JP6135249B2 - 応力発光材料用原料組成物、応力発光材料、及びその応用 - Google Patents
応力発光材料用原料組成物、応力発光材料、及びその応用 Download PDFInfo
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- JP6135249B2 JP6135249B2 JP2013074422A JP2013074422A JP6135249B2 JP 6135249 B2 JP6135249 B2 JP 6135249B2 JP 2013074422 A JP2013074422 A JP 2013074422A JP 2013074422 A JP2013074422 A JP 2013074422A JP 6135249 B2 JP6135249 B2 JP 6135249B2
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- CXVGEDCSTKKODG-UHFFFAOYSA-N sulisobenzone Chemical compound C1=C(S(O)(=O)=O)C(OC)=CC(O)=C1C(=O)C1=CC=CC=C1 CXVGEDCSTKKODG-UHFFFAOYSA-N 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 229910002029 synthetic silica gel Inorganic materials 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 229910003451 terbium oxide Inorganic materials 0.000 description 1
- SCRZPWWVSXWCMC-UHFFFAOYSA-N terbium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[Tb+3].[Tb+3] SCRZPWWVSXWCMC-UHFFFAOYSA-N 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- LVEOKSIILWWVEO-UHFFFAOYSA-N tetradecyl 3-(3-oxo-3-tetradecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCC LVEOKSIILWWVEO-UHFFFAOYSA-N 0.000 description 1
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical compound FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 239000004308 thiabendazole Substances 0.000 description 1
- 235000010296 thiabendazole Nutrition 0.000 description 1
- WJCNZQLZVWNLKY-UHFFFAOYSA-N thiabendazole Chemical compound S1C=NC(C=2NC3=CC=CC=C3N=2)=C1 WJCNZQLZVWNLKY-UHFFFAOYSA-N 0.000 description 1
- 229960004546 thiabendazole Drugs 0.000 description 1
- 239000001016 thiazine dye Substances 0.000 description 1
- 239000001017 thiazole dye Substances 0.000 description 1
- QGHREAKMXXNCOA-UHFFFAOYSA-N thiophanate-methyl Chemical group COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC QGHREAKMXXNCOA-UHFFFAOYSA-N 0.000 description 1
- YRHRIQCWCFGUEQ-UHFFFAOYSA-N thioxanthen-9-one Chemical class C1=CC=C2C(=O)C3=CC=CC=C3SC2=C1 YRHRIQCWCFGUEQ-UHFFFAOYSA-N 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 229960000984 tocofersolan Drugs 0.000 description 1
- AOBORMOPSGHCAX-DGHZZKTQSA-N tocofersolan Chemical compound OCCOC(=O)CCC(=O)OC1=C(C)C(C)=C2O[C@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C AOBORMOPSGHCAX-DGHZZKTQSA-N 0.000 description 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- MZHULIWXRDLGRR-UHFFFAOYSA-N tridecyl 3-(3-oxo-3-tridecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCC MZHULIWXRDLGRR-UHFFFAOYSA-N 0.000 description 1
- DQWPFSLDHJDLRL-UHFFFAOYSA-N triethyl phosphate Chemical compound CCOP(=O)(OCC)OCC DQWPFSLDHJDLRL-UHFFFAOYSA-N 0.000 description 1
