.50
21) 加水分解シルク液 0.50
22) モノエタノールアミン(80%) 6.00
23) 精製水 残量
合 計 100.00
※3:固形分換算
製法
成分1〜13を80℃にて加温溶融したものに、成分14〜17,23を85℃にて加温溶融したものを加えて混合する。次いで撹拌しながら冷却を行い、45℃にて成分18〜22を加え、室温まで撹拌しながら冷却を行い、第一剤を得た。
成分 配合量(重量%)
1) セチルアルコール 1.50
2) セチル硫酸ナトリウム 0.50
3) プロピレングリコール 6.00
4) ジエチレントリアミン五酢酸五ナトリウム液(40%) 2.00
5) ヒドロキシエタンジホスホン酸(60%) 0.10
6) リン酸 0.02
7) リン酸水素二ナトリウム 0.10
8) 過酸化水素水(35%) 16.60
9) 精製水 残量
合 計 100.00
製法
成分1〜5を80℃にて加温溶融したものに、成分6,7,9を85℃にて加温溶融したものを加えて混合する。次いで撹拌しながら冷却を行い、40℃にて成分8を加え、室温まで撹拌しながら冷却を行い、第二剤を得た。
Claims (3)
- アルカリ剤を含有する第一剤と酸化剤を含有する第二剤とを混合して用いる染毛剤組成物であって、第一剤と第二剤との混合物中に次の成分(A)〜(D)
(A)ローズヒップ油
(B)多価アルコール
(C)酸化染料又は直接染料
(D)サンザシエキス及び/又はセイヨウサンザシエキス
を含有する染毛剤組成物。 - (B)が1,3−ブチレングリコール、プロピレングリコール、ジプロピレングリコール、グリセリン、ポリエチレングリコールから選ばれる1種以上であることを特徴とする請求項1記載の染毛剤組成物。
- (B)の含有量が、混合物中の1.0〜5.0重量%であることを特徴とする請求項1〜2のいずれか一項記載の染毛剤組成物。
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