- HSMVPDGQOIQYSR-KGENOOAVSA-N triflumizole Chemical compound C1=CN=CN1C(/COCCC)=N/C1=CC=C(Cl)C=C1C(F)(F)F HSMVPDGQOIQYSR-KGENOOAVSA-N 0.000 description 1
- WVLBCYQITXONBZ-UHFFFAOYSA-N trimethyl phosphate Chemical compound COP(=O)(OC)OC WVLBCYQITXONBZ-UHFFFAOYSA-N 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
- UWSCPROMPSAQOL-UHFFFAOYSA-N trimethylazanium;sulfate Chemical compound CN(C)C.CN(C)C.OS(O)(=O)=O UWSCPROMPSAQOL-UHFFFAOYSA-N 0.000 description 1
- CNUJLMSKURPSHE-UHFFFAOYSA-N trioctadecyl phosphite Chemical compound CCCCCCCCCCCCCCCCCCOP(OCCCCCCCCCCCCCCCCCC)OCCCCCCCCCCCCCCCCCC CNUJLMSKURPSHE-UHFFFAOYSA-N 0.000 description 1
- QOQNJVLFFRMJTQ-UHFFFAOYSA-N trioctyl phosphite Chemical compound CCCCCCCCOP(OCCCCCCCC)OCCCCCCCC QOQNJVLFFRMJTQ-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 description 1
- FIQMHBFVRAXMOP-UHFFFAOYSA-N triphenylphosphane oxide Chemical compound C=1C=CC=CC=1P(C=1C=CC=CC=1)(=O)C1=CC=CC=C1 FIQMHBFVRAXMOP-UHFFFAOYSA-N 0.000 description 1
- OOZKMYBQDPXENQ-UHFFFAOYSA-N tris(2,3-diethylphenyl) phosphite Chemical compound CCC1=CC=CC(OP(OC=2C(=C(CC)C=CC=2)CC)OC=2C(=C(CC)C=CC=2)CC)=C1CC OOZKMYBQDPXENQ-UHFFFAOYSA-N 0.000 description 1
- KOWVWXQNQNCRRS-UHFFFAOYSA-N tris(2,4-dimethylphenyl) phosphate Chemical compound CC1=CC(C)=CC=C1OP(=O)(OC=1C(=CC(C)=CC=1)C)OC1=CC=C(C)C=C1C KOWVWXQNQNCRRS-UHFFFAOYSA-N 0.000 description 1
- AJHKJOCIGPIJFZ-UHFFFAOYSA-N tris(2,6-ditert-butylphenyl) phosphite Chemical compound CC(C)(C)C1=CC=CC(C(C)(C)C)=C1OP(OC=1C(=CC=CC=1C(C)(C)C)C(C)(C)C)OC1=C(C(C)(C)C)C=CC=C1C(C)(C)C AJHKJOCIGPIJFZ-UHFFFAOYSA-N 0.000 description 1
- WTLBZVNBAKMVDP-UHFFFAOYSA-N tris(2-butoxyethyl) phosphate Chemical compound CCCCOCCOP(=O)(OCCOCCCC)OCCOCCCC WTLBZVNBAKMVDP-UHFFFAOYSA-N 0.000 description 1
- WGKLOLBTFWFKOD-UHFFFAOYSA-N tris(2-nonylphenyl) phosphite Chemical compound CCCCCCCCCC1=CC=CC=C1OP(OC=1C(=CC=CC=1)CCCCCCCCC)OC1=CC=CC=C1CCCCCCCCC WGKLOLBTFWFKOD-UHFFFAOYSA-N 0.000 description 1
- QEEHNBQLHFJCOV-UHFFFAOYSA-N tris(2-phenylphenyl) phosphate Chemical compound C=1C=CC=C(C=2C=CC=CC=2)C=1OP(OC=1C(=CC=CC=1)C=1C=CC=CC=1)(=O)OC1=CC=CC=C1C1=CC=CC=C1 QEEHNBQLHFJCOV-UHFFFAOYSA-N 0.000 description 1
- LIPMRGQQBZJCTM-UHFFFAOYSA-N tris(2-propan-2-ylphenyl) phosphate Chemical compound CC(C)C1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C(C)C)OC1=CC=CC=C1C(C)C LIPMRGQQBZJCTM-UHFFFAOYSA-N 0.000 description 1
- QQBLOZGVRHAYGT-UHFFFAOYSA-N tris-decyl phosphite Chemical compound CCCCCCCCCCOP(OCCCCCCCCCC)OCCCCCCCCCC QQBLOZGVRHAYGT-UHFFFAOYSA-N 0.000 description 1
- QFGXDXGDZKTYFD-UHFFFAOYSA-N tris[2,3-di(propan-2-yl)phenyl] phosphite Chemical compound CC(C)C1=CC=CC(OP(OC=2C(=C(C(C)C)C=CC=2)C(C)C)OC=2C(=C(C(C)C)C=CC=2)C(C)C)=C1C(C)C QFGXDXGDZKTYFD-UHFFFAOYSA-N 0.000 description 1
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 1
- ITRNXVSDJBHYNJ-UHFFFAOYSA-N tungsten disulfide Chemical compound S=[W]=S ITRNXVSDJBHYNJ-UHFFFAOYSA-N 0.000 description 1
- 235000013799 ultramarine blue Nutrition 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- 150000003682 vanadium compounds Chemical class 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
- 229910003454 ytterbium oxide Inorganic materials 0.000 description 1
- 229940075624 ytterbium oxide Drugs 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 229940098697 zinc laurate Drugs 0.000 description 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
- 229910000165 zinc phosphate Inorganic materials 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- NDKWCCLKSWNDBG-UHFFFAOYSA-N zinc;dioxido(dioxo)chromium Chemical compound [Zn+2].[O-][Cr]([O-])(=O)=O NDKWCCLKSWNDBG-UHFFFAOYSA-N 0.000 description 1
- IJQXGKBNDNQWAT-UHFFFAOYSA-L zinc;docosanoate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCCCCCC([O-])=O IJQXGKBNDNQWAT-UHFFFAOYSA-L 0.000 description 1
- GPYYEEJOMCKTPR-UHFFFAOYSA-L zinc;dodecanoate Chemical compound [Zn+2].CCCCCCCCCCCC([O-])=O.CCCCCCCCCCCC([O-])=O GPYYEEJOMCKTPR-UHFFFAOYSA-L 0.000 description 1
- CHJMFFKHPHCQIJ-UHFFFAOYSA-L zinc;octanoate Chemical compound [Zn+2].CCCCCCCC([O-])=O.CCCCCCCC([O-])=O CHJMFFKHPHCQIJ-UHFFFAOYSA-L 0.000 description 1
- 229910000166 zirconium phosphate Inorganic materials 0.000 description 1
- LEHFSLREWWMLPU-UHFFFAOYSA-B zirconium(4+);tetraphosphate Chemical compound [Zr+4].[Zr+4].[Zr+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LEHFSLREWWMLPU-UHFFFAOYSA-B 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
Landscapes
- Luminescent Compositions (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Description
本発明の説明の前に、まず本明細書で使用する語について説明する。本願明細書及び特許請求の範囲、要約書(以下、「本願明細書等」)において、「応力発光材料」とは、外部から印加された力(圧縮、変位、摩擦、衝撃など)の力学的刺激を受けて発光する材料そのもののことをいう。この応力発光材料を単独で、又は別の素材(例えば樹脂等)と組み合わせた後、成形して得られるものを「応力発光体」という。
まず本発明の第一の態様である応力発光材料用原料組成物について説明する。この組成物は、アルミナ及び/又は水酸化アルミニウムを含有する、ユーロピウム賦活アルミン酸ストロンチウム系応力発光材料を合成するための、応力発光材料の原料となる組成物である。本組成物に含まれる上記アルミナ及び/又は水酸化アルミニウム中のαアルミナの量は所定量以下、即ち、アルミナと水酸化アルミニウムの総量に占めるαアルミナの割合は90モル%以下であり、残りはαアルミナとは異なる結晶相を有するその他のアルミナ又は水酸化アルミニウムである。
変性シリコーンとしてはポリエーテル変性シリコーン、高級脂肪酸アルコキシ変性シリコーン、高級脂肪酸含有シリコーン、高級脂肪酸エステル変性シリコーン、メタクリル変性シリコーン、及びフッ素変性シリコーン等が挙げられる。
(1)ポリオキシアルキレン型
脂肪族アルコール(C4〜30)、[アルキル(C1〜30)]フェノール、脂肪族(C4〜30)アミンおよび脂肪族(C4〜30)アミドのAO(C2〜4)1〜30モル付加物。
脂肪族アルコールとしては、n−、i−、sec−およびt−ブタノール、オクタノール、ドデカノール等;(アルキル)フェノールとしては、フェノール、メチルフェノールおよびノニルフェノール等;脂肪族アミンとしては、ラウリルアミンおよびメチルステアリルアミン等;および脂肪族アミドとしては、ステアリン酸アミド等。
(2)多価アルコール型
C4〜30の脂肪酸(ラウリン酸、ステアリン酸等)と多価(2〜6またはそれ以上)アルコール(例えばGR、PE、ソルビトールおよびソルビタン)のモノエステル化合物。
(3)カルボン酸塩型
C4〜30の脂肪酸(前記に同じ)のアルカリ金属(上記に同じ)塩。
(4)硫酸エステル型
C4〜30の脂肪族アルコール(上記に同じ)および脂肪族アルコールのAO(C2〜4)1〜30モル付加物の硫酸エステルアルカリ金属(前記に同じ)塩等。
(5)スルホン酸塩型
[アルキル(C1〜30)]フェノール(上記に同じ)のスルホン酸アルカリ金属(前記に同じ)塩。
(6)リン酸エステル型
C4〜30の脂肪族アルコール(上記に同じ)および脂肪族アルコールのAO(C2〜4)1〜30モル付加物のモノまたはジリン酸エステルの塩[アルカリ金属(上記に同じ)塩、4級アンモニウム塩等]。
(7)1〜3級アミン塩型
C4〜30の脂肪族アミン[1級(ラウリルアミン等)、2級(ジブチルアミン等)および3級アミン(ジメチルステアリルアミン等)]塩酸塩、トリエタノールアミンとC4〜30の脂肪酸(上記に同じ)のモノエステルの無機酸(塩酸、硫酸、硝酸およびリン酸等)塩。
(8)4級アンモニウム塩型
C4〜30の4級アンモニウム(ブチルトリメチルアンモニウム、ジエチルラウリルメチルアンモニウム、ジメチルジステアリルアンモニウム等)の無機酸(上記に同じ)塩等。
炭酸ストロンチウム(堺化学工業株式会社製SW−K、23.45g)、酸化ユーロピウム(信越化学工業株式会社製、0.31g)、酸化アルミニウム(岩谷化学工業株式会社製、活性アルミナRG−40(θアルミナとηアルミナの混合物、αアルミナ含有率8モル%)、17.99g)を秤量し、水(90mL)中に入れてスラリー化後、3mm径アルミナボール(株式会社ニッカトー製、SSA−999W、190g)を粉砕メディアとして使用し、遊星ボールミルを用いて分散・粉砕・混合することによりスラリーを得た。得られたスラリーを130℃にて蒸発乾燥し、得られた固形物を乳鉢で解砕して粉末状の応力発光材料用原料組成物を得た。次いで、この組成物をアルミナ製坩堝に20g充填して、還元雰囲気(2%水素含有窒素)中で200℃/時で1200℃まで昇温し、そのまま4時間保持後、200℃/時で室温まで降温した。こうして得られた焼成物を、遊星ボールミルを用いてアルコール溶媒中で粉砕して整粒し、濾過・乾燥して目的の応力発光材料を粉末として得た。粉末は結晶構造解析により分析を行った。
炭酸ストロンチウム(堺化学工業株式会社製SW−K、23.23g)、酸化ユーロピウム(信越化学工業株式会社製、0.31g)、酸化ランタン(和光純薬工業株式会社製、試薬、0.290g)、酸化アルミニウム(岩谷化学工業株式会社製、活性アルミナ、RG−40、17.87g)、を秤量し、水(90mL)中に入れてスラリー化後、3mm径アルミナボール(株式会社ニッカトー製、SSA−999W、190g)を粉砕メディアとして使用し、遊星ボールミルを用いて分散・粉砕・混合することによりスラリーを得た。得られたスラリーを130℃にて蒸発乾燥し、得られた固形物を乳鉢で解砕して粉末状の応力発光材料用原料組成物を得た。次いで、この組成物をアルミナ製坩堝に20g充填して、還元雰囲気(2%水素含有窒素)中で200℃/時で1200℃まで昇温し、そのまま4時間保持後、200℃/時で室温まで降温した。こうして得られた焼成物を、遊星ボールミルを用いてアルコール溶媒中で粉砕して整粒し、濾過・乾燥して目的の応力発光材料を粉末として得た。
酸化ランタンを酸化セリウム(和光純薬工業株式会社製、試薬、0.30g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化ネオジム(和光純薬工業株式会社製、試薬、0.30g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酢酸サマリウム四水和物(和光純薬工業株式会社製、試薬、0.700g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化ガドリニウム(和光純薬工業株式会社製、試薬、0.32g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化テルビウム(和光純薬工業株式会社製、試薬、0.33g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酢酸ジスプロシウム四水和物(和光純薬工業株式会社製、試薬、0.72g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化ホルミウム(和光純薬工業株式会社製、試薬、0.33g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化エルビウム(和光純薬工業株式会社製、試薬、0.34g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化ランタンを酸化イッテルビウム(和光純薬工業株式会社製、試薬、0.35g)に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、高活性アルミナであるRK−40(ベーマイトとθアルミナとηアルミナの混合物の混合物、αアルミナ含有率1モル%、岩谷化学工業株式会社製)に変更したこと以外は実施例1と同様にして応力発光材料を粉末として得た。粉末は結晶構造解析により分析を行った。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例3と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例4と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例5と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例6と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例7と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例8と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例9と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例10と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、前述のRK−40に変更したこと以外は実施例11と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、RH−40(バイヤライトとベーマイトの混合物、岩谷化学工業株式会社製)を25.15g用いたこと以外は実施例1と同様にして応力発光材料を粉末として得た。粉末は結晶構造解析により分析を行った。
酸化アルミニウムの代わりに、前述のRH−40を24.98g用いたこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.98g用いたこと以外は実施例3と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.97g用いたこと以外は実施例4と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.96用いたこと以外は実施例5と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.95g用いたこと以外は実施例6と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.95g用いたこと以外は実施例7と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.94g用いたこと以外は実施例8と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.94g用いたこと以外は実施例9と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.94g用いたこと以外は実施例10と同様にして応力発光材料を粉末として得た。
酸化アルミニウムの代わりに、前述のRH−40を24.93g用いたこと以外は実施例11と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40(αアルミナ含有率98モル%、岩谷化学工業株式会社製)に変更したこと以外は実施例1と同様にして応力発光材料を粉末として得た。粉末は結晶構造解析により分析を行った。
酸化アルミニウムを、RA−40に変更したこと以外は実施例2と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例3と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例4と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例5と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例6と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例7と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例8と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例9と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例10と同様にして応力発光材料を粉末として得た。
酸化アルミニウムを、RA−40に変更したこと以外は実施例11と同様にして応力発光材料を粉末として得た。
酸化アルミニウムとして、RA−40(αアルミナ含有率98モル%、岩谷化学工業株式会社製)とRG−40(活性アルミナ、θアルミナとηアルミナの混合物、αアルミナ含有率8モル%、岩谷化学工業株式会社製)をαアルミナの含有量が表2記載の割合になるように混合して用いたこと以外は、実施例1と同様にして応力発光材料を粉末として得た。
Claims (3)
- 応力発光材料用原料組成物の焼成物である応力発光材料であって、
前記原料組成物は、アルミナ及び/又は水酸化アルミニウムを含有する、ユーロピウム賦活アルミン酸ストロンチウム系応力発光材料を合成するための応力発光材料用原料組成物であり、前記アルミナ及び/又は水酸化アルミニウム中のαアルミナの割合が90モル%以下であり、さらに共賦活剤として、Nd、Dy及びHoからなる群より選択される少なくとも1種を含有する組成物である
応力発光材料。 - 請求項1に記載の応力発光材料を含有する応力発光性塗料組成物。
- 請求項1に記載の応力発光材料を含有する樹脂組成物。
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